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On the limits of using combined U-series/ESR method to date fossil teeth from two Early Pleistocene archaeological sites of the Orce area (Guadix-Baza basin,Spain)
Authors:Mathieu Duval  Christophe Falguères  Jean-Jacques Bahain  Rainer Grün  Qingfeng Shao  Maxime Aubert  Jean-Michel Dolo  Jordi Agustí  Bienvenido Martínez-Navarro  Paul Palmqvist  Isidro Toro-Moyano
Institution:1. Centro nacional de investigación sobre la evolución humana (CENIEH), Paseo de Atapuerca s/n, 09002-Burgos, Spain;2. Muséum National d''Histoire Naturelle, Département de Préhistoire, UMR 7194, 1 rue R. Panhard 75013 Paris, France;3. Research School of Earth Science, The Australian National University, Canberra, ACT0200, Australia;4. CEA, I2BM, F-91401, Orsay, France;5. ICREA, Institut Català de Paleoecologia Humana i Evolució Social (IPHES), Universitat Rovira i Virgili (URV), Campus Catalunya, Avinguda de Catalunya, 35, 43002 Tarragona, Spain;6. Departamento de Ecología y Geología, Universidad de Málaga, Campus de Teatinos, 29071 Málaga, Spain;7. Museo Arqueológico de Granada, Carrera del Darro 41-43, 18010 Granada, Spain
Abstract:The combined U-series/electron spin resonance (ESR) dating method was applied to nine teeth from two Early Pleistocene archaeological sites located in the Orce area (Guadix-Baza Basin, Southern Spain): Fuente Nueva-3 (FN-3) and Barranco León (BL). The combination of biostratigraphy and magnetostratigraphy places both sites between the Olduvai and Jaramillo subchrons (1.78–1.07 Ma).Our results highlight the difficulty of dating such old sites and point out the limits of the combined U-series/ESR dating method based on the US model. We identified several sources of uncertainties that may lead to inaccurate age estimates. Seven samples could not be dated because the dental tissues had (230Th/234U) activity ratios higher than equilibrium, indicating that uranium had probably leached from these tissues. It was however possible to calculate numerical estimates for two of the teeth, both from FN-3. One yielded a Middle Pleistocene age that seems to be strongly underestimated; the other provided an age of 1.19 ± 0.21 Ma, in agreement with data obtained from independent methods. The latter result gives encouragement that there are samples that can be used for routine dating of old sites.
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