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51.
52.
This work aims to quantify sulfate ion concentrations in the system Na2SO4-H2O using Raman micro-spectroscopy.Raman spectra of sodium sulfate solutions with known concentrations were collected at ambient temperature(293 K) and in the 500 cm1-4000 cm-1 spectral region.The results indicate that the intensity of the SO42- band increases with increasing concentrations of sulfate ion.A linear correlation was found between the concentration of SO42-(c) and parameter I1,which represents the ratio of the area of the SO42- band to that of the O-H stretching band of water(As/Aw):I1=-0.00102+0.01538 c.Furthermore,we deconvoluted the O-H stretching band of water(2800 cm-1-3800 cm-1) at 3232 and 3430 cm-1 into two sub-Gaussian bands,and then defined Raman intensity of the two sub-bands as ABi(3232 cm-1) and AB2(3430 cm-1),defined the full width of half maximum(FWHM) of the two sub-bands as WB1(3232 cm-1) and WB2(3430 cm-1).A linear correlation between the concentration of SO42-(c) and parameter I2,which represents the ratio of Raman intensity of SO42-(As)(in 981 cm-1) to(AB1+AB2),was also established:I2=-0.0111+0.3653 c.However,no correlations were found between concentration of SO42-(c) and FWHM ratios,which includes the ratio of FWHM of SO42-(Ws) to WB1 WB2 and WB1+B2(the sum of WB1 and WB2),suggesting that FWHM is not suitable for quantitative studies of sulfate solutions with Raman spectroscopy.A comparison of Raman spectroscopic studies of mixed Na2SO4 and NaCI solutions with a constant SO42- concentration and variable CI- concentrations suggest that the I\ parameter is affected by CI-,whereas the I2 parameter was not.Therefore,even if the solution is not purely Na2SO4-H2O,SO42- concentrations can still be calculated from the Raman spectra if the H2O band is deconvoluted into two sub-bands,making this method potentially applicable to analysis of natural fluid inclusions. 相似文献
53.
贵州铁(稀土)多金属矿资源储量丰厚,但是因其赋存条件的特殊性,勘查具有一定的挑战性,在此开展铁(稀土)多金属矿的物探方法试验研究,对今后勘查工作具有重要的指导意义。这里简要介绍了AMT(音频大地电磁法)工作方法以及贵州威宁秋木构工区的地质和地球物理特征,重点讨论了AMT在秋木构工区铁(稀土)多金属矿勘查中的应用效果,通过对电阻率断面图的综合推断解释,划分出了二叠系宣威组与峨嵋山玄武岩组地层界面,圈出了含矿有利部位。经钻孔验证,取得了良好的找矿效果。 相似文献
54.
对长岭凹陷深层天然气藏储层——营城组火山岩中发育的流体包裹体进行了详细研究,结果表明在火山岩发育的石英、方解石细网脉中均存在较多的碳质流体包裹体,单个包裹体激光拉曼光谱分析结果表明其主要为CO2及CH4两种类型的碳质包裹体。其中方解石细网脉体中发育有原生及次生CH4包裹体,而含CO2包裹体多以原生包裹体产于石英细网脉中。很多含CO2包裹体的石英细脉中发现了含CH4包裹体的方解石脉体的角砾,这就表明石英细脉形成晚于方解石细脉。营城组火山岩储层中CO2及CH4包裹体的产状特征研究表明,松辽盆地深层天然气藏的形成系火山岩成岩后CO2及CH4等气体不同期次充注的结果,CH4气的充注时间早于CO2气,火山岩中发育的原生孔隙及次生裂隙为上述气体的充注和聚集提供了重要通道。 相似文献
55.
长安金矿位于哀牢山成矿带南段,是该成矿带上新近发现的又一大型金矿床。该区为哀牢山地体边缘地壳增生带,主要由深变质岩系组成,区内构造断裂发育,对岩浆活动和成矿作用有显著影响。本文总结了长安金矿的地质特征,并以该区的控矿断裂F6为主要研究目标,以地层岩性电性特征作为约束条件,分别展开了磁法、激电、瞬变电磁和大地电磁等综合物探手段的试验研究。研究结果表明,磁法对于该矿找矿效果不明显,瞬变电磁和大地电磁测深反演的电阻率低阻体,准确界定了控矿断裂F6的位置、倾向、断距以及深部延伸情况,通过激电异常可大致判断矿体的位置。所以在长安金矿区下一步的深部隐伏矿勘查中,结合瞬变电磁、激电、大地电磁等地球物理方法,辅以土壤化探异常进行约束,可以达到快速有效找矿之目的。 相似文献
56.
《Chemie der Erde / Geochemistry》2015,75(1):65-72
This study was conducted on recent desert samples—including (1) soils, (2) plants, (3) the shell, and (4) organic matter from modern specimens of the land snail Eremina desertorum—which were collected at several altitudes (316–360 m above sea level) from a site in the New Cairo Petrified Forest. The soils and shellE. desertorum were analyzed for carbonate composition and isotopic composition (δ18O, δ13C). The plants and organic matterE. desertorum were analyzed for organic carbon content and δ13C. The soil carbonate, consisting of calcite plus minor dolomite, has δ18O values from −3.19 to −1.78‰ and δ13C values −1.79 to −0.27‰; covariance between the two values accords with arid climatic conditions. The local plants include C3 and C4 types, with the latter being dominant. Each type has distinctive bulk organic carbon δ13C values: −26.51 to −25.36‰ for C3-type, and −13.74 to −12.43‰ for C4-type plants.The carbonate of the shellE. desertorum is composed of aragonite plus minor calcite, with relatively homogenous isotopic compositions (δ18Omean = −0.28 ± 0.22‰; δ13Cmean = −4.46 ± 0.58‰). Most of the δ18O values (based on a model for oxygen isotope fractionation in an aragonite-water system) are consistent with evaporated water signatures. The organic matterE. desertorum varies only slightly in bulk organic carbon δ13C values (−21.78 ± 1.20‰) and these values suggest that the snail consumed more of C3-type than C4-type plants. The overall offset in δ13C values (−17.32‰) observed between shellE. desertorum carbonate and organic matterE. desertorum exceeds the value expected for vegetation input, and implies that 30% of carbon in the shellE. desertorum carbonate comes from the consumption of limestone material. 相似文献
57.
58.
Satellite data obtained over synoptic data-sparse regions such as an ocean contribute toward improving the quality of the initial state of limited-area models. Background error covariances are crucial to the proper distribution of satellite-observed information in variational data assimilation. In the NMC (National Meteorological Center) method, background error covariances are underestimated over data-sparse regions such as an ocean because of small differences between different forecast times. Thus, it is necessary to reconstruct and tune the background error covariances so as to maximize the usefulness of the satellite data for the initial state of limited-area models, especially over an ocean where there is a lack of conventional data. In this study, we attempted to estimate background error covariances so as to provide adequate error statistics for data-sparse regions by using ensemble forecasts of optimal perturbations using bred vectors. The background error covariances estimated by the ensemble method reduced the overestimation of error amplitude obtained by the NMC method. By employing an appropriate horizontal length scale to exclude spurious correlations, the ensemble method produced better results than the NMC method in the assimilation of retrieved satellite data. Because the ensemble method distributes observed information over a limited local area, it would be more useful in the analysis of high-resolution satellite data. Accordingly, the performance of forecast models can be improved over the area where the satellite data are assimilated. 相似文献
59.
In this study,the authors introduce a new bogus data assimilation method based on the dimension-reduced projection 4-DVar,which can resolve the cost function directly in low-dimensional space.The authors also try a new method to improve the quality of samples,which are the base of dimension-reduced space projection bogus data assimilation (DRP-BDA).By running a number of numerical weather models with different model parameterization combinations on the typhoon Sinlaku,the authors obtained two groups of samples with different spreads and similarities.After DRP-BDA,the results show that,compared with the control runs,the simulated typhoon center pressure can be deepened by more than 20 hPa to 30 hPa and that the intensity can last as long as 60 hours.The mean track error is improved after DRP-BDA,and the structure of the typhoon is also improved.The wind near the typhoon center is enhanced dramatically,while the warm core is moderate. 相似文献
60.
This paper discusses an important issue related to filter divergence in the dimension-reduced projection,four-dimensional variational data assimilation(DRP-4-DVar) approach.Idealized experiments with the Lorenz-96 model over a period of 200 days showed that the amplitudes of the root mean square errors(RMSEs) reached the same levels as those of the state variables after approximately 100 days because of the accumulation of sampling errors following the cycle of assimilation.Strategies to reduce sampling errors are critical to ensure the quality of ensemble-based assimilation.Numerical experiments showed that localization and reducing observational errors can alleviate,but cannot completely overcome,the filter divergence in the DRP-4-DVar approach,while the method of perturbing observations and the inflation technique can efficiently eliminate the filter divergence problem. 相似文献