排序方式： 共有37条查询结果，搜索用时 454 毫秒
1.
2.
乙酰褐藻酸丙二酯的制备与表征 总被引：1，自引：0，他引：1
为了改变褐藻酸丙二酯的溶解性,本文以氢碘酸为催化剂,将褐藻酸丙二酯与乙酐反应,制备了乙酰褐藻酸丙二酯。生成物不溶于水,可溶于多种中等极性的有机溶剂。本文用IR,~1H-NMR,HGPC对其进行了表征,并对反应条件对产率的影响进行了探讨。 相似文献
3.
黑鲷(Acanthopagrus schlegeli)肿瘤坏死因子α cDNA的克隆及特征分析 总被引：1，自引：0，他引：1
采用同源克隆的方法，从黑鲷中获得肿瘤坏死因子(TNFα)全长cDNA序列。该序列含1288个核苷酸，可编码253个氨基酸的TNF前体蛋白。它是一种跨膜蛋白，无糖基化位点和信号肽结构。黑鲷TNFα与其它鱼类的TNFα的相似性很高，占据进化上独立的分支；与哺乳类TNFα和TNFG源于共同的祖先。基因结构分析显示，该基因含有TNF家族pmfile和TNF家族的标签序列；在参与TNFα基因二硫键形成的两个半胱氨酸和TNFα三聚体形成的位点高度保守；空间结构模拟显示，它与哺乳类TNFα的空间结构相似，都是由两个β折叠片组成，每个折叠片包含5个反向平行的β链。表达研究结果表明，黑鲷TNFα在检测的各个组织中均为组成型表达，表现为在刺激与非刺激鱼体中，都可以检测到黑鲷TNFα的表达，但是其表达水平在不同组织中有很大差异。黑鲷TNFα在头肾、脾脏和鳃的表达量较高，而在心脏、肝脏、血液、肾脏和大脑中表达量较低。 相似文献
4.
5.
In this study a field‐sampling technique for dissolved hydrogen (H2) in groundwater will be presented which allows the transport of gaseous samples into the laboratory for further analysis. The method consists of transferring the headspace trapped in a gas‐sampling bulb which is continuously purged by groundwater into previously evacuated vials using a gas‐tight syringe. Three transfer steps with preceding evacuation of the vial led to a H2‐recovery of 100 % in laboratory experiments. The method has been applied to determine H2 concentrations in an aquifer contaminated with chlorinated solvents. Tests concerning the effect of different pumping techniques on H2 concentrations revealed that most reliable values were obtained with a bladder pump, while an electrically driven submersible pump generated considerable amounts of hydrogen due to electrochemical interactions with the sampled water. Concentrations of dissolved hydrogen in field and laboratory samples were about two orders of magnitude higher when sampling was performed with the electrically driven submersible pump compared to sampling with the bladder pump and a peristaltic pump. Lab experiments with a Plexiglas reservoir to produce H2‐enriched water were used to study the effect of two tubing materials (PVC, polyamide) on H2 losses. PVC tubing turned out to allow transfer of H2‐enriched water over 25 m without significant losses, while PA‐tubing was not suitable for sampling of H2. 相似文献
6.
以反应谱和功率谱密度函数表征的强震运动的统计特性 总被引：1，自引：0，他引：1
文中利用我国海城和唐山地震１９０条强震记录和美国西部１３８条强震记录研究了以反应谱和功率谱密度函数表征的强震运动的统计特性。反应谱用最大地面加速度归一化，即表为谱放大系数，功率谱密度函数用金井清谱描述。文中研究了参数的统计值和依赖性，以及谱放大系数和金井清谱参数与场地条件、震源和震中距等之间的相关性，分析比较了中美两国强震运动谱的统计特性，并对我国地震工程应用的强震运动谱的统计参数值的选取提出了建议。 相似文献
7.
The gel-permeation chromatography system with multicomponent detection of organic carbon, organic nitrogen, organic halogen, and UV/vis absorption measurement is shown to be a useful tool for characterization of industrial wastewaters and wastewater treatment processes. The proposed system was used to investigate biologically treated wastewater from chemical industry, whereby one branch stream was identified to be the main source of persistent halogenated organics. Various treatment processes of pulp mill wastewater were also evaluated revealing that precipitation with aluminium is very effective for the removal of the high molecular fraction whereas the biological treatment is generally less selective. In the biological treatment of tannery wastewaters, it has been shown that the aerobic treatment, in contrast to anaerobic step, causes evident alterations of the composition of the polar DOC fraction. The nitrogen containing compounds are also better decomposed in the aerobic step compared to the anaerobic one. 相似文献
8.
以无水乙醇为溶剂、1-丁基-3-甲基咪唑四氟硼酸盐([Bmim]BF4)离子液体为表面活性剂,以钛酸四丁酯、六水合硝酸镧为原料,采用共沉淀法制备了不同掺镧量的La-TiO2光催化材料。采用X-射线衍射仪(XRD)、傅里叶变换红外光谱仪(FTIR)、场发射扫描电镜(FESEM)、差热-热重分析仪(TG-DSC)、紫外-可见吸收光谱仪(UV-vis)、比表面及孔隙度分析仪(BET)对其结构、形貌、热稳定性、光学性能及比表面积进行表征。所制备产品的光催化性能在紫外光下进行了光催化降解甲基橙实验,实验结果表明在离子液体的量为0.5mL,掺杂镧量为5%的TiO2纳米材料对甲基橙的降解效果相对较好,降解率最高达到98.73%。 相似文献
9.
Nowadays,the preservation of natural resources,the reuse,and the recycling of waste and by-products in the cement industry are gaining increasing attention in a sustainable development project.In this perspective,many studies focus on finding solutions in order to propose environmentally friendly materials.Nowadays the sediments represent a way to preserve the natural resources by their reuse as a secondary raw material in multiple applications(concrete,roads,landscaped mound,etc.).However,they commonly contain contaminants,organic matter(5%-30%),high water content(50%-200%),and relatively small particle size(Dmax≤300 mm).Therefore to improve the mechanical properties of this material as well as its physiochemical ones,specific methods of characterization and appropriate treatment techniques(calcination,chemical treatment,etc.)are required.This article presents a bibliographical review of the efficient use of sediments in cementitious matrix.It details experimental tests that must be performed to ensure the durability of sediment-based structure and assess their environmental impact under prescribed conditions. 相似文献
10.