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Min Wang Wei Wang Benlin He Mingliang Sun Yansheng Yin Lan Liu Wuyuan Zou Xuefei Xu 《中国海洋大学学报(英文版)》2010,9(4):376-380
TiO2 films were formed on metallic titanium substrates by the anodic oxidation method in H2SO4 solution under the 80V D.C.. Phase component and microstructure were characterized by X-ray diffraction (XRD) and scanning
electron microscopy (SEM). Water contact angles on titanium oxide film surface were measured under both dark and sunlight
illumination conditions. Corrosion tests were carried out in seawater under different illumination conditions by electrochemistry
impedance spectrum (EIS) and polarization curves. The result showed that the TiO2 film prepared by the anodic oxidation method was anatase with a uniform structure and without obvious pores or cracks on
its surface. The average water contact angle of the film was 116.4° in dark, in contrast to an angle of 42.7° under the UV
illumination for 2 hours, which demonstrates good hydrophobic property. The anti-corrosion behavior of the TiO2 film was declining with the extended immersion time. Under dark conditions, however, the hydrophobic TiO2 film retarded the water infiltrating into the substrate. The impedance changed slowly and the corrosion current density was
2 orders of magnitude lower than that with the film illuminated by sunlight. All of those mentioned above indicate that the
TiO2 film possesses much better performance under dark condition, and it can be applied as an engineering material under dark
seawater environment. 相似文献
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利用黄梅台长期稳定、连续、可靠、精确的观测资料,应用EIS2000[1]地震前兆信息处理与软件系统及MapInfo软件系统,通过对比分析气象变化、人为干扰、仪器故障等非地形变信息和误差干扰因素,多方法分析、处理了台站水管仪、伸缩仪两套仪器定点形变观测资料.从资料分析结果中掌握某些基本常见的规律,为台站人员在日常资料处理... 相似文献
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铜合金在海水中电化学阻抗谱特征研究 总被引:5,自引:0,他引:5
利用电化学阻抗谱(EIS)对紫铜和铜镍合金在静止、洁净海水中表面成膜的过程进行了监测,根据不同阶段的EIS特征建立不同等效电路模型进行拟合分析。获得了铜合金基体及其表面膜层对应的界面电化学信息参数,通过比较3种金属(B10,TUP,B30)表面膜层随时间变化的差异。探讨了合金成分对表面成膜过程的影响。结果表明。浸泡前期B10和TUP的耐蚀性较差,但随着海水中浸泡时间增加,三者的耐蚀能力逐渐接近。TUP的EIS显示了其表面内、外膜层信息。B10表面膜层的成长速度和稳定性均不如B30,反映出合金中镍含量的增多,增加了铜镍合金表面成膜产生钝化的效应。 相似文献
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以本校环境科学专业《环境信息系统》课程实验课为例,探讨了实验课的设计与实践结果。以学习Access与北京超图公司研发的Supermap GIS为主,实验课分为数据库的基本操作、SuperMap GIS软件的基础操作和空间查询、空间分析等3个部分,要求学生掌握一定的理论知识后,按照各实验要求进行上机验证。近10 a实践证明,该实验设计能达到预期效果,但仍需在实际教学中不断完善。 相似文献
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以MgCl2溶液模拟氯氧镁水泥孔隙液,研究了A3钢在MgCl2溶液中的腐蚀行为和腐蚀速率,并利用电化学测试仪对A3钢腐蚀过程的电化学特征进行了研究。实验结果表明,随着MgCl2浓度的减小以及在MgCl2溶液中浸泡时间的延长,A3钢的腐蚀失重速率逐渐变小;极化曲线测试与腐蚀失重试验结果相吻合;阻抗曲线(EIS)研究发现,随着A3钢在MgCl2溶液中浸泡时间的延长钝化膜的电阻变大;扫描电镜观察表明,经MgCl2溶液腐蚀后,在A3钢样品表面产生了许多腐蚀产物,XRD分析证实主要产物为Fe3O4和MgFe2O4。 相似文献
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