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193nmLA-ICPMS对国际地质标准参考物质中42种主量和微量元素的分析 总被引：31，自引：16，他引：31
本文采用配备有 193nm Ar F准分子 (excimer)激光器的 Geo L as2 0 0 M剥蚀系统和 Elan6 10 0 DRC ICP- MS对 4个美国地质调查所 (USGS)玻璃标准参考物质以及 3个美国国家标准技术研究院 (NIST)人工合成硅酸盐玻璃标准参考物质中几乎覆盖整个质量数范围 (从 7L i到 2 38U)的 38个微量和 4个主量 (Na、Mg、Ti和 Mn)元素进行了分析。分析结果表明 ,无论是对 USGS还是 NIST玻璃 ,元素分析的相对标准偏差 RSDs和分析值与参考值之间的相对偏差 (RDs)一般优于 10 % ,RSD和RD较大的元素主要出现在含量很低或不均匀样品中。稀土元素的 RSD显示 ,除 AGV- 2 G可能存在不均匀现象外 ,其它所测样品在 6 0 μm尺度上 ,元素分布是均匀的。本研究证明 ,由于 ICP- MS具有 10 8cps(每秒计数 )的动态线性范围 ,本实验室的L A- ICPMS系统可定量分析含量在百分之几的主量元素及微量元素。分析精密度和准确度可与常规溶液雾化进样 ICP- MS方法相媲美 相似文献
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JAN-PIETER BUYLAERT GUNTHER GHYSELS REW S. MURRAY KRISTINA J. THOMSEN DIMITRI VANDENBERGHE FRANS DE CORTE IRENÉE HEYSE PETER VAN DEN HAUTE 《Boreas: An International Journal of Quaternary Research》2009,38(1):160-175
We report on quartz Optically Stimulated Luminescence (OSL) dating of the infill of 14 relict sand wedges and composite-wedge pseudomorphs at 5 different sites in Flanders, Belgium. A laboratory dose recovery test indicates that the single-aliquot regenerative-dose (SAR) procedure is suitable for our samples (measured to a given dose ratio 0.980 ± 0.005; n =139). Completeness of resetting of the wedge infill of two samples was confirmed by single-grain analyses. The suite of optical ages indicates that repeated thermal contraction cracking, degradation and infilling with wind-blown sediment appear to have been commonplace in Flanders during the Late Pleniglacial (Oxygen Isotope Stage 2; OIS2); more specifically, around the Last Glacial Maximum (LGM, ∼21 kyr ago) and the transition period between the LGM and the start of the Lateglacial (∼15 kyr ago). Optical dating at one site has revealed two significantly older wedge levels, the younger inset into the older; the younger wedge has an age of 36 ± 4 kyr (Middle Pleniglacial; OIS3), the older wedge 129 ± 11 kyr, which points to formation during the Late Saalian (OIS6). Our OSL ages of the wedges and host sediments bracket formation of the BGB (Beuningen Gravel Bed: a widespread deflation horizon in northwestern Europe) at between ∼15 and 18 kyr; this is in good agreement with previous OSL dating studies. We conclude that optical dating using quartz SAR OSL establishes an absolute chronology for these periglacial phenomena and allows secure palaeoenvironmental reconstructions to be made. 相似文献
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GUNTHER KLETETSCHKA Peter J. WASILEWSKI Patrick T. TAYLOR 《Meteoritics & planetary science》2000,35(5):895-899
Abstract— Recent discovery of intense magnetic anomalies on Mars, which are due to remanent magnetization, requires some explanation for the possible minerals responsible for the anomalous signature. Thermoremanent magnetization (TRM) in single domain (SD) and multidomain (MD) sized magnetite, hematite, and pyrrhotite, all potential minerals, are considered. The intensity of TRM (in 0.05 mT) is in descending order: SD‐sized magnetite, SD‐sized pyrrhotite, MD‐sized hematite, MD‐sized pyrrhotite, MD‐sized magnetite, SD‐sized hematite. The TRM intensity is <4% of the saturation isothermal remanence (SIRM) for all but the MD hematite, which may have >50% of the SIRM. Each of these minerals and estimated concentrations of magnetic remanence carriers (assumed to be titanomagnetite) in the Shergotty‐Nakhla‐Chassigny martian meteorites are used in a thin sheet approximation model to reveal the concentration of each mineral required for the generation of an observed magnetic anomaly (1500 nT at 100 km altitude) assuming TRM acquisition in a 0.05 mT magnetic field. 相似文献
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The Braccia gabbro complex (Eastern Central Alps, Northern Italy)intruded the boundary between the Adriatic lowermost continentalcrust and the subcontinental upper mantle in Permian times.The gabbro complex consists mainly of gabbro–norites withminor dykes of quartz diorite and Fe–Ti–P-rich diorite.The gabbro–norites contain abundant cumulus clino- andorthopyroxene and only small amounts of olivine, indicatingcrystallization at high pressure ( 相似文献
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