| 乌江流域水库沉积物中生物硅的测定方法及其环境意义 |
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| 引用本文： | 雷云逸,汪福顺,陆丹萍,梅航远.乌江流域水库沉积物中生物硅的测定方法及其环境意义[J].矿物学报,2011,31(1):30-35. |
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| 作者姓名： | 雷云逸 汪福顺 陆丹萍 梅航远 |
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| 作者单位： | 1. 上海大学理学院化学系,上海,200444
2. 上海大学环境与化学工程学院射线应用研究所,上海,200444 |
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| 基金项目： | 国家自然科学基金，上海市青年科技启明星计划，环境地球化学国家重点实验室开放课题 |
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| 摘 要： | 采用碱提取法中的单点法与多点法相结合,测定了乌江流域水库沉积物中生物硅的含量,并对多点提取法进行了改良。采用多个离心管分装定量样品进行连续振荡,每小时提取1个样品进行测定。对多个时间点的提取结果,利用线性回归法分析得出最佳提取时间,优化最佳提取液,然后利用单点提取-硅钼蓝检测法测定沉积物中生物硅的含量。该方法既保证了单点法的快速,也减小了多点法的多次提取操作与提取时的体积误差。本文根据测定结果探讨了乌江流域水库沉积物中生物硅含量变化规律及其环境意义。
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| 关 键 词： | 沉积物生物硅 乌江流域 水库 |
Determination of Biogenic Silica in Sediments of Reservoirs in the Wujiang River and its Environment Significance |
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| LEI Yun-yi,WANG Fu-shun,LU Dan-ping,MEI Hang-yuan.Determination of Biogenic Silica in Sediments of Reservoirs in the Wujiang River and its Environment Significance[J].Acta Mineralogica Sinica,2011,31(1):30-35. |
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| Authors: | LEI Yun-yi WANG Fu-shun LU Dan-ping MEI Hang-yuan |
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| Institution: | LEI Yun-yi1,WANG Fu-shun2,LU Dan-ping1,MEI Hang-yuan2,YIN Ran2(1.Department of Chemistry,Shanghai University,Shanghai 200444,China,2.College of Environment and Chemical Engineering,China) |
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| Abstract: | In this study,biogenic Silica in sediments of reservoirs in the Wujiang Drainage Basin was determined,by means of the wet-alkaline extraction procedure with the combination of single-point and multi-point extraction methods.The multi-point extraction procedure was improved in this study.A batch of sediment samples were put into centrifuge tubes,and continuously vibrated in a constant temperature bath oscillator.Contents of biogenic silica(BSi) of the extracted samples were measured every hour through wet-al... |
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| Keywords: | sediment biogenic silica the Wujiang Drainage Basin reservoir |
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