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根据红土镍矿中镁橄榄石的存在形式,采用高温固相法合成Mg2SiO4,通过正交试验优化Mg2SiO4在高浓度氢氧化钠中的浸出过程,利用XRD对浸出反应渣进行物相分析,探讨了液固比、氢氧化钠浓度、反应时间和反应温度对Mg2SiO4中SiO2的浸出率的影响。结果表明:Mg2SiO4在高浓度氢氧化钠中浸出过程优化实验条件为,反应温度220℃,反应时间120min,液固比6∶1,NaOH浓度85%;浸出反应渣的XRD分析结果表明:NaOH介入硅酸盐晶格中,其中间产物为Na2MgSiO4,Mg2+经过碱熔融过程可以脱离SiO4阵列,以Mg(OH)2形式从其硅酸盐中得以释放。 相似文献
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吉林省晚印支期—燕山期成矿事件年谱的拟建及特征 总被引:4,自引:0,他引:4
吉林省铁、镍、钒、钛、钨、钼、金、银、铜、铅、锌、锑等内生金属矿产主要是晚印支—燕山期成矿事件的产物,已有测年数据拟建的成矿事件年谱所显示的结构特征表明:①、可划分出230~180 Ma、180~130 Ma、130~100 Ma三个时段和六个亚时区;②、180 Ma±、130 Ma±、100 Ma±的三大成矿峰期,均处于早期盆地闭合,新期盆地打开的转换期;③、三大成矿峰期由老而新主矿种由钼—金(银)—铜的演化。上述特征受该地质时期区域构造-岩浆作用和岩石圈的演化所制约。 相似文献
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延吉盆地老头沟、三峰洞、帽儿山等地发育有多个呈孤峰状产出的安山岩地质体,长期以来被作为次火山岩体描述.作者在朝阳川镇德新村东发现其不整合覆盖于龙井组之上,确定其为一套喷出相火山岩,新建德新组,根据龙井组及区域上珲春组时代限定,推断其时代为晚白垩世. 相似文献
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Naphthenic acids in petroleum are considered a class of biological markers. Their potential use in source correlation and as an indicator of biodegradation was reported in the past ( Dzidic et al. ,1988 ; Behar and Albrecht, 1984). Due to their highly complicated properties, detailed characterization of the acids is difficult. A method based on positive ion CI (chemical ionization) mass spectrometry using isobutane reagent gas to produce ( M 15)^ ions was applied to the analysis of naphthenic acid esters. Since the complex mixture of naphthenic acids cannot be separated into individual components, only the determination of relative distribution of acids classified in terms of hydrogen deficiency was possible. The identities and relative distribution of fatty and mono-, di-, tri-, and higher polycyclic acids were obtained from the intensities of the ( M 15 )^ ions according to z-series formula CπH2π 2 O2 of naphthenic acids. The components are characterized on the basis of group type and carbon number distributions. A comparison of the FAB and CI results showed that the group type distributions obtained bv both methods agree surprisingly well.The results indicated this method is simple, rapid and easy to operate. The geochemical implication of naphthenic acids was investigated by using a set of well-characterized crude oil samples. It is found that the naphthenic acid distribution can be used as a fingerprint for oil-oil and oil-source correlations. 相似文献