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电感藕合等离子体原子发射光谱法快速测定地质样品中的钒
引用本文:赵平,李天祥,吴靖,杨刚.电感藕合等离子体原子发射光谱法快速测定地质样品中的钒[J].贵州地质,2007,24(1):74-77.
作者姓名:赵平  李天祥  吴靖  杨刚
作者单位:1. 中国地质大学材化学院,湖北,武汉,430074;国土资源部贵阳矿产资源监督检测中心,贵州,贵阳,550004
2. 贵州大学化工学院,贵州,贵阳,550003
3. 国土资源部贵阳矿产资源监督检测中心,贵州,贵阳,550004
摘    要:炭质页岩中钼、镍、钒、磷等元素的含量相对较高;作者采用充氩电荷注入检测器(CID)-电感藕合等离子体全谱直读原子发射光谱仪,建立了适应于地质样品中钒的快速测定的方法。方法的特点是:线性范围宽、快速、准确、稳定性好且能同时测试多种元素;该方法也可同时用于:Mn、Cu、Pb、Zn、Co、N i、P等杂质元素的快速测定。通过对实际样品的检测,取得良好结果,与化学法测定结果基本吻合。

关 键 词:电感藕合等离子体全谱直读原子发射光谱  地质样品  
文章编号:1000-5943(2007)01-0074-04
修稿时间:2007-01-24

Determination of Vanadium in Geological Samples by Inductively Coupled Plasma Emission Spectrometer
ZHAO Ping,LI Tian-xiang,WU Jing,YANG Gang.Determination of Vanadium in Geological Samples by Inductively Coupled Plasma Emission Spectrometer[J].Guizhou Geology,2007,24(1):74-77.
Authors:ZHAO Ping  LI Tian-xiang  WU Jing  YANG Gang
Institution:1 Faculty of Material Science and Chemical Engineering, China University of Geosciences, Wuhan 430074 China ; 2 MLR Guiyang Supervision and Testing Center of Mineral Resources, Guiyang 550004, China; 3 School of Chemical and Engineering, Guizhou University, Guiyang 55003, China
Abstract:The traditional methods for analyzing vanadium in ores are weight method,capacities method,polarogram method and atom absorb spectral luminosity method,but the determining contents spans of those methods are small,the operation is miscellaneous and trivial.In this paper,charge injection pouring device(CID) Inductively Coupled Plasma-Optical Emission Spectrometry with directly reading display is applying to rapidly accurate measure the element content in vanadium ore.This method's characteristics are that the linearity range is broad,the measurement is quickly and accurate,the stability is easy to be obtained and the various elements can be measured at the same time.This method is able to measure Mn,Cu,Pb,Zn,Co,Ni and P quickly.The experimental results show excellent equivalence with chemical method's results for all elements.
Keywords:Inductively Coupled Plasma-Optical Emission Spectrometry  geological samples  vanadium
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