醋酸丁酯萃取-无火焰原子吸收法测定化探样品中痕量金   总被引：3，自引：0，他引：3  

刘菊琴  杨永理  韦山桃 《矿产与地质》2003,17(3):261-262,F003

在KBr存在下,用小体积醋酸丁酯萃取金后,用无火焰原子吸收法测定化探样品中痕量金的分析方法较化学富集光谱法具灵敏度高(检出下限可达0.05×10-9)、精度好、简便快速、成本低等优点.通过批量化探样的检验,证明该方法足已满足化探样品对金的测定要求.  相似文献   

Major goal achieved with major GAMs     

by Robert E. Mace  Cindy Ridgeway 《Ground water》2005,43(2):163-163

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Passive diffusion ground water samplers at a site with heterogeneous hydrostratigraphy: Pilot study results   总被引：1，自引：0，他引：1  

by Craig E. Divine  Laura L. Madsen  Scott D. Andrews  Theresa Santangelo-Dreiling 《Ground Water Monitoring & Remediation》2005,25(1):90-99

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氢化物发生-原子荧光光谱法则定锑精矿中的微量砷     

韦山桃  卢启余 《矿产与地质》2007,21(4):482-486

使用氢化物发生—原子荧光光谱法测定锑精矿中的微量砷在国内外报道较少。文章在锑干扰状况试验、高锰酸钾溶液消除干扰的最佳条件选择试验、锑精矿中共存元素的干扰和消除试验的基础上,对样品进行了实测,并就其灵敏度、准确度和精密度进行了讨论。研究表明,该方法是测定锑精矿中微量砷的有效方法。  相似文献   

Author''s Reply     

by M. Massabò  F. Catania  O. Paladino 《Ground water》2010,48(1):17-18

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METHODS   总被引：2，自引：0，他引：2  

Fig. Biandantang Lake  sampling sites are indicated by black circles 《中国海洋湖沼学报》2000,18(1):221-226

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Trespassing Across America: One Man's Epic,Never-Done Before (and Sort of Illegal) Hike Across the Heartland     

Reviewed by Joseph J. Kerski 《The Journal of geography》2017,116(4):185-186

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红黏土承载比的土团尺寸效应研究     

谈云志  郑爱  吴翩  付伟 《岩土力学》2013,34(5):1242-1246

高液限红黏土用于路基填筑时,因其不良的水理特性,需要掺石灰或水泥改良。但红黏土成团现象十分突出,进行灰土拌和时不易达到均匀状态,影响预期改良效果。通过对不同直径的红黏土土团及石灰改良土土团进行承载比试验,结果表明：干密度随着土团直径尺寸的增大呈现先增大后减小的特征,红黏土和石灰土的最大干密度对应的土团直径处在0.2～ 5 mm范围内;而最大承载比CBR值对应的土团直径分别处在5～10 mm和2～5 mm的范围内。石灰土和红黏土的吸水率、膨胀率均随着土团尺寸的增大,呈现先减小后增大的整体变化趋势。在2～10 mm的范围内,两种土的膨胀量最小。石灰改良只对直径小于5 mm的土团的膨胀特性起到明显的抑制作用。可见,现场施工中严格控制土团的大小对保证土体的强度和水稳定性具有十分重要的意义。  相似文献   

Calibration of Parameter Fields Consisting of Multiple Statistical Populations     

by Gijs M.C.M. Janssen  Johan R. Valstar 《Ground water》2010,48(1):92-105

If a parameter field to be calibrated consists of more than one statistical population, usually not only the parameter values are uncertain, but the spatial distributions of the populations are uncertain as well. In this study, we demonstrate the potential of the multimodal calibration method we proposed recently for the calibration of such fields, as applied to real-world ground water models with several additional stochastic parameter fields. Our method enables the calibration of the spatial distribution of the statistical populations, as well as their spatially correlated parameterization, while honoring the complete prior geostatistical definition of the multimodal parameter field. We illustrate the implications of the method in terms of the reliability of the posterior model by comparing its performance to that of a "conventional" calibration approach in which the positions of the statistical populations are not allowed to change. Information from synthetic calibration runs is used to show how ignoring the uncertainty involved in the positions of the statistical populations not only denies the modeler the opportunity to use the measurement information to improve these positions but also unduly influences the posterior intrapopulation distributions, causes unjustified adjustments to the cocalibrated parameter fields, and results in poorer observation reproduction. The proposed multimodal calibration allows a more complete treatment of the relevant uncertainties, which prevents the abovementioned adverse effects and renders a more trustworthy posterior model.  相似文献   

MTBE, TBA, and TAME Attenuation in Diverse Hyporheic Zones     

by James E. Landmeyer  Paul M. Bradley  Donald A. Trego  Kevin G. Hale  Joseph E. Haas II 《Ground water》2010,48(1):30-41

Groundwater contamination by fuel-related compounds such as the fuel oxygenates methyl tert -butyl ether (MTBE), tert -butyl alcohol (TBA), and tert -amyl methyl ether (TAME) presents a significant issue to managers and consumers of groundwater and surface water that receives groundwater discharge. Four sites were investigated on Long Island, New York, characterized by groundwater contaminated with gasoline and fuel oxygenates that ultimately discharge to fresh, brackish, or saline surface water. For each site, contaminated groundwater discharge zones were delineated using pore water geochemistry data from 15 feet (4.5 m) beneath the bottom of the surface water body in the hyporheic zone and seepage-meter tests were conducted to measure discharge rates. These data when combined indicate that MTBE, TBA, and TAME concentrations in groundwater discharge in a 5-foot (1.5-m) thick section of the hyporheic zone were attenuated between 34% and 95%, in contrast to immeasurable attenuation in the shallow aquifer during contaminant transport between 0.1 and 1.5 miles (0.1 to 2.4 km). The attenuation observed in the hyporheic zone occurred primarily by physical processes such as mixing of groundwater and surface water. Biodegradation also occurred as confirmed in laboratory microcosms by the mineralization of U- ¹⁴C-MTBE and U-¹⁴C-TBA to ¹⁴CO₂ and the novel biodegradation of U- ¹⁴C-TAME to ¹⁴CO₂ under oxic and anoxic conditions. The implication of fuel oxygenate attenuation observed in diverse hyporheic zones suggests an assessment of the hyporheic zone attenuation potential (HZAP) merits inclusion as part of site assessment strategies associated with monitored or engineered attenuation.  相似文献