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使用盐湖提锂镁渣和矿物掺合料,如粉煤灰、硅灰和矿渣等,与磷酸二氢钾反应,制作磷酸钾镁水泥(Magnesium Potassium Phosphate Cement,MKPC)。研究了MgO/KH2PO4摩尔配比(M/K)和矿物掺合料对MKPC凝结时间、抗压强度和水化放热速率的影响,并使用X射线衍射(X-ray diffraction,XRD)和低真空扫描电子显微镜(Scanning Electron Microscopy,SEM)分析MKPC的水化产物。研究表明,M/K对MKPC抗压强度影响显著,最佳M/K为4~6。M/K为5时,MKPC在各龄期的抗压强度值均较高,28d抗压强度高达98MPa。掺加矿物掺合料会降低MKPC的抗压强度,当粉煤灰、硅灰和矿渣的掺量分别为水泥质量的20%,10%和20%时,28d抗压强度可以分别达到45.9MPa、33.3MPa和36.7MPa。凝结时间超过20min,能够满足快速修复的要求。在不考虑Mg3B2O6的影响下,掺加矿物掺合料会延缓MKPC凝结时间和降低放热速率。 相似文献
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掺砂水泥土的力学特性研究 总被引：3，自引：0，他引：3
通过室内掺砂水泥土的无侧限抗压强度试验,探讨在不同掺砂量、不同龄期条件下,其无侧限抗压强度发展规律。试验研究表明：在水泥掺量一定的条件下,掺入一定量的砂,可以明显地提高水泥土的强度。当水泥掺量为10%时,掺砂量为50%的水泥土强度达到最佳。而且根据实测的应力-应变曲线,详细地分析了掺砂水泥土的破坏形式为脆性剪切破坏,且随着掺砂量的增加,掺砂水泥土的剪切角逐渐增大。与此同时,还从不同的角度分析了掺砂水泥土无侧限抗压强度增长的原因,从而为工程应用提供了试验数据和理论依据。 相似文献
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This paper presents the results of a series of studies on the influence of curing conditions onthe strength development of high strength concrete.The 1-,3-,7-,14-and 28-day strengths of four dif-ferent mixes of Grade 75～80 concrete,with or without pulverized fuel ash and/or condensed silica fume,under five different curing regimes were investigated.It is revealed that the curing conditions have signifi-cant influence on both the short term and long term strength development of the concrete and that con-crete mixes of the same grade but containing different mineral admixtures show distinct favour for a cur-ing regime.These results will be helpful for evaluating suitable curing methods for high strength concretewith different mix proportions. 相似文献
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Stabilization of fuel oil contaminated soil—A case study 总被引：1，自引：0，他引：1
Sanjay J. Shah A. V. Shroff Jignesh V. Patel K. C. Tiwari D. Ramakrishnan 《Geotechnical and Geological Engineering》2003,21(4):415-427
Fuel oil contamination brings adverse effect on basic geotechnical properties of foundation soil. The present study pertains to one such case, from the petrochemical complex near Vadodara City in Gujarat State, India. Here, the fuel oil contaminated soil samples exhibit drastic changes in their geotechnical parameters. Noteworthy among such deleterious changes are: decrease in maximum dry density (–4%), cohesion (–66%), angle of internal friction (–23%) and unconfined compressive strength (UCS) (–35%) and increase in liquid limit (+11%). An attempt has been made to stabilize the contaminated soil using various additives viz., lime, fly ash and cement independently as well as an admixture of different combinations. It is apparent from the test results that the stabilization agents improved the geo-technical properties of the soil by way of cation exchange, agglomeration, and pozzuolanic actions. The best results were observed when a combination of 10% lime, 5% fly ash and 5% cement was added to the contaminated soil. The improvement in unconfined compressive strength (UCS), cohesion and angle of internal friction can be attributed to neo-formations such as Calcium Silicate Hydrates (CSH, CSH-1) that coats and binds the soil particles. Formation of stable complex between oil and metallic cations, results in reduction of leachableoil. 相似文献
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预应力管道压浆浆液外加剂种类及配合比的选取是管道压浆工艺的重要部分。为研究减水剂和矿物掺和料对管道压浆浆液的影响及作用机理,进而研制一种流动性、保水性及力学性能优异的管道压浆浆液,本研究采用单组分掺和试验的方法,对掺有减水剂与矿物掺合料两种不同压浆浆料进行流动性、压力泌水率、沉积密度比、抗压及抗折性能试验研究,并得到不同掺量外加剂对压浆浆液和易性与力学性能的影响和作用机理,以及合适的外加剂掺量配比。研究表明：聚羧酸减水剂30 min与60 min流动度最佳,且压力泌水率表现也较为良好,综合考虑聚羧酸减水剂为压浆浆液的优良减水剂;聚羧酸减水剂掺量在0.4%～0.5%时,浆液的流动性与保水性表现良好,随掺量的继续增加,流动性提升较小;微珠由于其物理性质以及化学性质,对提高压浆浆液和易性与力学性能的效果较为明显;微珠掺量在10%～15%时,压浆浆液的和易性达到临界状态。 相似文献
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水泥-水玻璃浆液在灌浆、堵水等工程中具有广泛的应用,而浆液的凝固特性对灌浆、堵水效果具有直接的影响。在对水泥-水玻璃浆液凝结硬化机理分析的基础上,对不同水灰比浆液的胶凝时间和流动度进行了试验研究,并对FDN、SM、NF、UNF-5、柠檬酸、多聚磷酸钠、酒石酸钾钠、酒石酸、磷酸氢二钠等外加剂对浆液凝固特性的影响进行了对比试验研究。在此基础上重点对磷酸氢二钠的缓凝性能进行了试验分析,初步获得了磷酸氢二钠对水泥-水玻璃浆液的凝固性能的影响规律。最后按初凝时间设计了几种水泥-水玻璃浆液的配方。 相似文献
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电感耦合等离子体原子发射光谱法(ICP-AES)测定纯铜中多种杂质元素 总被引：1，自引：0，他引：1
本文采用电感耦合等离子体发射光谱法同时测定纯铜中的Fe、P、Cd、Co、Mn、Ni、Pb、Zn、As、Sb、Bi、Sn、S、Ag、Se、Cr、Si、Mg、Te、Al、Ti、Hg、Be、Zr、B等25种杂质元素,并以差减法计算基体铜的含量,实现了对试样基体及杂质元素含量的同时测定。以基体匹配法配制工作曲线,有效地消除基体干扰。结果表明该方法对25种杂质元素的回收率在94~103.5%,相对标准偏差低于3.0%。方法简单、快速,测定结果满意。 相似文献
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