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用四种不同类型高压釜研究Na2SnF6在200--647℃,、1kbar条件下的水解特征。实验表明,淬火速率影响实验结果的精度。快速淬火高压釜及金袋摇摆釜是研究这类化学平衡反应的理想设备，采用水解法可获得水解常数及热焓。 相似文献
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由于具有优异的电学、光学、化学、力学等性能,高纯α-Al_2O_3粉体在新兴产业中具有举足轻重的作用。而通过铝粉和水之间的水解反应和焙烧工艺制备的α-Al_2O_3粉体虽然因其能耗低、环境污染小、纯度高等特点达到了产业化应用需求,但是如何实现所制备的α-Al_2O_3粉体结构、形貌和分散性可控是目前阻碍该种α-Al_2O_3粉体直接应用与高新技术领域的关键问题之一。本论文结合目前水解法制备高纯α-Al_2O_3粉体中存在的问题,首先通过改进的水解法和水热处理水解产物的方法制备了高纯γ-Al(OH)_3和γ-AlOOH前驱体,继而通过优化焙烧工艺制备出了形貌和结构可控的α-Al_2O_3粉体。 相似文献
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利用阳离子交换实验方法,将天然蛭石转化为羟基Al3+型蛭石,通过X射线衍射、差热分析,研究铝离子在蛭石层间域中的赋存状态.结果显示,Al3+交换蛭石中的层间铝不能用KCl溶液将其提取出来,但可用柠檬酸钠溶液可以将其提取出来,是一种非交换性的聚合羟基铝.Al3+的离子电势虽然很高,但Al3+交换蛭石的脱水温度却低于蛭石原矿.表明Al3+进入蛭石层间域后发生水解反应,生成Al(OH)2+和Al(OH)2+从而降低了Al3+的有效离子电势,使其脱水温度降低.Al3+进入蛭石层间域后发生水解反应,其可能的水解反应式为[Al(OH2)6]3+〈=〉[Al(OH)x(OH2)6-x]3-x+xH+,其中x＜3. 相似文献
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YU Lina WANG Dongfeng SU Lin LUO Yi SUN Liping XUEChanghu 《中国海洋大学学报(英文版)》2005,4(3):272-275
Hydrolysis activities of PACC （particle of agarose-Ce^4＋ complex, newly made through double emulsification） for compounds containing phosphodiester or peptide bonds were studied. The results showed that PACC could hydrolyze organophosphorous pesticides not only in water but also in vegetable juice or tea extract. Hydrolysis rates of methamidophos, omethoateand chlorpyrifos in water are 32.39%, 27.12% and 46.62% respectively, those of chlorpyrifos and methamidophos in mung sprout juice 38.28% and 35.45% respectively, and that of chlorpyrifos in tea extract 59.76%. Hydrolysis rates of BSA （bovine serum albumin） in water and protein in tea extract by PACC increase by 54.30% and 86.46% respectively as compared with the control. 相似文献
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Protein and RNA in lake sediments tend to be decomposed progressively with time and sedimentation depth. Their concentrations
tend to decrease starting from the sedimentation depth of 17 cm and that of 19 cm, respectively. However, the products of
their decomposition —amino acids and nucleotides show different rules of variation. At the depth from 27 cm to 30 cm the amino
acids are most abundant in the pore waters of lake sediments. Such variation tendency seems to be related to the extent to
which microbes utilize amino acids and nucleotides. Due to polymerization in the geological processes and the adsorption of
protein on minerals and organic polymers, below the sedimentation depth of 17 cm there is still a certain amount of protein
in the sediments. With the time passing by, protein has been well preserved in various sediment layers, indicating that its
decomposition is relatively limited. The peak values of protein content in the sediments of the two lakes are produced in
the surface layers at the depth of 10 cm, implicating that the surface sediments are favorable to the release of protein.
The contents of amino acids in the pore waters of lake sediments are closely related to the activities of microbes. Below
the depth of 27 cm, the amino acids are significantly accumulated in Lake Aha sediments, probably indicating the weakening
of microbial activities.
The research project was financially supported jointly by the Ntional Natural Science Foundation of China (No. 40173038) and
the Guizhou Provincial Foundation (No. 3090) and the Chinese Academy of Sciences Knowledge-Innovation Foundation (KZCX2-105). 相似文献
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