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40Ar/39Ar step heating of thermally overprinted biotite,hornblende and potassium feldspar from Eldora,Colorado
Authors:Glenn W Berger
Institution:Geophysics Division, Department of Physics, University of Toronto, Toronto, Ont. Canada
Abstract:40Ar/39Ar incremental heating experiments were applied to hornblendes, coarse-grained biotites and K-feldspars from 1400 m.y. old rocks near the contact with the ~60 m.y. old Eldora stock in the Front Range of Colorado. The aim was to distinguish, on the basis of argon isotopic data alone, a partially re-set K-Ar date from an undisturbed or a completely overprinted K-Ar date. In the laboratory heating of biotites the radiogenic argon (40Ar*) and potassium-derived39Ar (39Ar*) were released in two stages — in the range ~600–900°C and above ~900°C. The two biotites furthest from the contact and the one adjacent to the contact give well-defined apparent-age plateaus at ~1230 m.y. and 63 m.y. respectively for all argon released above ~600°C. The 1230-m.y. date may represent a thermal event or the end of a long cooling while the 63-m.y. date essentially represents the time of reheating. Partially overprinted biotites at intermediate distances have significantly anomalous plunges in apparent ages for argon released above ~900°C, thus distinguishing them from undisturbed and completely outgassed biotites.The bulk of the40Ar* and39Ar* in the hornblendes was released in the range ~950–1100°C. The hornblende furthest from the contact gives a well-defined plateau at 1400 m.y. for the 98% of the argon that was released above ~950°C. A partially overprinted hornblende from near the contact gives an apparent plateau at ~1050 m.y. The existence of such a false plateau precludes the distinction of partially overprinted K-Ar hornblende dates from undisturbed K-Ar hornblende dates without independent evidence. Reasonable estimates of the time of reheating are not recovered in the age spectra for partially overprinted hornblende and biotites.For the feldspars the bulk of the40Ar* and39Ar* was released in the laboratory heating between about 900°C and 1200°C, probably reflecting phase changes near these temperatures. The argon released below about 900°C records reasonable maximum dates for the time of the thermal overprinting. For the microcline 22500 (the sample number specifies the distance, in feet, from the contact) this effect is slight — a minimum date of 147 m.y. occurs in 2.3% of the total39Ar*. For samples 2400, 1070, and 85 the respective minimum dates are similar at 72, 81, and 68 m.y. and dramatically improve on the total or integrated dates of 238, 358 and 211 m.y. The high-temperature (>900°C) apparent ages for these three feldspars do not define plateaus and are geologically meaningless. The high-temperature apparent ages for the last 50% of the39Ar* released from 22500 do define a plateau, but the 1060-m.y. date is also probably geologically meaningless.
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