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1.
Mössbauer spectra (MS) of blue, green and yellow beryl (ideally Be3Al2Si6O18) containing approximately 1% of iron were obtained at 295 and 500 K. Room temperature (RT) spectra of both blue and green samples showed the presence of an asymmetric Fe2+ doublet (ΔE Q~2.7 mm/s, δ~1.1 mm/s), with a very broad low-velocity peak. There is no clear evidence for the presence of a ferric component. The MS of the yellow sample at RT consists of an intense central absorption with parameters typical for Fe3+ (ΔE Q~0.4 mm/s, δ~0.29 mm/s), plus an apparently symmetrical Fe2+ doublet. This sample acquires a light-blue shade upon heating in air at about 620 K. Thermal treatments at high temperatures caused no significant changes in the MS, but the green and yellow beryl acquire a blue colour. All these results are interpreted in relation to the existence of channel water and the distribution of iron among the available crystallographic sites.  相似文献   
2.
Effect of heat treatment on tourmaline from Brazil   总被引：4，自引：0，他引：4  
The crystal-chemical behaviour of tourmaline from Araçuaí, Minas Gerais state, Brazil, when subjected to heating in air atmosphere has been studied by several techniques, including EMPA, UV–Vis, TGA, and Mössbauer spectroscopy. The tourmaline samples are typically intermediate members of the elbaite-schorl series. The origin of colour and of its change after treatment has been discussed in terms of local disorder, presence of metal transition elements, oxidation of ferrous iron at the octahedral site, and simultaneous trap of the excess electron. These findings may be used to enhance the colour in tourmaline crystals or generate wanted colour changes.  相似文献   
3.
The present study deals with the correlation between the geotectonic features of the basement and the internal structure, shape, geologic evolution, etc. of the major sedimentary basins of the South American platform. The Paraná, Parnaíba and Amazonas basins occupy an area of the order of 3.6 × 106 km2, and their sedimentary cratonic sequences were deposited from Silurian to Triassic times. Subsidence rates are estimated around 15 m/Ma in the main depocenters.A geologic study was carried out along the basement features in the surroundings of such basins in order to identify the major structural, geotectonic and geochronological discontinuities. The extension of these basement characteristics towards the interior of the basins are examined. Basement core samples from deep wells were investigated through petrological and geochronological analyses, and pre-existing geophysical and structural maps of those basins were taken again into consideration.It can be concluded that many of the identified basement discontinuities display a direct influence on the depositional history of the basins as well as on their internal subdivisions and external outlines. Basement structures generated during the late Precambrian Brasiliano Cycle turned out to be particularly important.The Paraná and Parnaíba basins are considered to represent cratonic basins, located on rigid lithosphere, tectonically stabilized in the latest Precambrian/early Palaeozoic, and their subsidence is attributed to the establishement of some initial rifted grabens. The Amazonas basin is more complex and includes three large sub-basins with distinct evolutions, each located on a different tectonic segment of the basement.  相似文献   
4.
Eight samples of the beryl variety aquamarine were selected from four pegmatites in the Governador Valadares and Araçuaí regions in northeastern Minas Gerais State, Brazil. These samples were fully characterized by chemical analysis, infrared and UV-visible spectroscopy, thermal analyses, and high-temperature X-ray diffraction (from room temperature up to 800 °C). Several physical and chemical properties of beryl were found to depend on the amount of water and ions residing in the structural channels. The thermal expansion coefficients from room temperature to about 800 °C are temperature-independent, with αa ? ?3.2 × 10?6 ° C?1 and αc ? ?8.7 × 10?6 ° C?1. The contraction of both a and c unit-cell parameters with increasing temperature and the shift of the infrared band centered at about 1200 cm?1 were tentatively ascribed to interactions between channel water and the silicate rings.The color of beryl seems to be dictated by the relative proportions of Fe3+ in the octahedralsites and of fe2+ in the channels. Thus, deep-blue samples have little Fe3+, whereas greener samples have more Fe3+ or less channel Fe2+.  相似文献   
5.
New K–Ar and 40Ar/39Ar data of tholeiitic and alkaline dike swarms from the onshore basement of the Santos Basin (SE Brazil) reveal Mesozoic and Tertiary magmatic pulses. The tholeiitic rocks (basalt, dolerite, and microgabbro) display high TiO2 contents (average 3.65 wt%) and comprise two magmatic groups. The NW-oriented samples of Group A have (La/Yb)N ratios between 15 and 32.3 and range in age from 192.9±2.2 to 160.9±1.9 Ma. The NNW-NNE Group B samples, with (La/Yb)N ratios between 7 and 16, range from 148.3±3 to 133.9±0.5 Ma. The alkaline rocks (syenite, trachyte, phonolite, alkaline basalts, and lamprophyre) display intermediate–K contents and comprise dikes, plugs, and stocks. Ages of approximately 82 Ma were obtained for the lamprophyre dikes, 70 Ma for the syenite plutons, and 64–59 Ma for felsic dikes. Because Jurassic–Early Cretaceous basic dikes have not been reported in SE Brazil, we might speculate that, during the emplacement of Group A dikes, extensional stresses were active in the region before the opening of the south Atlantic Ocean and coeval with the Karoo magmatism described in South Africa. Group B dikes yield ages compatible with those obtained for Serra Geral and Ponta Grossa magmatism in the Paraná Basin and are directly related to the breakup of western Gondwana. Alkaline magmatism is associated with several tectonic episodes that postdate the opening of the Atlantic Ocean and related to the upwelling of the Trindade plume and the generation of Tertiary basins southeast of Brazil. In the studied region, alkaline magmatism can be subdivided in two episodes: the first one represented by lamprophyre dykes of approximately 82 Ma and the second comprised of felsic alkaline stocks of approximately 70 Ma and associated dikes ranging from 64 to 59 Ma.

Resumo

Novos dados K–Ar e 40Ar/39Ar de enxames de diques toleíticos e alcalinos localizados no embasamento onshore da Bacia de Santos (SE Brasil) apontam para diferentes pulsos magmáticos ocorridos entre o Jurássico e o Terciário. Os diques de rochas toleíticas (basalto, diabásio e microgabro), são mais velhos, exibem altos teores de TiO2 (3,65% peso na média) e podem ser subdivididos em dois grupos magmáticos. O Grupo A aflora a norte da Bacia de Resende, compreende diques orientados na direção NW, com razões (La/Yb)N entre 15 e 32,3, e idades entre 192.9±2.2 e 160.9±1.9 Ma. O Grupo B aflora a sul e a leste da Bacia de Resende, engloba diques orientados na direção NNW e NNE, com razões (La/Yb)N entre 7 e 16, e idades obtidas entre 148.3±3 e 133.9±0.5 Ma. As rochas alcalinas (sienito, traquito, fonolito, basalto alcalino e lamprófiro) possuem teores médios de K, e afloram como diques, plugs e stocks.. As idades obtidas são de ca. 82 Ma para os diques lamprofíricos, de ca. 70 Ma para os plugs sieníticos, e entre 64 e 59 Ma para os diques félsicos. Como estas idades Jurássicas para diques toleíticos ainda não foram descritas para a região sudeste do Brasil, pode-se especular que durante o emplacement dos diques do GrupoA o cenário tectônico indicaria esforços extensionais anteriores à abertura do Oceano atlântico Sul, e contemporânea ao derrame basáltico do Karoo na África do Sul. Já os diques do Grupo B são contemporâneos ao magmatismo Serra Geral e ao enxame de diques de Ponta Grossa, e portanto este episódio está diretamente relacionado à separação entre o Brasil e África no Cretáceo. O magmatismo alcalino está associado a diversos episódios tectônicos que sucedem à abertura do Oceano Atlântico Sul e que resultaram no desenvolvimento das Bacias terciárias do sudeste brasileiro. Está provavelmente relacionado à chegada da Pluma de Trindade e as idades obtidas para a região em estudo indicam que o magmatismo lamprofírico é mais antigo (ca. 82 Ma), seguido pelos plútons sieníticos (ca. 70 Ma) e diques associados (64 a 59 Ma.)  相似文献   
6.
The Brazilian faxinal is a traditional agrosilvopastoral system, which combines extensive grazing, subsistence cropping and low impact forest extraction, managed within a communal property system. Today it is at serious risk of disappearing due to increasing grazing pressure and logging activities that are leading to environmental problems such as forest fragmentation and soil degradation. The objectives of the study were to: a) evaluate soil physical degradation levels in different grazing areas within the faxinal system; and b) correlate soil degradation, fodder quantity and livestock dynamics in different pasture areas according to the household's location. Landscape mapping, vegetation surveys, and livestock grazing dynamics were assessed. In addition, soil physical parameters were evaluated for each land use (e.g., resistance, bulk density, porosity, moisture, and water infiltration rates). Results showed that livestock grazing and household locations are the main driving forces that lead to forest fragmentation. The household location creates three interrelated gradients in the communal grazing land: 1) soil physical degradation decreases from the pasture areas to araucaria forests; 2) fodder quantity decreases from pastures to araucaria forests; and 3) the livestock grazing intensity decreases from pastures to araucaria forests. In addition, some management practices to mitigate land degradation, including improvement of pastures, installation of removable troughs for drinking water in the upland areas and restriction of livestock from the riparian zone, have been proposed.  相似文献   
7.
Biotic and abiotic factors are filters that prevent invasions in aquatic and terrestrial ecosystems. In this investigation we tested the hypothesis that the success of a non-native Poaceae (Urochloa subquadripara) is positively correlated with the richness of native macrophytes and negatively correlated with wind disturbance (fetch) and presence of riparian vegetation on coarse spatial scales. Our samplings were carried out in a tropical reservoir (Rosana Reservoir, Brazil). We first compared competing models using the Akaike criterion to find the main combinations of explanatory variables (native macrophyte richness, fetch, and presence of riparian vegetation) associated with the success of U. subquadripara. Then, we applied multiple regressions to assess the coefficient of determination of the best models selected according to the Akaike criterion. The probability of occurrence of U. subquadripara increased significantly with increases in the number of native macrophyte species, but decreased with fetch and the presence of riparian vegetation. Stand width and maximum depth of occurrence (indicators of the success of this Poaceae) were also positively related with native richness and negatively with fetch and riparian vegetation. Our results supported our expectation that wave disturbance is an important variable explaining U. subquadripara success. Because the less exposed sites are also more favorable for colonization by natives, positive relationships between the success of non-native species and native diversity emerge at the coarse scale. Taken together, our results support the theory of “biotic acceptance”; that is, favorable sites are more prone to colonization by both native and non-native species.  相似文献   
8.
Studies of soil erosion on small plots present upscaling problems. The results in the literature on the effect of slope length (i.e. scale) on runoff and soil erosion are contradictory. Furthermore, most studies that examine scale effects measured through erosion plots have been conducted in Mediterranean environments. The objective of this study was to assess the effects of plot size on runoff and soil loss in a subtropical environment. Other measurements were taken to appraise the topsoil property changes inside the plots. The soil was ploughed twice, the surface was leveled with a hoe and it was kept bare during the experiment. Data were collected from 10 paired plots, five plots measuring 10 m × 1 m and five plots measuring 1 m × 1 m, installed in the same pedo‐geomorphologic unit. Measurements were carried out from November 2008 to November 2009. During this period, 97 natural storms were registered. The results indicate that the small plots tended to have higher runoff (30% higher) compared to larger plots, especially during periods of greater rainfall volume, duration and intensity. The soil loss was similar in both the 1 m2 plots (6·33 kg/m2) and the 10 m2 plots (6·26 kg/m2). Moreover, the dynamics of the soil loss during the experiment was relatively similar across both plot sizes. The large plots tended to have a greater internal complexity. In these plots, the steps retreat were higher, the overland flow scars were more frequent, and points of rill initiation and protochannels emerged in several parts of the plots. The results of the small plots were comparable to the results obtained on the large plots, especially in relation to soil loss. These plots were useful for short‐term assessments of soil erosion. Copyright © 2011 John Wiley & Sons, Ltd.  相似文献   
9.
Samples of the eosphorite-childrenite [(Mn2+, Fe2+)AlPO4(OH)2H2O] series from Divino das Laranjeiras and Araçuaí (Minas Gerais State) and Parelhas (Rio Grande do Norte State) pegmatites have been investigated by X-ray diffraction, microprobe analysis and Mössbauer spectroscopy at 295 and 77 K. The Mössbauer spectra of ernstite [(Mn2+, Fe3+)AlPO4(OH)2-xOx] showed the existence of ferric ions in both A and B sites, whereas ferrous ions seem to be located exclusively in the A site. Nonoxidised samples show ferrous ions located in both sites, and no Fe3+ could be detected. The interpretation of the Mössbauer spectra of both, oxidised and nonoxidised samples, is difficult because the hyperfine parameters of these minerals are rather similar, rendering it difficult to make proper site assignments.  相似文献   
10.
Aquatic macrophytes produce large amounts of organic matter and have an essential structuring role in floodplains. This process highlights the importance of this community to aquatic biodiversity maintenance. We investigated the role of a flood disturbance on the response of macrophyte assemblages in regional and local structuring in the Upper Paraná River floodplain. Plant species were recorded before (November 2006) and after (March 2007) an uncommon increase in water level caused by the El Niño South Oscillation, which is considered a disturbance. Samples were taken in lakes and backwaters located in the floodplain and connected to three distinct rivers (that differentiate three sub-systems). Species richness and the assemblage structure of macrophyte patches underwent significant changes after the flood disturbance, depending on the specific sub-system (rivers) to which the lakes were connected. In addition, flood disturbance had a strong impact on community organization at the local scale. However, regionalization with respect to sub-systems remained significant after the flood disturbance. Our results emphasize the importance of connection to the river on macrophyte community composition and richness, and suggest that flood events in the Upper Paraná River floodplain disrupt community organization only at fine (local) scales.  相似文献   
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