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1.
A brief review is presented of my efforts to improve the accuracy of dating unheated sediments by TL and of the development of a new tephrochronometer. Specific applications to known-age deposits are outlined, as are studies of the depositional environment of subaqueous sediments. Removal of anomalous fading in loess by storage at 75°C for 8 days is demostrated.Throughout, for unheated sediments the preferential use of the partial bleach (R-gamma or R-beta) technique is emphasized, especially in situations where the growth curves are sublinear. Contrary to a widespread misconception, sublinearity does not invalidate the partial bleach method. Furthermore, examples are given of TL ‘sensitivity’ (or ‘efficiency’) changes occurring with the regeneration technique — changes that are variable and seemingly sample dependent.  相似文献   

2.
A review of current research on TL dating of loess   总被引：1，自引：0，他引：1  
The thick loess deposits of China, Central Europe and North America are particularly suitable for the application of the thermoluminescence (TL) dating method because individual grains are likely to have travelled large distances and thus been well exposed to light before deposition. Wind-blown silt grains collected close to glacial rivers in Alaska have been shown to give a ‘zero age’ of not more than 2 ka, demonstrating the efficiency of the zeroing mechanism.Differences in laboratory procedures can cause differences in the TL ages reported, particularly for loess over 100 ka. TL ages for interstadial soils in Europe are in agreement with the very few radiocarbon dates on reliable material, such as charcoal. On the other hand TL dates from sites in Belgium and north-western Germany indicate that the previously accepted chronology, which was based on two radiocarbon dates on humic-rich sediments, is incorrect.The use of the ‘last interglacial’ palaeosol for assessing the TL dates on loess above and below it is limited by the uncertainty in the timing of termination of soil-forming processes; 107 and 71 ka are the limits suggested by the astronomically-derived time scale. Results on deposits from China, North America, Alaska and Europe are discussed in this context.  相似文献   

3.
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4.
电子自旋共振(ESR)技术是一种确定物质成分和结构的顺磁性质的分析方法,也能够用于沉积物定年。该方法的测量技术和测年的物理机制等还处于发展阶段。冰川作用过程十分复杂,形成各种类型的冰川沉积物,其顺磁信号的归零机制有显著差异,ESR测年的实验方案也有所差异。因此,识别冰碛物类型,采集合适的样品对于ESR测年的准确性十分重要。冰下融出碛和滞碛经过了冰下磨蚀过程,结构致密,细颗粒基质含量高,石英砂中的一些杂质芯的ESR信号能够衰退。许多冰上融出碛,结构疏松,但细颗粒基质含量高,不但经过了搬运过程中的冰下磨蚀过程使ESR信号衰退,又经历了沉积时的冰上阳光直射过程使信号衰退,一些样品的ESR信号能够完全晒退。冰水湖泊和冰水河流沉积的细砂和粉砂来源于冰下研磨的产物,信号会衰退;在搬运沉积过程中又可能被阳光直射,信号进一步衰退。其它类型的冰碛物的ESR信号衰退机制不明,或粒径不适合用ESR方法测年。采集冰碛物ESR年代样品时,最好同时采集信号衰退机制相同的现代冰碛物样品,以便对照,并用于扣除可能的残留信号。  相似文献   

5.
At Pedregal, more than 40 m of sediments are exposed within a ‘fan complex’ formed between lateral moraines of the adjacent Mucuchache and El Caballo valleys. Early and late Mérida (Wisconsinan) glaciations are represented by till and till plus proglacial sediments, respectively. A middle Wisconsinan interstadial event, here termed the Pedregal interstade, began at the end of the Early Mérida glaciation at approximately 60 ka BP. Following the retreat of ice from the small Pedregal Basin, a lake formed when the local drainage was blocked due to movement of the Mesa de Caballo along the Boconó Fault. Shallow lake or no-lake phases lasted approximately a few hundred to, at most, 2000 years, and each lake phase was marked by peat accumulation. Four of seven peats identified formed during sufficiently long intervals for soil profiles (incipient to mature Spodosols) also to develop. The Spodosol with the strongest development (Eb/Bsb/Coxb/Cub horizons) is found adjacent to the lowest peat and reflects ongoing early Mérida stadial (MIS 3) conditions; the youngest peats, associated with weak podzolic soils (Eb/Bsb horizons), formed under slightly warmer interstadial conditions, presumably with less soil water. Cyclic lacustrine deposition is related to lake level and relative depth fluctuations, due in part to variable shoreline/delta progradation and shallowing as the lake deepened in general. Whereas final drainage of the lake is related to movement of the Boconó Fault and breach of the moraines that form the Mesa de Caballo, earlier lake level fluctuations appear related to climate change. Radiocarbon dating of the peats suggests they are related to warmer periods and may tentatively correlate with small ‘interstadials’ or ‘D-O events’ detected in the oxygen-isotope record of Greenland ice cores and North Atlantic marine sediments.  相似文献   

6.
Theoretical considerations imply that the suitability of glacially-deposited sediments for thermoluminescence (TL) dating will be influenced by transport routes within the ice, and by facies of deposition. Measurments on sediments obtained from the Austerdalsbreen glacier in western Norway indicate that zeroing of sediment does not occur at the base of a valley glacier, but that englacial and supraglacial sediments showed evidence of bleaching but not total zeroing. Analysis of sediments from recent glacial and fluvioglacial landforms showed no evidence that they had been zeroed prior to deposition. Results indicate that the TL-age of glacial landforms will be a function of the derivation and travel paths of the sediments of which it is composed rather than of the form itself. It is concluded that as knowledge of the rates of bleaching associated with various facies of transport and deposition of glacial sediments improves, so the potential of the technique to act as a diagnostic sedimentological tool will increase, even when dating of glacial deposits by TL is impossible.  相似文献   

7.
Although the term ‘geochemical baseline’ appears in the international geochemical mapping programmes IGCP 259 and 360, it has never been well defined. Several considerations relevant to such a definition are discussed. A geochemical baseline for an element refers to its natural variations in concentration in the surficial environment. Geochemical baselines were studied in Finland by comparing results from regional geochemical mapping programmes based on samples of till, clay and organic stream sediment. The geochemical background changes regionally with the basic geology and locally with the type and genesis of the overburden. Baseline concentrations depend on sample material collected, grain size and extraction method. In Finland, concentrations of potentially harmful elements tend to be higher in fine-grained marine and lacustrine sediments than in glacial till. Concentrations are also systematically higher in the < 0.06 mm fraction than in the < 2 mm size fraction of till samples. Only small proportions of the total heavy metal concentrations in Finnish marine clays are bioavailable. Geochemical baselines are needed for environmental legislation and political decision-making, especially in the assessment of contaminated soil. In many areas of Finland, natural concentrations of several heavy metals exceed the guide or limit values designated for contaminated soils. Thus baselines must always be verified in any assessment of sites for contamination.  相似文献   

8.
Thermoluminescence (TL) dating of shallow marine sediments from the well studied interglacial-carly glacial sequence at Fjtfsangcr, western Norway has yielded ages that with few exceptions become progressively older with depth. For Ecmian samples the TL method yielded a mean of 111,000 ± 23,000 years, close to the often postulated age of 125,000 years. For the Early Weichselian the TL dates were younger than suggested by the amino-acid method.  相似文献   

9.
A combination of ‘bomb spike’ calibration and conventional calibration of AMS 14C dating has been used to determine a detailed age-depth model for a 1-m sediment section collected from a salt marsh in Poole Harbour, southern England. These data were compared with the chronology obtained from 210Pb analysis and 137Cs age markers. We report post bomb values of over 1.46 F14C (> 146% modern 14C), and both the rising and falling limbs of the atmospheric ‘bomb spike’ are identified. Five pre-bomb samples were analysed using multi-target high-precision 2‰ AMS analysis, and after the replicates were combined the one-sigma uncertainty was as low as ± 9 14C yr on some ages. These data, and an additional three normal-precision pre-bomb 14C samples, were calibrated using CALIB 5.0 and the chronology constrained using the ‘prior knowledge’ of independent age markers obtained from the analysis of pollen and spheroidal carbonaceous particle (SCPs). No agreement was found between the 14C ‘bomb spike’ dates and the CRS 210Pb chronology modelled for this sequence. In addition, poor agreement was found between the signal of the 1960s weapons test fallout indicated by the 14C ‘bomb spike’ dates and the timing suggested by the 137Cs data. This disagreement is attributed to the influence of the local discharge of 137Cs from the former UKAEA site at Winfrith. We use our new chronology to confirm the existence of an acceleration in sedimentation rates in Poole Harbour during the last 100 yr previously reported for this site by Long et al. (Long, A.J., Scaife, R.G., Edwards, R.J. 1999. Pine Pollen in intertidal sediments from Poole Harbour, UK; implications for late-Holocene sediment accretion rates and sea-level rise. Quaternary International, 55, 3–16.), and conclude that ‘bomb spike’ 14C calibration dating may offer a more robust alternative to the use of 210Pb chronologies for dating sediment deposition in salt-marsh environments. In addition, we demonstrate how the use of high-precision AMS analysis has the potential for reducing some of the uncertainties involved in the high-resolution dating of recent salt-marsh sediments.  相似文献   

10.
Molluscan fossils collected from shallow water marine sediment across NW Europe and nearby Arctic regions have been analysed for the extent of isoleucine epimerization ( ratio) in indigenous protein residues. The ratios confirm that essentially all ‘classical’ Eemian sites from NW Europe are of the same age, and are correlative with the type locality near Amersfoort in the Netherlands; shells from interglacial marine sediment beneath the type Weichselian till in Poland also correlate with the type Eemian site. ratios in Holsteinian marine shells (0.29) are substantially higher than in their Eemian counterparts (0.17); ‘Late Cromerian’ shells yield even higher ratios (0.46). ratios in late glacial shells (0.06) and Middle Weichselian shells (0.09) permit differentiation from modern (0.01) and last interglacial material. Based on the position of the Matuyama-Brunhes boundary and the differences in ratios, the Eemian must correlate with isotope substage 5e, whereas the Holsteinian is most likely substage 7c, possibly stage 9 but certainly younger than stage 11. Intra-Saalian warm periods may be terrestrial equivalents of the younger substages of stage 7. Extensive pre-Eemian marine sediments along the SW coast of Denmark previously correlated with the Holsteinian are shown to be of ‘Late Cromerian’ age. The underlying till there is the first widespread evidence of a pre-Elsterian till in NW Europe. ratios in molluscs from last interglacial sites along the Arctic coast of the USSR, the Arctic Islands and eastern Greenland are substantially lower than in their European counterparts due to their low thermal histories. The combined mid- and high-latitude data are used to develop a predictive model for the expected ratio in any of several moderate epimerization-rate taxa for last interglacial sites with mean temperatures between −20 and +15°C.Not all sites could be unambiguously assigned to an established interglacial. The Fjøsanger (Norway) and Margareteberg (Sweden) sites previously thought to be Eemian, yield ratios higher than in secure nearby Eemian material. It is yet unresolved whether these are aberrant sites or if they predate the last interglacial. In situ shoreline deposits encountered in borings in SW Belgium and in exposures on the Belgium coastal plain contain molluscs that yield ratios intermediate between secure Eemian and Late Weichselian ratios, raising the possibility that a late stage 5 high-sea-level event attained near-modern levels in the southern North Sea basin. Resolution of these uncertainties is the focus of future work.  相似文献   

11.
第四纪沉积物光释光测年中等效剂量测定方法的对比研究   总被引：12，自引：0，他引：12  
陈杰  魏兰英 《地球化学》1999,28(5):443-452
准确地测定碎屑矿物沉积后吸收的等效剂量第四纪沉积物释光测年中最关键的一环。用光释光测年技术对几年全新世坡积物,古土地和黄土等样品中的石英,长石等碎屑矿物进行了测定等效剂量的对比研究。  相似文献   

12.
天山乌鲁木齐河源末次冰期冰川沉积光释光测年   总被引：6，自引：5，他引：1  
乌鲁木齐河源地区是中国冰川遗迹保存最丰富、地貌最典型的区域之一,是根据冰川遗迹重建第四纪冰川历史的理想地区。大量的研究工作以及技术测年结果也使其成为试验冰川沉积光释光（optically stimulated luminescence,OSL）测年可行性的理想地点。共采集了6个冰碛及上覆黄土样品用于光释光测年。提取38~63 μm的石英颗粒,运用SAR-SGC法测试等效剂量。各种检验表明测试程序是适用的。通过地貌地层关系、重复样品、已有年代的对比等方法,检验该地冰川沉积OSL测年的可行性。结果表明,OSL年代结果与地貌地层新老关系非常吻合,与已有的其他测年技术的年代结果也具可比性,表明这些样品的OSL信号在沉积之前晒退较好,OSL年代是可信的。冰川观测站侧碛垄的OSL年代为14.8±1.2 ka;9号冰川支谷口附近冰碛的OSL年代为13.5±1.1 ka和17.2±1.3 ka;上望峰冰碛的OSL年代为20.1±1.6 ka。综合OSL年代结果与此前其他测年结果,这几套冰碛垄形成于深海氧同位素MIS 2阶段应该是比较统一的认识。上望峰冰碛上覆黄土的OSL年代（10.5±0.8 ka）也印证了该结论。OSL年代指示上望峰冰碛对应于末次冰期最盛期,冰川观测站和9号冰川支谷谷口冰碛对应于晚冰期。下望峰冰碛的OSL年代为36.3±2.8 ka,对应于MIS 3阶段。下望峰冰碛的形成时代,仍有待更多沉积学以及测年工作进一步确定。  相似文献   

13.
The uranium/thorium (U/Th) dating method was applied to pedogenic/diagenic ferricretes developed within glacial drifts from the northern West Coast Ranges of Tasmania. The dates derived from the method are, by definition, minima for the sediments, with the ferricretes being secondary mineral deposits which appear in the form of bands, horizons or nodules comprised of indurated masses of iron oxy(hydr)oxides developed post-depositionally within the host sediment or soil. The absence of such deposits in well-identified drift sediments of the last glaciation suggests the development of ferricrete horizons in glacial drifts occurred during earlier interstadials and interglacials. This has been confirmed by the uranium/thorium dating of ferricrete bands within glacigenic sediments obtained from three drill cores from the Boco Valley. The ages derived were found to be consistent with estimates for the timing of glaciation derived from palaeomagnetic analyses, radiocarbon dating and relative dating techniques. The results show that the uranium/thorium method can be used to successfully date ferricretes obtained from within glacial sediments of ages <350000 yr and provides valuable information regarding the minimum age of the host sediment. © 1997 John Wiley & Sons, Ltd.  相似文献   

14.
Auto-regenerative dating of zircon grains from fired materials has been shown to be a very powerful technique. The high internal dose rate in zircon gives a measurable auto-regenerated TL signal a few months after the natural TL measurement, allowing the determination of age without dosimetry. The technique has been extended to zircon grains from sediments, using optically stimulated luminescence (OSL) techniques to measure the natural signal. The auto-regenerated signal is only a few hundred photons and cannot be measured above background using present OSL techniques, so it is counted using the highly sensitive TL reader developed for fired zircon grains. Preliminary measurements on fired zircons are in good accord with TL dating and the known ages, but precision becomes poor for samples <1 ka in age. Possible improvements using auto-regenerative phototransfer TL dating are discussed.  相似文献   

15.
释光测年是可对冰川地貌进行直接定年的一种测年技术,已被广泛应用于冰川沉积测年中,推动了第四纪冰川研究的深入发展。但冰川沉积释光测年还没有达到标准化的程度,实际应用中仍有不少问题需要探究,其中最受关注的是冰川沉积物释光信号晒退不完全的问题,即样品在埋藏前因曝光机会有限导致信号没有归零或仅部分归零。冰川沉积释光信号晒退程度与地貌部位和沉积环境密切相关。冰川沉积释光采样需注意几个方面：（1）详细的地貌学和沉积学调查及对采样点的选择;（2）较适合释光测年的冰水沉积和冰缘风成沉积采集及其与冰川作用期次的联系;（3）冰碛夹层中的冰水砂透镜体的选取;（4）冰碛垄采样时垂直与水平方向上的考量;（5）岩石释光测年的发展使砾石成为当前第四纪冰川释光测年采样的一种选择。室内进行释光等效剂量测试时,也有几个关键的选择：（1）粗颗粒石英光释光测年是末次冰期以来冰川作用的首选方法;（2）如果样品年代老于石英测年上限,或者石英不适合测试,则可考虑钾长石后红外高温释光测年方法;（3）单颗粒、小测片和岩石释光埋藏测年技术可以鉴别样品的晒退情况,是目前最适合冰川沉积释光测年的几种选择;（4）如有条件,尝试用不同矿物、不同粒径、不同方法进行测试对比和交叉检验。要获得第四纪冰川释光测年的最佳年代学结果,地貌学、沉积学和年代学的结合是非常必要的。  相似文献   

16.
北美五大湖区的安大略湖北岸Don Valley Brickyard、Scarborough Bluffs、Bowmanville Bluffs剖面共同构成了北美东北部最长也是最厚的陆地第四纪沉积记录, 较完整地记录了晚更新世劳伦泰德冰盖(the Laurentide Ice Sheet)的演化. 晚更新世劳伦泰德冰盖演化的重建有赖于这些经典剖面中重要沉积地层单元的准确年代学控制. 传统的地层年代学主要是依靠少量14C年代, 将主要的混杂堆积单元(diamicton)解释为气候变冷环境下的冰川扩张, 并与指示全球冰量变化的深海氧同位素曲线一一比对建立起来的. 这样建立起来的年代学存在很大的不确定性. 20世纪80-90年代的少量热释光年代也不相吻合, 最近的13个长石红外释光定年则只集中于Bowmanville Bluffs的一个分层, 并未建立整个剖面的地层年代学, 使这些经典沉积剖面的年代学一直没有得到系统的建立. 应用石英光释光SAR-SGC法测试了Bowmanville Bluffs剖面Glaciofluvial Sand单元的2个冰水沉积样品, 年代结果分别为(41.6±3.8) ka、(48.1±4.4) ka, 分析表明这一年代结果偏老, 石英颗粒可能晒褪不完全. 由于大测片无法识别晒褪不完全的颗粒, 因此, 测试更多的剖面序列的光释光年代并尝试采用粗颗粒小测片或单颗粒技术解决样品颗粒晒褪不完全的问题将是必要的.  相似文献   

17.
The Hitura open pit exposes a sedimentary sequence up to 50 m thick representing Late Saalian to Holocene glacial and non-glacial sediments. The sequence was investigated using sedimentological methods, OSL-dating and pollen and diatom analyses to reconstruct the Middle Weichselian (MWG) glacial event in the central part of the Scandinavian Ice Sheet (SIS). The results indicate that the sediment succession represents two entire glacial advance and retreat cycles. The lowermost deposits are Late Saalian esker and delta sediments overlain by sediments that correlate with the early Eemian lacustrine phase. Remnants of the Eemian soil post-dating the lacustrine phase were also observed. The area was ice-free during the entire Early Weichselian (EWG). The first glacial advance recorded in the sediments is related to the MWG. It started 79 kyr ago, deformed underlying sediments and deposited an immature till, including large detached sediment pods containing remains of organic material, soils and fluvial sediments representing allochthonous material from EWG ice-free stadials and interstadials. The glacial deposits are conformably overlain by glaciolacustrine and littoral accumulations, indicating MWG deglaciation between 62 and 55 kyr ago. Based on the fabric measurements from the till unit overlying the MWG sediments, ice advance during the Late Weichselian (LWG) was initially from the west and later from a north-northwesterly direction. The Hitura strata provide the first dating of the MWG deglaciation (55 to 62 kyr ago) from central parts of the SIS. It can be considered as a key site for studying the growth and decay of SIS during the poorly known early parts of the glaciation.  相似文献   

18.
Dating of speleothems by TL and ESR is seriously complicated by radioactive disequilibria in the uranium series. This paper presents a simple method which takes into consideration the U-series disequilibria in the case where the annual dose is determined by gamma scintillation spectrometry. The method described is based on the concept of an appropriately defined ‘laboratory age’ and enables direct reading of the age of a sample from the curve (the GH plot) independently of the results of measurements.  相似文献   

19.
A 10.5 m core from Changeable Lake in the Severnaya Zemlya Archipelago just north of the Taymyr Peninsula intersects ca. 30 cm of diamicton at its base, interpreted as a basal till. Because the upper 10.13 m of this core consists of non‐glacial sediments, a maximum numeric age for these non‐glacial sediments would provide a clear lower limit to the timing of the last glaciation in the area of Changeable Lake. Radiocarbon (14C) dating of several materials from this core yielded widely scattered results. Consequently we applied photonic dating to sediments above the diamicton. The experimental single‐aliquot‐regenerative (SAR) dose fine‐grain method was applied to two samples, using the ‘double SAR’ approach. With one exception, these fine‐grain SAR results and the results of application of the SAR method to sand‐sized quartz grains from two samples, at ca. 9.95 m and ca. 10.05 m depth, are discrepant with age estimates from the multi‐aliquot infrared‐photon‐stimulated luminescence (IR‐PSL) method applied to fine grains. Multi‐aliquot IR‐PSL dating of 10 samples produces ages increasing monotonically from ca. 4 ka at 2 m to 53 ± 4 ka at 9.97 m. These self‐consistent multi‐aliquot IR‐PSL ages, along with limiting 14C ages of >47 ka at ca. 10 m, provide direct evidence that glacial ice did not advance over this lake basin during the Last Glacial Maximum, and thus delimit the northeastern margin of the Barents–Kara Sea ice‐sheet to somewhere west of this archipelago. The last regional glaciation probably occurred during marine isotope stage (MIS) 4 or earlier. Copyright © 2004 John Wiley & Sons, Ltd.  相似文献   

20.
Nick Eyles   《Sedimentary Geology》2006,190(1-4):257-268
Water plays a dominant role in many glacial processes and the erosional, depositional and climatic significance of meltwaters and associated fluvioglacial processes cannot be overemphasized. At its maximum extent c. 20,000 years ago, the volume of the Laurentide ice sheet was 33 × 106 km3 (about the same as the volume of all ice present today on planet Earth). The bulk of this was released as water in little more than 10,000 years. Pulses of meltwater flowing to the Atlantic Ocean from large ice dammed lakes altered thermohaline circulation of the world's oceans and global climate. One such discharge event via Hudson Bay at 8200 years BP released 160,000 km3 of water in 12 months. Global sea levels recovered from glacial maximum low stands reached at about 20,000 years ago at an average rate of 15 m per thousand years but estimates of shorter term rates suggest as much as 20 m sea level rise in 1000 years and for short periods, rates as high as 4 m per hundred years. Meltwaters played a key role in lubricating ice sheet motion (and thus areal abrasion) across the inner portions of the ice sheet where it slid over rigid crystalline bedrock of the Canadian Shield. The recharge of meltwater into the ice sheets bed was instrumental in generating poorly sorted diamict sediments (till) by sliding-induced shearing and deformation of overpressured sediment and soft rock. The transformation of overpressured till into hyperconcentrated slurries in subglacial channels may have generated a highly effective erosional tool for selective overdeepening and sculpting of bedrock substrates. Some workers credit catastrophic subglacial ‘megafloods’ with the formation of drumlins and flutes on till surfaces. Subglacial melt river systems were instrumental in reworking large volumes of glaciclastic sediment to marine basins; it has been estimated that less than 6% of the total volume of glaciclastic sediment produced during the Pleistocene remains on land. Fluvioglacial and glaciolacustrine sediments and landforms dominate large tracts of the ‘glacial’ landscape in North America. The recharge of subglacial meltwater into underlying bedrock and sediment aquifers created transient reversals in the long-term equilibrium flow directions of basinal fluids. With regard to pre-Pleistocene glacial record, meltwaters moved enormous volumes of terrestrial ‘glaciclastic’ sediment to marine basins and thus played a key role in preserving a record of glaciation, a record otherwise almost entirely lost on land.  相似文献   

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