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电感耦合等离子体质谱法分析汤岗子热矿泥白粉中的矿物元素
引用本文:侯冬岩,回瑞华,许利民,刘俊会.电感耦合等离子体质谱法分析汤岗子热矿泥白粉中的矿物元素[J].岩矿测试,2010,29(1):47-50.
作者姓名:侯冬岩  回瑞华  许利民  刘俊会
作者单位:1. 鞍山师范学院化学系,辽宁,鞍山,114007
2. 鞍山市科技局,辽宁,鞍山,114044
3. 国家农业深加工产品质量监督检验中心,吉林,长春,130002
基金项目:鞍山市重大科技项目资助 
摘    要:对汤岗子热矿泥白粉中矿物元素进行分析研究。采用微波消解法处理样品,运用电感耦合等离子体质谱法对汤岗子热矿泥白粉中钠、镁、钾、钙、铁、锌、锰、铜、硒、锗、钼、铬、铝、镍、砷、汞、铅等17个矿物元素进行分析。结果表明,在优化实验条件下,方法检出限为0.000279 9~14.66μg/L,相对标准偏差(RSD,n=6)为0.18%~6.20%,回收率为91.1%~108.2%。汤岗子热矿泥白粉中含有丰富的矿物元素。

关 键 词:电感耦合等离子体质谱法  矿物元素  汤岗子热矿泥白粉
收稿时间:2009/4/19 0:00:00
修稿时间:2009/9/10 0:00:00

Determination of Mineral Elements in Thermal Mineral Mud from Tanggangzi Hotspring by Inductively Coupled Plasma-Mass Spectrometry
HOU Dong yan,HUI Rui hu,XU Li min and LIU Jun hui.Determination of Mineral Elements in Thermal Mineral Mud from Tanggangzi Hotspring by Inductively Coupled Plasma-Mass Spectrometry[J].Rock and Mineral Analysis,2010,29(1):47-50.
Authors:HOU Dong yan  HUI Rui hu  XU Li min and LIU Jun hui
Institution:Department of Chemistry, Anshan Normal University;Department of Chemistry, Anshan Normal University;Science and Technology Office of Anshan;China Quality Supervision Testing Center for Agricultural Deep Processing Products
Abstract:The mineral elements in the thermal mineral mud samples from Tanggangzi hotspring were analyzed. The thermal mineral mud samples were decomposed by microwave digestion and the elements of Na, Mg, K, Ca, Fe, Zn, Mn, Cu, Se, Ge, Mo, Cr, Al, Ni, As, Hg and Pb in the samples were analyzed by inductively coupled plasma-mass spectrometry (ICP-MS). The results showed that under optimum conditions, the detection limits of the method for these elements were in the range of 0.0002799~14.66 μg/L. The recovery of the method for these elements was 91.1%~108.2% with precision of 0.18%~6.20%RSD (n=6). The results also indicated that the thermal mineral mud from Tanggangzi hotspring contained abundant of mineral elements.
Keywords:inductively coupled plasma-mass spectrometry  mineral element  thermal mineral mud of Tanggangzi
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