| 灰尘中主次量元素的X射线荧光光谱分析 |
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| 引用本文： | 王志刚,李凤全,潘虹梅.灰尘中主次量元素的X射线荧光光谱分析[J].岩矿测试,2008,27(5):383-385. |
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| 作者姓名： | 王志刚 李凤全 潘虹梅 |
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| 作者单位： | 浙江师范大学地理系地理过程实验室,浙江,金华,321004 |
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| 摘 要： | 采用粉末压片-X射线荧光光谱法对灰尘样品中P、Ti、V、Ni、Cu、Zn、Ga、Rb、Sr、Nb、Cs、Ba、La、Hf、Zr、Pb、Al2O3、CaO、Fe2O3、K2O、MgO、Na2O、SiO2等主次量组分进行测定。探讨了谱线校正,使用经验系数法和康普顿散射线作内标校正基体效应。用国家一级标准物质进行验证,测定值与标准值相符。
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| 关 键 词： | 粉末压片 X射线荧光光谱法 主次量元素测定 灰尘 |
| 收稿时间： | 2007/12/11 0:00:00 |
| 修稿时间： | 2008/2/26 0:00:00 |
X-ray Fluorescence Spectrometric Determination of Major and Minor Elements in Dust Samples |
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| WANG Zhi-gang,LI Feng-quan and PAN Hong-mei.X-ray Fluorescence Spectrometric Determination of Major and Minor Elements in Dust Samples[J].Rock and Mineral Analysis,2008,27(5):383-385. |
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| Authors: | WANG Zhi-gang LI Feng-quan and PAN Hong-mei |
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| Institution: | Department of Geography, Zhejiang Normal University;Department of Geography, Zhejiang Normal University;Department of Geography, Zhejiang Normal University |
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| Abstract: | X-ray fluorescence spectrometric method with powdered pellet sample preparation for the determination of P, Ti, V, Ni, Cu, Zn, Ga, Rb, Sr, Nb, Cs, Ba, La, Hf, Zr, Pb, Al2O3, CaO, Fe2O3, K2O, MgO, Na2O, SiO2 in dust samples was developed. Compton scattering line was selected as internal standard and the empirical coefficient method was used for the matrix effect correction. The method has been applied to the determination of these elements in National Standard Reference Materials and the results are in agreement with certified values. |
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| Keywords: | powder pellet X-ray fluorescence spectrometry determination of major and minor elements dust |
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