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The International Atomic Energy Agency (IAEA) organised a proficiency test (PT), IAEA‐CU‐2010‐02, for the determination of elements in sewage sludge. The PT sample was analysed by semi‐absolute standardless k0‐instrumental neutron activation analysis (k0‐INAA). Results for seven elements (As, Co, Cr, Fe, Hg, Se, Zn) were submitted to the IAEA by our laboratory. All of our results were scored ‘acceptable’ by the ‘result evaluation criteria’ adopted by the IAEA. The same analytical methodology produced quantitative results for twenty‐six additional elements. In total, thirty‐six elements were determined with uncertainty varying from 4 to 11%. This paper presents the provisional mass fractions of twenty‐six additional elements (Ag, Al, Br, Ca, Ce, Cl, Dy, Eu, Ga, Hf, I, K, La, Mg, Mn, Na, Rb, Sb, Sc, Sm, Ta, Tb, Th, V, U, W) not reported by the IAEA. The analytical methodology was discussed with important sources of spectral, nuclear and fission‐product interferences. It was shown that the important components of uncertainties were the k0 factor, Q0 factor, detector efficiency, mass and counting statistics. The methodology was validated by analysing the IAEA‐S7 reference material.  相似文献   
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We report an approach for the accurate and reproducible measurement of boron isotope ratios in natural waters using an MC‐ICP‐MS (Neptune) after wet chemistry sample purification. The sample matrix can induce a drastic shift in the isotopic ratio by changing the mass bias. It is shown that, if no purification is carried out, the direct measurement of a seawater diluted one hundred times will induce an offset of ?7‰ in the isotopic ratio, and that, for the same concentration, the greater the atomic mass of the matrix element, the greater the bias induced. Whatever the sample, it is thus necessary to remove the matrix. We propose a method adapted to water samples allowing purification of 100 ng of boron with a direct recovery of boron in 2 ml of 3% v/v HNO3, which was our working solution. Boron from the International Atomic Energy Agency IAEA‐B1 seawater reference material and from the two groundwater reference materials IAEA‐B2 and IAEA‐B3, was chemically purified, as well as boron from the certified reference material NIST SRM 951 as a test. The reproducibility of the whole procedure (wet chemistry and MC‐ICP‐MS measurement) was ± 0.4‰ (2s). Accuracy was verified by comparison with positive‐TIMS values and with recommended values. Seawater, being homogeneous for boron isotope ratios, is presently the only natural water material that is commonly analysed for testing accuracy worldwide. We propose that the three IAEA natural waters could be used as reference samples for boron isotopes, allowing a better knowledge of their isotopic ratios, thus contributing to the certification of methods and improving the quality of the boron isotopic ratio measurements for all laboratories.  相似文献   
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Starting from the 1980's of last century, China has launched the national plan of constructing nuclear power plants along the coastline region in eastern China. Currently, in some of these candidate sites, nuclear facilities have been installed and are in operation, but some other nuclear power plants are still under construction or in site evaluation. In 2012 the Atomic Energy Commission issued the specific guide for volcanic hazards in site evaluation for nuclear installations(IAEA Safety Standards Series No. SSG-21), which was prepared under the IAEA's program for safety standards. It supplements and provides recommendations for meeting the requirements for nuclear installations established in the safety requirements publication on site evaluation for nuclear installations in relation to volcanic hazards. To satisfy the safety standards for volcanic hazard, we follow the IAEA SSG-21 guidelines and develop a simple and practical diffusion program in order to evaluate the potential volcanic hazard caused by tephra fallout from the explosive eruptions. In this practice, we carried out a case study of the active volcanoes in north Hainan Province so as to conduct the probabilistic analysis of the potential volcanic hazard in the surrounding region. The Quaternary volcanism in north Hainan Island, so-called Qiongbei volcanic field is characterized by multi periodic activity, in which the most recent eruption is dated at about 4 000a BP. According to IAEA SSG-21, a capable volcano is one for which both 1)a future eruption or related volcanic event is credible; and 2)such an event has the potential to produce phenomena that may affect a site. Therefore, the Qiongbei volcanic field is capable of producing hazardous phenomena that may reach the potential nuclear power plants around. The input parameters for the simulation of tephra fallout from the future eruption of the Qiongbei volcanic field, such as the size, density and shape of the tephra, the bulk volume and column height, the diffusion parameter P(z), wind direction and intensity, were obtained by field investigation and laboratory analysis. We carried out more than 10000 tephra fallout simulations using a statistical dataset of wind profiles which are obtained from China Meteorological Data Sharing Service System(CMDSSS). Tephra fallout hazard probability maps were constructed for tephra thickness threshold of 1cm. Our results show that the tephra produced by the future large-scale explosive eruption from the Qiongbei volcanic field can affect the area in a range about 250km away from the eruption center. In summary, the current key technical parameters related to volcanic activity and potential hazards in IAEA/SSG-21 guidelines, such as 10Ma volcanic life cycle and 1×10-7 volcanic disaster screening probability threshold, etc. are based on the volcanic activity characteristics in the volcanic island arc system. In consideration of the relatively low level of volcanic activity compared with volcanic island arc system due to the different tectonic background of volcanism in mainland China, the time scale of volcanic disaster assessment in IAEA SSG-21 guideline is relatively high for volcanoes in mainland China. We suggest that the study of "conceptual model" of volcanic activity should be strengthened in future work to prove that there is no credible potential for future eruptions, so that these volcanoes should be screened out at early stage instead of further evaluation by probabilistic model.  相似文献   
4.
潘华  吴健 《震灾防御技术》2006,1(2):121-128
本文分析了国际原子能机构新颁布的安全导则“EvaluationofSeismicHazardsforNuclearPowerPlants(NS-G-3.3)”与前版导则相比在内容、方法上的一些显著的变化;同时,结合我国核电厂厂址地震安全性评价的方法和实践,对该新版导则在我国的引进和应用中应该注意的问题,进行了评述。  相似文献   
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