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Determination of Bromine and Iodine in U.S.G.S. Standard Marine Mud (MAG-1)
Authors:WJ ULLMAN  GT TISUE
Institution:Ecological Sciences Section, Division of Radiological and Environmental Research, Argonne National Laboratory, Argonne, Illinois, USA;Department of the Geophysical Sciences, University of Chicago, Chicago, Illinois, USA;Center for Great Lakes Studies, University of Wisconsin, Milwaukee, Wisconsin, USA
Abstract:The concentrations of bromine and iodine in USGS reference material MAG-1 were determined by standard addition with secondary-source x-ray fluorescence spectrometric detection. Three determinations of bromine in the same sample yielded 311, 309 and 346 μg Br/g solid. The iodine content was found to be 380 μg I/g solid. The determination of bromine in a second bottle of MAG-1 (266 ± 9 μg Br/g) indicated that a large variation in halogen concentration may exist between samples of this reference material.
Keywords:
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