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1.
用包埋脱水法冰冻保存海洋饵料金藻 总被引:4,自引:0,他引:4
用包埋脱水法冰冻保存绿色巴夫藻(Pavlova uiridis)、湛江等鞭金藻(Isochrysis zhanjiangensis)和球等鞭金藻(Isochrysis galbana 3011)等三种海洋饵料金藻,探讨了脱水速率、胶球含水量以及化冻后恢复方法对冰冻保存存活率的影响。结果表明,三种藻都在-0.9%含水量/h的平均脱水速率下获得最高存活率:各种藻在冰冻前的胶球最佳含水量不同,绿色巴夫藻为35%,湛江等鞭金藻和球等鞭金藻都为30%。化冻后,含绿色巴夫藻的胶球在培养基中22℃暗放置48h存活率最高;另两种藻在相对湿度为75%的气相中22℃暗放置12h存活率最高。在本实验条件下,绿色巴夫藻、湛江等鞭金藻和球等鞭金藻的冰冻保存的存活率可分别达到74%、15%和17%。 相似文献
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利用Paterson气体介质高温高压流变仪对纯叶蛇纹岩在100~400MPa围压、25~700℃温度和10-5~1.5×10-6s-1应变速率下进行了三轴压缩变形实验。实验结果表明叶蛇纹石在低压条件下表现为脆性破裂,高压或脱水条件下表现为半脆性破裂。随着温度的增加,叶蛇纹石的强度显示逐渐降低的趋势;尤其在脱水条件下,温度的增加可导致叶蛇纹石强度大幅度地降低,而且此时预热时间对强度的影响比未发生脱水时更加显著。结合前人的研究并对比发现,围压在室温下的增加导致叶蛇纹岩强度增加;但在高温下围压的增加导致试样强度整体上降低,这很可能是试样内聚力的局部损失与韧性增强引起的。围压和温度的升高,以及断层面上流体的增加很可能会增加破裂面的韧性,从而减小摩擦系数。此外,叶蛇纹石并非以往人们所认为的那样具有极低的强度,其强度要比低温蛇纹石(如利蛇纹石和纤蛇纹石)的大得多,即便在高温(大约600℃)下差应力大于约600MPa和中-低温(≤400℃)下差应力大于约1000MPa时仍没有表现出明显屈服的迹象。在脱水条件下,蛇纹岩并没有发生脱水致脆,相反脱水使得试样的断裂行为变得更加温和些。因此,俯冲带蛇纹岩脱水更可能诱发其周围更加脆性的岩石发生地震而不是脱水的蛇纹岩本身发生地震。 相似文献
3.
Dehydration experiments on natural omphacites: qualitative and quantitative characterization by various spectroscopic methods 总被引:1,自引:0,他引:1
M. Koch-Müller I. Abs-Wurmbach D. Rhede V. Kahlenberg S. Matsyuk 《Physics and Chemistry of Minerals》2007,34(9):663-678
A series of natural omphacites from a wide range of P, T occurrences were investigated by electron microprobe (EMP), infrared (IR)-, Mössbauer (MS)- and optical spectroscopy in the UV/VIS spectral range (UV/VIS), secondary ion mass spectrometry (SIMS) and single crystal structure refinement by X-ray diffraction (XRD) to study the influence of hydrogen loss on valence state and site occupancies of iron. In accordance with literature data we found Fe2+ at M1 as well as at M2, and in a first approach assigned Fe3+ to M1, as indicated by MS and XRD results. Hydrogen content of three of our omphacite samples were measured by SIMS. In combination with IR spectroscopy we determined an absorption coefficient: ε i,tot = 65,000 ± 3,000 lmolH2O ?1 cm?2. Using this new ε i,tot value, we obtained water concentrations ranging from 60 to 700 ppm H2O (by weight). Hydrogen loss was simulated by stepwise heating the most water rich samples in air up to 800°C. After heat treatment the samples were analyzed again by IR, MS, UV/VIS, and XRD. Depending on the type of the OH defect, the grade of dehydration with increasing temperature is significantly different. In samples relatively poor in Fe3+ (<0.1 Fe3+ pfu), hydrogen associated with vacancies at M2 (OH bands around 3,450 cm?1) starts to leave the structure at about 550°C and is completely gone at 780°C. Hydrogen associated with Al3+ at the tetrahedral site (OH bands around 3,525 cm?1, Koch-Müller et al., Am Mineral, 89:921–931, 2004) remains completely unaffected by heat treatment up to 700°C. But all hydrogen vanished at about 775°C. However, this is different for a more Fe3+-rich sample (0.2 Fe3+ pfu). Its IR spectrum is characterized by a very intense OH band at 3,515 cm?1 plus shoulder at 3,450 cm?1. We assign this intense high-energy band to vibrations of an OH dipole associated with Fe3+ at M1 and a vacancy either at M1 or M2. OH release during heating is positively correlated with decrease in Fe2+ and combined with increase in Fe3+. That dehydration is correlated with oxidation of Fe2+ is indirectly confirmed by annealing of one sample in a gas mixing furnace at 700°C under reducing conditions keeping almost constant OH? content and giving no indication of Fe2+-oxidation. Obtained data indicate that in samples with a relatively high concentration of Fe2+ at M2 and low-water concentrations, i.e., at a ratio of Fe2+ M2/H > 10 dehydration occurs by iron oxidation of Fe2+ exclusively at the M2 site following the reaction: \( {\left[ {{\text{Fe}}^{{{\text{2 + [ M2]}}}}{\text{OH}}^{ - } } \right]} = {\left[ {{\text{Fe}}^{{{\text{3 + [ M2]}}}} {\text{O}}^{{{\text{2}} - }} } \right]} + {\text{1/2}}\;{\text{H}}_{{\text{2}}} \uparrow . \) In samples having relatively low concentration of Fe2+ at M2 but high-water concentrations, i.e., ratio of Fe2+ M2/H < 5.0 dehydration occurs through oxidation of Fe2+ at M1. 相似文献
4.
Non-volcanic deep low-frequency tremors accompanying slow slips in the southwest Japan subduction zone 总被引:5,自引:1,他引:5
Non-volcanic deep low-frequency tremors in southwest Japan exhibit a strong temporal and spatial correlation with slow slip detected by the dense seismic network. The tremor signal is characterized by a low-frequency vibration with a predominant frequency of 0.5–5 Hz without distinct P- or S-wave onset. The tremors are located using the coherent pattern of envelopes over many stations, and are estimated to occur near the transition zone on the plate boundary on the forearc side along the strike of the descending Philippine Sea plate. The belt-like distribution of tremors consists of many clusters. In western Shikoku, the major tremor activity has a recurrence interval of approximately six months, with each episode lasting over a week. The tremor source area migrates during each episode along the strike of the subducting plate with a migration velocity of about 10 km/day. Slow slip events occur contemporaneously with this tremor activity, with a coincident estimated source area that also migrates during each episode. The coupling of tremor and slow slip in western Shikoku is very similar to the episodic tremor and slip phenomenon reported for the Cascadia margin in northwest North America. The duration and recurrence interval of these episodes varies between tremor clusters even on the same subduction zone, attributable to regional difference in the frictional properties of the plate interface. 相似文献
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S. K. Deb M. H. Manghnani K. Ross R. A. Livingston P. J. M. Monteiro 《Physics and Chemistry of Minerals》2003,30(1):31-38
A Raman scattering and X-ray diffraction study of the thermal decomposition of a naturally occurring, ettringite-group crystal
is presented. Raman spectra, recorded with increasing temperature, indicate that the thermal decomposition begins at ≈55 °C,
accompanied by dehydration of water molecules from the mineral. This is in contrast to previous studies that reported higher
temperature breakdown of ettringite. The dehydration is completed by 175 °C and this results in total collapse of the crystalline
structure and the material becomes amorphous. The Raman scattering results are supported by X-ray diffraction results obtained
at increasing temperatures.
Received: 9 July 2001 / Accepted: 14 August 2002 相似文献
7.
Ductile extensional movements along the steeply inclined Hoher-Bogen shear zone caused the juxtaposition of Teplá-Barrandian
amphibolites, granulites, and metaperidotites against Moldanubian mica schists and paragneisses. Garnet pyriclasites are well
preserved within low-strain domains of this shear zone. Their degree of metamorphism is significantly higher than that of
the surrounding rocks. Microstructural and mineral chemical data suggest in situ formation of the garnet pyriclasite by dehydration
of pyroxene amphibolite at T>750–840°C and P<10–13 kbar including recrystallization-accommodated grain-size reduction of plagioclase
and clinopyroxene, nucleation of garnet, and breakdown of amphibole into garnet+clinopyroxene+rutile. Subsequent decompression
and retrograde extensional shearing led to the formation of mylonitic epidote amphibolite. The presence of lower crustal and
mantle-derived slices within the Hoher-Bogen shear zone supports the view that (a) in Upper Devonian times the Teplá-Barrandian
unit was thrust over Moldanubian rocks as a complete crustal unit, and (b) that during the subsequent Lower Carboniferous
orogenic collapse, the garnet pyriclasite and metaperidotite were scraped off from the basal parts of the Teplá-Barrandian
unit being dragged into the Hoher-Bogen shear zone due to dramatic and large-scale elevator-style movements.
Received: 23 March 1999 / Accepted: 25 August 1999 相似文献
8.
根据硼酸铝晶须合成工艺要求 ,研究了以工业一级品明矾作为反应原料的可行性 ,确定了明矾筛选、脱水、球磨及筛分工艺条件。 相似文献
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