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火焰原子吸收法测定化探样品中的银铜铅锌
引用本文:潘自平.火焰原子吸收法测定化探样品中的银铜铅锌[J].贵州地质,2003,20(3):192-194.
作者姓名:潘自平
作者单位:贵州省地质矿产中心实验室,贵州,贵阳,550004
摘    要:样品经硝酸、氢氟酸、高氯酸分解,制成硝酸溶液,经巯基棉层析柱过滤富集Ag,并用2mol/LHBr溶液洗脱,用火焰原子吸收法测定洗脱液中的Ag和滤液中的Cu,Pb,Zn。用该法测定化探样品中银和铜铅锌,检出限低,结果准确度和精密度均令人满意。

关 键 词:巯基棉富集  化探样品  原子吸收法          光谱法
文章编号:1000-5943(2003)03-0192-03
修稿时间:2003年2月20日

Flame-AAS Determination of Ag and Cu,Pb,Zn in the Samples of Geochemical Prospecting by Mercapto Cotton in Enriching Ag
PAN Zi - ping.Flame-AAS Determination of Ag and Cu,Pb,Zn in the Samples of Geochemical Prospecting by Mercapto Cotton in Enriching Ag[J].Guizhou Geology,2003,20(3):192-194.
Authors:PAN Zi - ping
Abstract:The sample through the dissolution in NHO3 acid, HF acid and HC1O4 is made into the nitric solution. By making use of the mercapto cotton to filter out the Ag of enrichment and then fulfilling washing desulfuration in 2mol/ L hydro - bromine, flame atomic absorption method is put to determine Ag in washing desulfuration resolution and Cu, Pb, Zn in filtrate. This method in mensurating Ag and Cu, Pb, Zn is of low detection limit and accurate results.
Keywords:mercapto cotton enrichment  samples of geochemical prospecting  atomic absorption
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