| 高氯酸-盐酸体系-火焰原子吸收光谱法测定铅精粉中的银 |
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| 引用本文： | 张旺强,王春妍,陈月源,巨力佩,李瑞仙.高氯酸-盐酸体系-火焰原子吸收光谱法测定铅精粉中的银[J].岩矿测试,2010,29(6):707-710. |
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| 作者姓名： | 张旺强 王春妍 陈月源 巨力佩 李瑞仙 |
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| 作者单位： | 国土资源部兰州矿产资源监督检测中心, 甘肃 兰州 730050;兰州兰石机械制造有限公司, 甘肃 兰州 730050;国土资源部兰州矿产资源监督检测中心, 甘肃 兰州 730050;国土资源部兰州矿产资源监督检测中心, 甘肃 兰州 730050;国土资源部兰州矿产资源监督检测中心, 甘肃 兰州 730050 |
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| 摘 要： | 采用X射线衍射技术(XRD)对水镁石原矿和不同工艺条件生产的出口镁砂产品进行了物相组成分析,水镁石原矿粉中主相Mg(OH)2含量达到85.9%,杂质主要是Mg3Si2(OH)4O5、CaCO3和CaMg(CO3)2;轻烧镁砂中的Mg(OH)2大部分已经分解为MgO,但还有12.3%的Mg(OH)2未分解,并在低温煅烧的情况下生成了微量的新相Mg2SiO4;重烧镁砂中的Mg(OH)2已经完全分解为MgO,杂质主要存在形式是Mg2SiO4和CaCO3,占总量的18.5%。实验结果将成为提高水镁石矿煅烧生产的镁砂品质而改进提纯工艺的参考依据。
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| 关 键 词： | 煅烧水镁石 镁砂 X射线衍射 物相分析 |
| 收稿时间： | 2010/3/29 0:00:00 |
| 修稿时间： | 2010/7/22 0:00:00 |
Determination of Silver in Lead Concentrate Powder Samples by Flame Atomic Absorption Spectrometry in HClO4-HCl System |
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| ZHANG Wang-qiang,WANG Chun-yan,CHEN Yue-yuan,JU Li-pei and LI Rui-xian.Determination of Silver in Lead Concentrate Powder Samples by Flame Atomic Absorption Spectrometry in HClO4-HCl System[J].Rock and Mineral Analysis,2010,29(6):707-710. |
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| Authors: | ZHANG Wang-qiang WANG Chun-yan CHEN Yue-yuan JU Li-pei and LI Rui-xian |
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| Institution: | Lanzhou Testing and Quality Supervision Center for Geological and Mineral Products, The Ministry of Land and Resources, Lanzhou 730050, China;LanZhou Petroleum Machine Maufacturing Company LTD, Lanzhou 730050, China;Lanzhou Testing and Quality Supervision Center for Geological and Mineral Products, The Ministry of Land and Resources, Lanzhou 730050, China;Lanzhou Testing and Quality Supervision Center for Geological and Mineral Products, The Ministry of Land and Resources, Lanzhou 730050, China;Lanzhou Testing and Quality Supervision Center for Geological and Mineral Products, The Ministry of Land and Resources, Lanzhou 730050, China |
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| Abstract: | The X-ray diffraction(XRD) has been used to analyze phase composition of magnesite clinker from calcinated brucite with different process conditions.The major phase of raw brucite powder is Mg(OH)2 with content up to 85.9% and major impurities are Mg3Si2(OH)4O5,CaCO3 and CaMg(CO3)2.Most of Mg(OH)2 are decomposed into MgO under light calcined condition(700~1000℃) during the calcination at low temperature and about 12.3% of un-decomposed Mg(OH)2 forms new phase of Mg2SiO4.Mg(OH)2 in brucite is completely decomposed into MgO under dead-burned condition(1400~1800℃) and the impurities are Mg2SiO4 and CaCO3 with total content of 18.5%.The results provide the guidance for reforming purification process and improving the quality of magnesite clinker. |
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| Keywords: | HClO4-HCl flame atomic absorption spectrometry lead concentrate powder silver |
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