Investigating the potential of HCl-only treated samples using range-finder OSL dating |
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| Institution: | 1. Research Laboratory for Archaeology and the History of Art, University of Oxford, Dyson Perrins Building, South Parks Road, Oxford OX1 3QY, UK;2. Department of Classics, Cornell University, 120 Goldwin Smith Hall, Ithaca 14853-3201, NY, USA;3. Department of Classical, Near Eastern, and Religious Studies, University of British Columbia, Buchanan C227, 1866 Main Mall, Vancouver V6T 1Z1, BC, Canada |
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| Abstract: | Rapid sample preparation and measurement protocols for optically stimulated luminescence (OSL) dating have been investigated as a method of increasing the throughput of samples (e.g. Roberts et al. 2009). Here, we investigate the potential of dating samples treated using only hydrochloric acid (HCl) for providing accurate range-finder ages for quartz. The equivalent dose (De) is underestimated for older samples using a standard single-aliquot regenerative-dose (SAR) protocol, but measurement of the post-IR OSL signal (e.g. Roberts and Wintle, 2003) provides De estimates within 15% of the ‘target fully prepared De’ for two-thirds of samples. The application of a standardised growth curve (SGC) is also investigated. For these dune samples, the most efficient preparation and measurement procedure from which accurate De estimates can be obtained is treatment with HCl-only, measurement of the natural and regenerative post-IR OSL signal, and calculation using a region-independent SGC. A slightly longer protocol incorporating an additional preparation stage of heavy liquid density separation can be used to improve De estimates in samples where feldspar-contamination is thought to be particularly problematic. In practice, these time savings of days to weeks in the preparation and measurement protocols mean that a large number of samples can first be rapidly treated with HCl, the post-IR blue OSL signal measured using a shortened double-SAR protocol, and De calculated by applying an independent SGC before then deciding which samples require full preparation and measurement, rather than the inefficiency of committing time and resources to all samples if this is unnecessary for the context of a particular suite of samples. The potential of this rapid preparation and measurement protocol is discussed in relation to sand dune dating studies. |
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| Keywords: | Optically stimulated luminescence Range-finder OSL dating Quartz Rapid sample preparation Standardised growth curve |
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