Z-2700石墨炉原子吸收测定化探样品中痕量金     

萧莲萍  王作华  陈义 《吉林地质》2011,30(3):96-97,101

本文采用泡塑富集化探样品中痕量金,用石墨炉原子吸收法测定痕量金。试样经灼烧,王水密封溶矿,泡塑富集,硫脲解脱等过程进行了改进及条件控制,该方法具有检出限低,灵敏度高,操作简便,速度快,劳动强度小,适用地质化探样品中痕量金的测定。  相似文献   

近岸波生流运动三维数值模拟及验证   总被引：3，自引：0，他引：3       下载免费PDF全文

解鸣晓  张玮 《水科学进展》2011,22(3):391-399

开发建立了近岸波生流运动三维数值计算模式。模式中,引入了三维时均剩余动量、破波表面水滚、波浪水平与垂向紊动作为主要驱动力,同时考虑了波流共同作用的底部剪切力。推导了可综合反映底坡、能量传递率和密度影响的水滚能量传输方程;将Larson-Kraus的二维波浪水平紊动系数表达式拓展至三维。采用大量实测数据和文献资料测试验证了所建模式,表明所建模式可有效模拟波浪增减水、底部离岸流、沿岸流、裂流、堤后环流等不同维度的波生流现象。此外,研究也表明破波水滚效应可解释波生流峰值向岸推移的物理现象,从而在模拟中不能忽略;破波带内沿岸流速垂向较为均匀的现象与波浪附加垂向紊动有关。  相似文献   

塞曼石墨炉原子吸收法测定地球化学样品中银元素     

白志斌 《西部资源》2011,(5):55-56

对塞曼效应石墨炉原子吸收法对地质样中痕量银的测定进行了研究。简化了样品处理过程。对地质标样及实际样品分析获得了满意的结果加标回收率为96.2%-103.5%,相对标准偏差为3.04%-4.77%所采用的方法快速、简便,准确。  相似文献   

快速程序升温-石墨炉原子吸收光谱法测定地质样品中痕量镉     

吴峥  牟乃仓  王龙山  张飞鸽  高登峰  王光照 《岩矿测试》2011,30(2):186-189

建立了快速程序升温-石墨炉原子吸收光谱测定地质样品中痕量镉的分析方法.样品用硝酸-氢氟酸-高氯酸进行前处理,为提高分析效率,改进了石墨炉升温程序,省去了常规方法中的灰化步骤,使测定镉的程序升温时间由常规的90～100 s降至24 s,工作效率显著提高.方法检出限为0.011 μg/g,加标回收率为93.5%～106.0...  相似文献   

Design principle for parameters and interferences of tungsten carbide insert interface on roller bits          下载免费PDF全文

YIN Kun  JONG Yonchol  BO Kun  CHOE Jongman 《世界地质(英文版)》2013,16(1):43-47

The lifetime of roll-bits with inserted tooth will be obviously decreased while drilling in strata and the tungsten carbide can be integrally separated from the roll-cone,which will need more trip out time to replace the roller bit.This study provides an entire analysis on stress as well as strength for teeth and tooth holes in loaded conditions.Qualities of tooth drop from matrix within roller bit.The optimized interferences of teeth inserted into the bit can be reasonably obtained by the critical interference derived from some relevant influence factors on the tooth-fixing quality of roller bits.  相似文献   

Testing of dynamically substructured,base‐isolated systems using adaptive control techniques     

J. Y. Tu  P. Y. Lin  D. P. Stoten  G. Li 《地震工程与结构动力学》2010,39(6):661-681

Experimental techniques for testing dynamically substructured systems are currently receiving attention in a wide range of structural, aerospace and automotive engineering environments. Dynamic substructuring enables full‐size, critical components to be physically tested within a laboratory (as physical substructures), while the remaining parts are simulated in real‐time (as numerical substructures). High quality control is required to achieve synchronization of variables at the substructuring interfaces and to compensate for additional actuator system(s) dynamics, nonlinearities, uncertainties and time‐varying parameters within the physical substructures. This paper presents the substructuring approach and associated controller designs for performance testing of an aseismic, base‐isolation system, which is comprised of roller‐pendulum isolators and controllable, nonlinear magnetorheological dampers. Roller‐pendulum isolators are typically mounted between the protected structure and its foundation and have a fundamental period of oscillation far‐removed from the predominant periods of any earthquake. Such semi‐active damper systems can ensure safety and performance requirements, whereas the implementation of purely active systems can be problematic in this respect. A linear inverse dynamics compensation and an adaptive controller are tailored for the resulting nonlinear synchronization problem. Implementation results favourably compare the effectiveness of the adaptive substructuring method against a conventional shaking‐table technique. A 1.32% error resulted compared with the shaking‐table response. Ultimately, the accuracy of the substructuring method compared with the response of the shaking‐table is dependent upon the fidelity of the numerical substructure. Copyright © 2009 John Wiley & Sons, Ltd.  相似文献   

高温炉燃烧-红外吸收法测定重铀酸盐中硫质量分数     

刘香英  崔建勇  刘高辉  袁建  夏晨光 《铀矿地质》2017,(3):170-173

建立了高温燃烧红外碳硫仪测定重铀酸盐中硫质量分数的分析方法。样品以五氧化二钒为助熔剂,在高温炉燃烧后,用红外吸收测定重铀酸盐中的硫,样品分析重现性好,精密度高,相对标准偏差为0.26%;样品加标回收率在97.1%~103%之间。  相似文献   

砂砾石大坝填筑碾压的相关试验与研究          下载免费PDF全文

张朋辉  韩赛超  李晓帅  张小东 《探矿工程》2017,44(5):72-77

针对南疆砂砾石填筑大坝进行碾压试验，验证坝体填筑设计压实标准的合理性、检验22 t自行式振动碾的适用性及其性能的可靠性。本试验主要采用室内相对密度试验、现场的碾压测定出碾压遍数、碾压沉降及相应密实度及其他试验参数，通过试验参数列表、试验参数包络线图与设计标准值的比较，得出最佳砂砾石填筑方案，同时也确定大坝填筑时的施工碾压控制参数，从而确保了工程质量。  相似文献   

塞曼石墨炉原子吸收法直接测定海水中的铜     

李攻科  黄卓尔  杨秀环  张展霞 《热带海洋学报》1991,(2)

本文选择酒石酸消除海水基体对铜信号的干扰,用塞曼石墨炉原子吸收法直接测定海水中的铜。从Cu的原子化曲线可知,加入酒石酸后,背景值减小,Cu原子吸收信号增强,且出现时间提前,表明酒石酸是有效的海水基体改进剂。用P.E.Z3030光谱仪测得双蒸水及海水中的元素Cu的特征质量(m。)分别为12.5pg及12.7pg;检测限分别为0.18μg/L和0.19μg/L,表明基体效应已消除,符合海洋监测要求。可用纯Cu标准溶液作校正曲线,以国家海洋局的两个标准海水样品中的Cu评定本法的准确度,相对偏差为0及-4.6%,与经典的经富集后的FAAS法的结果相比,相对偏差在3.0—6.5％范围内。用不同类型的光谱仪测定了30个海水样品,回收率在89—104％范围内。本法操作简便、快速。  相似文献   

Boussinesq-type modelling using an unstructured finite element technique     

Ole R. Srensen  Hemming A. Schffer  Lars S. Srensen 《Coastal Engineering》2004,50(4):181-198

A model for solving the two-dimensional enhanced Boussinesq equations is presented. The model equations are discretised in space using an unstructured finite element technique. The standard Galerkin method with mixed interpolation is applied. The time discretisation is performed using an explicit three-step Taylor–Galerkin method. The model is extended to the surf and swash zone by inclusion of wave breaking and a moving boundary at the shoreline. Breaking is treated by an existing surface roller model, but a new procedure for the detection of the roller thickness is devised. The model is verified using four test cases and the results are compared with experimental data and results from an existing finite difference Boussinesq model.  相似文献