| 空气滤膜采集大气浮尘样品中多元素的测定 |
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| 引用本文： | 陈波,冯永明,刘洪青.空气滤膜采集大气浮尘样品中多元素的测定[J].岩矿测试,2009,28(5):435-438. |
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| 作者姓名： | 陈波 冯永明 刘洪青 |
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| 作者单位： | 安徽省地质实验研究所,安徽合肥,230001 |
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| 摘 要： | 用氢氟酸-盐酸-硝酸-高氯酸体系对空气滤膜上附着的浮尘样品进行分解,电感耦合等离子体发射光谱法、电感耦合等离子体质谱法同时测定溶液中15个主量和微量元素铁、铜、锌、镍、镧、铈、锂、锰、铬、镉、钴、铅、钍、铊、铀。将国家一级标准物质模拟浮尘样品加入空白滤膜进行测定,结果与标准值相符。各元素4次测定结果的相对标准偏差(RSD)小于5%。
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| 关 键 词： | 空气滤膜 电感耦合等离子体发射光谱法 电感耦合等离子体质谱法 酸溶 主量和微量元素 国家标准物质 大气浮尘 |
| 收稿时间： | 2008/11/1 0:00:00 |
| 修稿时间： | 2008/12/29 0:00:00 |
Determination of Multi-elements in Airborne Dust with Air Filtrer Membrance Sampling |
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| CHEN Bo,FENG Yong ming and LIU Hong qing.Determination of Multi-elements in Airborne Dust with Air Filtrer Membrance Sampling[J].Rock and Mineral Analysis,2009,28(5):435-438. |
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| Authors: | CHEN Bo FENG Yong ming and LIU Hong qing |
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| Institution: | Anhui Research Institute of Geological Experiment;Anhui Research Institute of Geological Experiment;Anhui Research Institute of Geological Experiment |
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| Abstract: | Airborne dust sample was collected with air filtrer membrance and then dissolved with mixed acid of HF-HCl-HNO3-HClO4.15 elements including Fe,Cu,Zn,Ni,La,Ce,Li,Mn,Cr,Cd,Co,Pb,Th,Tl,and U in the sample solution were determined by inductively coupled plasma-atomic emission spectrometry(ICP-AES) and inductively coupled plasma-mass spectrometry(ICP-MS).The National Standard Reference Materials,simulated as airborne dust,were collected with air filtrer membrance and analyzed by ICP-AES and ICP-MS.The results were in agreement with the certified values with precision of less than 5%RSD(n=4) for all these elements. |
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| Keywords: | air filter membrance inductively coupled plasma-atomic emission spectrometry inductively coupled plasma-mass spectrometry acid digestion major and trace elements National Standard Reference Materials airborne dust |
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