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石墨炉原子吸收法测定地质样品中的微量银
引用本文:姜云,王卿.石墨炉原子吸收法测定地质样品中的微量银[J].山东地质,2008(7):98-100.
作者姓名:姜云  王卿
作者单位:山东省地质科学实验研究院,山东济南250013
摘    要:研究了石墨炉原子吸收法测定地质样品中微量Ag的方法,探索了以NH4IrCl6做基体改进剂的最佳仪器工作条件。在取样0.2000g,定容25mL的情况下,方法检出限为0.010ug/g,用国家标准物质验证,其准确度(RE%)小于10%,10次测定的精密度(RSD%)小于10%。

关 键 词:石墨炉原子吸收法  检测方法  微量银  地质样品

How to Determine Micro- silver in Geological Samples by Using Graphite Fire Atomic Absorption Spectrum Method
JIANG Yun,WANG Qing.How to Determine Micro- silver in Geological Samples by Using Graphite Fire Atomic Absorption Spectrum Method[J].Geology of Shandong,2008(7):98-100.
Authors:JIANG Yun  WANG Qing
Institution:(Shandong Institute and Laboratory of Geological Sciences, Shandong Jinan 250013, China)
Abstract:Micro - silver in geological samples are determined by using the method of graphite fire atomic absorption spectrum. It realized the best equipment conditions by using NH 4 IrCl 6 as the matrix modifier. Under the condition of sampling 0.2000g and constant volume of 25 mL, the method detection limit is 0.010ug/g. As tested by national standards, its accuracy ( RE% ) is less than 10%, and the precision ( RSD% ) in 10 times determination are less than 10%.
Keywords:Graphite fire atomic absorption spectrum  silver  geological samples
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