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聚氯酯泡沫塑料富集——ICP-MS测定化探样中微量金的方法
引用本文:李锟.聚氯酯泡沫塑料富集——ICP-MS测定化探样中微量金的方法[J].化工矿产地质,2007,29(4):242-244.
作者姓名:李锟
作者单位:中化地质矿山总局中心实验室,河北涿州072754
摘    要:试样经王水分解,在10%的王水溶液介质中,加一定量的铁盐,用聚氨酯泡沫塑料吸附富集金,1%硫脲溶液解脱,ICP—MS进行测定。实验结果表明,这种方法精密度高、准确度好,检出限低。其测定范围为0.028—500ng/g。

关 键 词:王水分解  泡塑富集  硫脲解脱  ICP-MS测定
文章编号:1006-5296(2007)04-0242-03
收稿时间:2007-07-12
修稿时间:2007年7月12日

ENRICHMENT OF POLYAMINOESTER FOAMED PLASTICS --MEASURE TO DETERMINE THE TRACE AU BY ICP-MS
Li kun.ENRICHMENT OF POLYAMINOESTER FOAMED PLASTICS --MEASURE TO DETERMINE THE TRACE AU BY ICP-MS[J].Geology of Chemical Minerals,2007,29(4):242-244.
Authors:Li kun
Abstract:The samples are decomposed by aqua regia, that is, adding some molysite in 10% aqua regia solution, the Au in the samples will be absorbed by the polyaminoester foamed plastics. Then it is disembarrssed by 1% thiourea solution and determined by ICP-MS. It has been found that the determination has higher precision, better accuracy and lower detection limit, the measurement range 0.028 - 500ng/g.
Keywords:decomposed by aqua regia  Enrichment of the foamed plastics  disembarrassed by thiourea  determined by ICP-MS
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