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The study of the chemical stability of vitreous material in aqueous media is well‐established. There has to date been little consideration of the implications of variations in the chemical durability of tephra in Quaternary tephrochronology. Chemical alteration can take the form of cationic leaching from the matrix, or complete destruction of the silica network, either of which could constrain the ability to chemically identify distal tephra. Here we apply established models of vitreous durability to the published chemical analyses of a large number of Icelandic tephras in order to predict their relative durabilities under equivalent conditions. This suggests that some important tephras have relatively poor chemical stability, and that rhyolitic tephras are, in general, more stable than basaltic. We conclude that tephras should be expected to show predictable differential chemical stability in the post‐depositional environment. Copyright © 2003 John Wiley & Sons, Ltd. 相似文献
3.
电感耦合等离子体发射光谱法同时测定玻璃中铝钙铁钾镁钠钛硫 总被引:2,自引:2,他引:0
通过选择分析谱线、处理样品方法和消除干扰因素等实验,建立了电感耦合等离子体发射光谱法同时测定玻璃中的Al2O3、CaO、Fe2O3、K2O、MgO、Na2O、TiO2和SO3的方法,克服了利用常规化学法测定玻璃中各氧化物步骤繁琐、耗时长、工作量大的不足。方法的回收率为95.0%~103.0%,精密度(RSD,n=10)为0.20%~1.72%。方法具有快速、简便、线性范围宽等优点,分析误差满足常规化学分析法的要求。用于钠钙硅玻璃及其制品的分析,结果令人满意。 相似文献
4.
Pressures of Crystallization of Icelandic Magmas 总被引:1,自引:0,他引:1
Iceland lies astride the Mid-Atlantic Ridge and was createdby seafloor spreading that began about 55 Ma. The crust is anomalouslythick (20–40 km), indicating higher melt productivityin the underlying mantle compared with normal ridge segmentsas a result of the presence of a mantle plume or upwelling centeredbeneath the northwestern edge of the Vatnajökull ice sheet.Seismic and volcanic activity is concentrated in 50 km wideneovolcanic or rift zones, which mark the subaerial Mid-AtlanticRidge, and in three flank zones. Geodetic and geophysical studiesprovide evidence for magma chambers located over a range ofdepths (1·5–21 km) in the crust, with shallow magmachambers beneath some volcanic centers (Katla, Grimsvötn,Eyjafjallajökull), and both shallow and deep chambers beneathothers (e.g. Krafla and Askja). We have compiled analyses ofbasalt glass with geochemical characteristics indicating crystallizationof ol–plag–cpx from 28 volcanic centers in the Western,Northern and Eastern rift zones as well as from the SouthernFlank Zone. Pressures of crystallization were calculated forthese glasses, and confirm that Icelandic magmas crystallizeover a wide range of pressures (0·001 to 1 GPa), equivalentto depths of 0–35 km. This range partly reflects crystallizationof melts en route to the surface, probably in dikes and conduits,after they leave intracrustal chambers. We find no evidencefor a shallow chamber beneath Katla, which probably indicatesthat the shallow chamber identified in other studies containssilica-rich magma rather than basalt. There is reasonably goodcorrelation between the depths of deep chambers (> 17 km)and geophysical estimates of Moho depth, indicating that magmaponds at the crust–mantle boundary. Shallow chambers (<7·1 km) are located in the upper crust, and probablyform at a level of neutral buoyancy. There are also discretechambers at intermediate depths (11 km beneath the rift zones),and there is strong evidence for cooling and crystallizing magmabodies or pockets throughout the middle and lower crust thatmight resemble a crystal mush. The results suggest that themiddle and lower crust is relatively hot and porous. It is suggestedthat crustal accretion occurs over a range of depths similarto those in recent models for accretionary processes at mid-oceanridges. The presence of multiple stacked chambers and hot, porouscrust suggests that magma evolution is complex and involvespolybaric crystallization, magma mixing, and assimilation. KEY WORDS: Iceland rift zones; cotectic crystallization; pressure; depth; magma chamber; volcanic glass 相似文献
5.
火山玻璃风化层的透射电镜研究 总被引:2,自引:0,他引:2
利用透射电镜(TEM)和X射线能谱(EDX)研究了长白山天池火山1000年和4000年前两次大喷发产生的火山玻璃风化层特征.TEM分析显示,4000年前大喷发浮岩中的火山玻璃风化层平均厚度3.7 mm,1000年前大喷发浮岩中的火山玻璃风化层平均厚度为1.0 mm.EDX分析显示,两次大喷发浮岩中的火山玻璃风化层化学组成与火山玻璃相比富Al、Fe,而si减少.火山玻璃风化层富Al发生在Al的浓度较高的中到弱酸溶液中(pH=5~6),火山玻璃表面形成含有少量的非晶质的Al、Si、Fe物质,这些非品质的次生物质是火山玻璃风化早期阶段形成的.天池火山喷发物中火山玻璃的微观特征的差异可能与火山喷发年代和喷发后的环境有关,研究天池火山不同期次喷发物中火山玻璃的微观特征具有一定的理论和实际应用价值. 相似文献
6.
Martin Rosner Michael Wiedenbeck Thomas Ludwig 《Geostandards and Geoanalytical Research》2008,32(1):27-38
An analytical artefact is reported here related to differences in instrumental mass fractionation between NIST SRM glasses and natural geological glasses during SIMS boron isotope determinations. The data presented demonstrated an average 3.4‰ difference between the NIST glasses and natural basaltic to rhyolitic glasses mainly in terms of their sputtering-induced fractionation of boron isotopes. As no matrix effect was found among basaltic to rhyolitic glasses, instrumental mass fractionation of most natural glass samples can be corrected by using appropriate glass reference materials. In order to confirm the existence of the compositionally induced variations in boron SIMS instrumental mass bias, the observed offset in SIMS instrumental mass bias has been independently reproduced in two laboratories and the phenomenon has been found to be stable over a period of more than one year. This study highlights the need for a close match between the chemical composition of the reference material and the samples being investigated. 相似文献
7.
Masanori Kurosawa Simon E. Jackson Shigeho Sueno 《Geostandards and Geoanalytical Research》2002,26(1):75-84
Fifty elements in NIST SRM 614 and 616 glass reference materials were determined by laser ablation microprobe-inductively coupled plasma-mass spectrometry (LAM-ICP-MS). The values determined for NIST SRM 614 agreed well with the NIST-certified and information values (mean relative difference ± 3.6%), except for B, Sc and Sb. The values determined for NIST SRM 616 agreed with the NIST-certified and information values within a mean relative difference of ± 1.5%, except for B, Sc and Ga. In addition, at an 80 μm sampling scale, NIST SRM 614 and 616 glass discs were homogeneous for trace elements within the observed precisions of 5 and 15% (mean), respectively. Detection limits were in the range 0.01 - 0.3 μg g−1 for elements of lower mass numbers (amu < 80) and 1 - 10 ng g−1 for heavy elements (amu > 80). Detection at the sub ng g−1 level is possible for most of the heavy elements by using an ablation pit size larger than 10 0 μm. 相似文献
8.
Philip J. Potts Michael Thompson Stephen Wilson 《Geostandards and Geoanalytical Research》2002,26(2):197-235
Results are presented for round one of a new international proficiency testing programme designed for microprobe laboratories involved in the routine analysis of silicate minerals. The sample used for this round was TB-1, a basaltic glass fused and prepared by the USGS. Thirty nine laboratories contributed data to this round, the majority of major element results being undertaken by EPMA and the majority of trace elements by LA-ICP-MS. Assigned values were derived from the median of results produced by nine selected laboratories that analysed powdered material by conventional ICP-MS, INAA and XRF techniques using bulk powders of the sample. Submitted microprobe results were evaluated using a target precision calculated using the Horwitz function, adopting the same criteria as those used for "applied" geochemistry laboratories in the companion GeoPT proficiency testing programme for laboratories involved in the routine bulk analysis of silicate rocks. An evaluation of results from participating microprobe laboratories indicated that overall, data were compatible with this precision function. A comparison between the performance of bulk and microprobe techniques used in the analysis of the basaltic glass showed remarkably good agreement, with significant bias only observed for the major oxide MgO. 相似文献
9.
Yugo Nakamura Yoshinori Katayama Kazuomi Hirakawa 《Journal of Volcanology and Geothermal Research》2002,114(3-4)
Refractive indices of incompletely hydrated tephra glasses vary widely. Thus, glass refractive index is not a practical indicator for identifying Holocene tephras. Hydration near the surface of tephra glass shards can be removed by either hydrofluoric acid treatment or annealing for 12 h at 400°C. The annealing procedure is a particularly reliable and simple way to dehydrate tephra glasses. Standard deviations (s) of refractive indices for glasses after 12 h annealing are small (s=0.0014–0.0018), in contrast with untreated glasses (s=0.0034–0.0405). The refractive indices of dehydrated tephra glasses are 0.006–0.014 lower than those of the untreated (hydrated) glasses. Using the 400°C 12-h annealing procedure, values for the refractive indices of eight Holocene tephras in Hokkaido were obtained. These refractive indices are useful indicators for identification and correlation of Holocene tephras. 相似文献
10.