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1.
Dunite samples have been deformed non-coaxially at high temperatures and pressures. In samples which were deformed by translation glide on {Okl}[100], olivine [100] = Z-axes rotated toward the maximum extensile-strain axis. In samples which were partly or completely recrystallized syntectonically the new olivine grains attained preferred orientations with [010] = X and [100] = Z parallel to the maximum and least principal compressive stress axes, respectively. These results may be used for kinematic and dynamic analysis of naturally deformed dunites and peridotites.  相似文献   

2.
吴健君 《沉积学报》1990,8(2):135-139
针对《T》文所说的线计法存在忽略4.5ф以下的细颗粒,导致曲线形态畸变,提出用粗略筛折法“杂基处理”来修改线计法资料,使其与筛析资料形态符合等问题,本文分析了《T》文所示资料,通过正反两方面的对比、剖析,证明问题的产生是由于其计量方法不当,与抽样方法本身无关,线计法资料是可信赖的。粗略筛析法“杂基处理”的提出是不必要的。而且无论在理论上、方法上都存在许多问题,它是粒度计量错误基础上畸生出来的产物。因此,不宜采用。  相似文献   

3.
应用电感耦合等离子体质谱法(ICP-MS)分析环境地质样品中的Cd时,Zr、Mo元素的氧化物和氢氧化物会对Cd造成严重干扰,导致结果有明显的偏差。针对此问题,本文建立了膜去溶-ICP-MS直接测定环境地质样品中微量Cd的分析方法,该方法可有效地消除Zr、Mo氧化物和氢氧化物对Cd的干扰,保证结果准确、可靠。膜去溶-ICP-MS相比于常规ICP-MS测定Cd的方法,可将Zr、Mo氧化物和氢氧化物对Cd的干扰降低到0.001%,检测灵敏度提高3.5倍左右。在给定条件下,Cd的检出限为0.28 ng/L,测定下限为2.2 ng/L,精密度(RSD,n=12)为2.2%。利用该方法分析20种岩石、土壤和沉积物国家标准物质的测定值与标准值相符,表明膜去溶-ICP-MS法直接测定环境地质样品中痕量或超痕量Cd时具有一定的应用潜力。同时,用该方法对2016年中核集团组织的实验室间两个比对样品中的Cd进行测定,稳健Z比分数分别为0.500和-0.964,Z的绝对值都小于2。  相似文献   

4.
Two-dimensional finite element analysis has been used to find load–transfer relationships for translation of an infinitely long pile through undrained soil for a variety of soil-constitutive models. It has been shown that these load–transfer curves can be used as p–y curves in the analysis of single piles undergoing lateral pile head loading in undrained soils with non-linear stress–strain laws. Lateral pile response deduced from 2-D analysis input to the subgrade reaction method has been compared to the behaviour of a single pile analysed using three-dimensional finite element analysis. Good agreement between the two methods for non-linear soils suggests that the 2-D analysis may form a useful design method for calculation of p–y curves. Copyright © 1999 John Wiley & Sons, Ltd.  相似文献   

5.
Using a set of copper assay values (from soil samples collected near Surda, Singhbhum Dt., Bihar) and applying numerical methods, such as relaxation, trend surface, composite analysis, and linear moving average, residuals have been determined. Zones of positive and negative anomalies are delineated and an attempt has been made to correlate with the structural phenomena and drainage pattern of the region.  相似文献   

6.
Inter‐laboratory comparison of laser ablation ICP‐MS and SIMS U‐Pb dating of synthetic detrital zircon samples provides an insight into the state‐of‐the art of sedimentary provenance studies. Here, we report results obtained from ten laboratories that routinely perform this type of work. The achieved level of bias was mostly within ± 2% relative to the ID‐TIMS U‐Pb ages of zircons in the detrital sample, and the variation is likely to be attributed to variable Pb/U elemental fractionation due to zircon matrix differences between the samples and the reference materials used for standardisation. It has been determined that ~ 5% age difference between adjacent age peaks is currently at the limit of what can be routinely resolved by the in situ dating of detrital zircon samples. Precision of individual zircon age determination mostly reflects the data reduction and procedures of measurement uncertainty propagation, and it is largely independent of the instrumentation, analytical technique and reference samples used for standardisation. All laboratories showed a bias towards selection of larger zircon grains for analysis. The experiment confirms the previously published estimates of the minimum number of grains that have to be analysed in order to detect minor zircon age populations in detrital samples.  相似文献   

7.
Summary Shore hardness has been used to estimate some mechanical and physical properties of rocks for many years. This study differs from previous studies in a way that it is directly oriented to rock cuttability. Two Shore hardness values (SH 1 andSH 2) and a coefficient of deformation value (K) have been measured for 30 different rock samples. In the first stage of the study, optimum specific energy values for 16 different rock samples obtained from full-scale cutting tests were correlated with the Shore hardness values of the same rock samples changingSH 1 values from 9 to 66 andSH 2 values from 25 to 83, with deformation coefficient values changing from 26 to 195. In the second stage, the performance of a roadheader used in the Kü?üksu (Istanbul) tunnel was recorded in detail and the instantaneous cutting rate of the machine was determined. Then, the relationship between Shore hardness values, deformation coefficient and the instantaneous cutting rate of the machine was determined for different formations encountered. It is concluded that there is a relationship between Shore hardness values, optimum specific energy and compressive strength, which may be used to estimate the rock cuttability and the instantaneous cutting rates of roadheaders within certain limits of reliability.  相似文献   

8.
A direct, sensitive and simple method for the determination of sub-microgram amounts of platinum in acid leachates from geological materials is described. The sample is sized to plus 80-mesh and roasted at 700°C. During this operation the most important interfering elements such as C, S, Hg, Se, Te and As are eliminated. Anions and small amounts of most cations found in strongly acid leachates from rock samples do not interfere. Hydrogen peroxide is used as the oxidant during leaching with 5–7 M HCI. Platinum is reacted with Sn2+ after filtration. Addition of Rhodamine 6G precipitates a red quaternary complex. The colloidal suspension is suitable for spectrophotometric determination of platinum. While the reagent absorbance at 530 nm decreases, a peak due to the colloid appears at 565 nm. Beer's law is obeyed up to 0.6 absorbance unit, which corresponds to about 1.7 μg/ml of Pt. The sensitivity (3 times the noise level) corresponds to 0.01 μg/ml of Pt. A test procedure is described for serial analysis of 1–3-g powdered samples which enables an operator to perform from 30 to 50 analyses per man-day in the concentration range of 0.1–17 ppm of platinum. The procedure has been validated against standard samples and a recovery of 90% has been obtained with unspiked samples.  相似文献   

9.
Fire has been considered one of the most important factors in the expansion of savannas in the Gran Sabana region. In Urué, an important fire event that occurred before 1.6 kyr BP led to the replacement of ‘primary’ forests by savannas and morichales (monospecific communities of the palm Mauritia). In the present work, the secondary succession after fire is reconstructed by palynological analysis of a previously dated clay core, and the results are compared with those from studies based on present‐day ecosystems. Charcoal analysis is used to infer fire incidence and surface samples are used as modern analogues. The secondary succession is subdivided into seven seral stages: open secondary forests, helechal or dense fern community, transitional savanna, wet savanna with morichales, treeless savanna, wet savanna with morichales, and treeless savanna. Fires were common at the beginning, but climate constituted the main successional control from the transitional savanna stage onwards. The process is characterised by a continuous impoverishment of taxa, but there was a steady increase in Mauritia, due to its ability to colonise new habitats created by disturbances. The conclusions of this palynological reconstruction show good correspondence with present‐day studies on fire ecology. Copyright © 1999 John Wiley & Sons, Ltd.  相似文献   

10.
空心包体应力计广泛用于测量地应力,目前采用热敏电阻进行完全温度自补偿。通过对热敏电阻和DS18B20温度传感器进行综合比较和分析,发现采用DS18B20测量工作应变片的温度变化更有优势。设计了一种使用DS18B20作为敏感元件的测温电路系统,采用单片机进行控制,数码管进行显示,经实验室试验校核及在煤矿现场应用,证明了其可靠性和可行性。   相似文献   

11.
The degree of graphitization of carbonaceous material (CM) has been widely used as an indicator of metamorphic grade. Previous work has demonstrated that peak metamorphic temperature (T) of regional metamorphic rocks can be estimated by an area ratio (R2) of peaks recognized in Raman spectra of CM. The applicability of this method to low‐pressure (<3 kbar) contact metamorphism was tested using Raman spectroscopic analyses of samples from two contact‐metamorphic aureoles in Japan (Daimonji and Kasuga areas). A suitable measurement procedure allows the dependence of the geothermometer on sample type (thin section, chip) and incident angle of laser beam relative to the c‐axes of CM to be tested. Two important general results are: (i) in addition to standard thin sections, chips are also suitable for spectral analysis; and (ii) the incident angle of the laser beam does not significantly affect the temperature estimation, i.e. spectral measurements for the geothermometer can be carried out irrespective of the crystallographic orientation. A laser wavelength of 532 nm was used in this study compared with 514.5 nm in an independent previous study. A comparison shows that the use of a 532‐nm laser results in a slightly, but systematically larger R2 ratio than that of a 514.5‐nm laser. Taking this effect into account, our results show that there is a slight but distinct difference between the R2–T correlations shown by contact and regional metamorphic rocks: the former are slightly better‐crystallized (have slightly lower R2 values) than the latter at the same temperature. This difference is interpreted as due to the degree of associated deformation. Despite the slight difference, the results of this study coincide within the estimated errors of ±50 °C with those of the previously proposed Raman CM geothermometer, thus demonstrating the applicability of this method to contact metamorphism. To facilitate more precise temperature estimates in regions of contact metamorphism, a new calibration for analyses using a 532‐nm laser is derived. Another important observation is that the R2 ratio of metamorphosed CM in pelitic and psammitic rocks is highly heterogeneous with respect to a single sample. To obtain a reliable temperature estimate, the average R2 value must be determined by using a substantial number of measurements (usually N > 50) that adequately reflects the range of sample heterogeneity. Using this procedure (with 532‐nm laser) and adapting our new calibration, the errors of the Raman CM geothermometer for contact metamorphic rocks decrease to ～±30 °C.  相似文献   

12.
This paper deals withR-mode cluster analysis for more than 6000 analytical data from the samples of tectonite and mineralized rocks using the method of multivariate statistical analysis on the basis of division of the tectonic fault systems in the Malage Ore Field andR-mode factor analysis for the analytical data from tectonite samples collected along various directions of the faults according to fourteen variables related to the mineralizing elements which are selected in terms ofR-mode cluster analysis from the chemical composition of tectonites. Thus the distribution characteristics of primary halo anomalies have been revealed with respect to the metallogenetic elements Sn, Cu, and Pb, Zn. The tecto-geochemical features are shown by the primary halo anomalies, thus providing the theoretical basis for metallogenetic forecast in the ore field.  相似文献   

13.
A multivariate statistical technique (principal component analysis) has been used to investigate the granulometric features of 414 samples of pyroclastic rocks: 216 samples were collected from areas of recent and active volcanism in Central and Southern Italy; data for the remaining 198 samples were obtained from the literature and relate to products from Somma-Vesuvio, Mount St Helens and the Japanese volcanic arc. The analysis offers an improved means of discriminating pyroclastic deposits using their grain-size characteristics.  相似文献   

14.
Stress-path dependent behavior of a weathered clay crust   总被引：1，自引：0，他引：1  
Triaxial compression and oedometer consolidation tests are commonly performed to evaluate the strength and deformation behavior of soils. However, in the field, the stress paths imposed by various engineering works may deviate from the stress paths conventionally used in laboratory tests. Moreover, the stress-paths followed by different soil elements under a foundation are different. To obtain representative soil parameters, the laboratory stress path should be similar to that followed in the field. In this study, a significant number of stress-path triaxial tests, with stress probes in various directions, have been conducted to study the stress-path dependent behavior of an overconsolidated weathered crust of Champlain clay in Eastern Ontario. Both undrained and drained tests have been conducted for samples isotropically consolidated to the in situ vertical stress and anisotropically consolidated to in situ state of stress. The yield locus of the clay crust has been defined. It has been observed that the strength-deformation and yielding behavior of this weathered clay crust highly depends on the stress-path as well as on the in situ stress history.  相似文献   

15.
Ordination is a multivariate technique developed by plant ecologists which has proven effective in the interpretation of paleoenvironments. It allows gradational relationships among samples to be depicted in contrast to other quantitative techniques which classify samples into discrete groups. In this study, ordination is used to interpret textural data for 62 bottom samples taken from the Cape Hatteras, North Carolina, continental margin. The ordination suggests the existence of six sedimentary facies that are similar to those obtained by cluster analysis using a dendrograph display. The facies represented are: littoral sands and outer-shelf shelly sands; inner-shelf sands; outer-shelf sands and silts; outer-shelf slope silts; and two highly biogenic, deep-water silt and clayey silt facies with similar characteristics. The facies are related in a qualitative manner to the environmental processes operating off Cape Hatteras. Chicago Bridge Technical Paper No. 5139.  相似文献   

16.
Botanical analyses of fossil and modern arctic ground squirrel (Urocitellus parryii) caches and nests have been used to reconstruct the past vegetation from some parts of Beringia, but such archives are understudied in Alaska. Five modern and four fossil samples from arctic ground squirrel caches and nests provide information on late Pleistocene vegetation in Eastern Beringia. Modern arctic ground squirrel caches from Alaska's arctic tundra were dominated by willow and grass leaves and grass seeds and bearberries, which were widespread in the local vegetation as confirmed by vegetation surveys. Late Pleistocene caches from Interior Alaska were primarily composed of steppe and dry tundra graminoid and herb seeds. Graminoid cuticle analysis of fossil leaves identified Calamagrostis canadensis, Koeleria sp. and Carex albonigra as being common in the fossil samples. Stable carbon isotopes analysis of these graminoid specimens indicated that plants using the C3 photosynthetic pathways were present and functioning with medium to high water-use efficiency. Fossil plant taxa and environments from ground squirrel caches in Alaska are similar to other macrofossil assemblages from the Yukon Territory, which supports the existence of a widespread mammoth steppe ecosystem type in Eastern Beringia that persisted throughout much of the late Pleistocene.  相似文献   

17.
A saline circuit has been studied as a model of coastal evaporite system. The lipid composition of diverse salt ponds encompassing calcite, gypsum and halite domains has been determined. Most of the lipid materials has been found in the carbonate samples and is related to algal/cyanobacterial debris. Lipids in the gypsum domain are of heterotropic microbialorigin and extreme halophilic bacteria constitute the main lipid contribution in the halite samples. n-Alkane distributions with high predominance of n-docosane constitute a previously described feature of sedimentary evaporitic conditions that is charateristics of the intermediate calcite/gypsum samples. In the calcite domain, the presence of C20 highly branched isoprenid olephines, tetrahymanol and the large amounts of phytol constitute likely precursors of lipids usually found in evaporitic environments (i.e. C20 highly branched isoprenoid alkanes, gammacerane and high phytane/pristane ratios). Their occurence point to dehydration and hydrogenations as two main diagenetic processes leading to the formation of “evaporitic molecular markers”.  相似文献   

18.
During the routine analysis of chip samples from water boreholes it was noted that the DeBakken granite south of Kenhardt has high uranium and tin contents. Rock samples collected on surface, however, revealed low concentrations of both these elements indicating that they have been leached from the surface samples. The distribution of thorium in the borehole profiles showed that while both tin and uranium have been removed above the water table, other “immobile” elements and thorium remained unaffected.The geological data showed that the leaching took place since the start of the Tertiary. Initially, the movement of uranium was vertical and accumulated in pedogenic calcrete above the granite. This vertical leaching was controlled by fluctuations in the water table and took place from the Pliocene to Pleistocene. Later, in the Holocene, the pedogenic calcrete was removed and deposited as non-pedogenic calcrete along the rivers. These nodular calcrete deposits, which are abundant in Namaqualand, are mineralized only along those rivers which drain the DeBakken granite, indicating that this granite was the source of the uranium.When the water table reached depths of ten metres or more the vertical migration of uranium ceased and horizontal leaching caused by the movement of ground water became active. Where the water table cuts the surface, such as in the pans, uranium deposition due to evaporation of groundwater is still active.Leaching of uranium from this granite, together with the formation of the secondary deposits is mineralogically controlled, and is ascribed to the fact that uranium is not hosted in zircon. Granites such as the DeBakken granite, in which the uranium is hosted in biotite, monazite and apatite, cannot be recognized by surface sampling and hence a lithogeochemical approach, using sub-surface samples has to be adopted. Calculations showed that approximately 1400 tons of uranium metal has been leached from this granite since the start of the Tertiary and that the maximum reserve of the province as a whole is relatively small.The distribution of tin is erratic, and although it has been leached from the surface samples, it has not been transported for any significant distance. Thus the tin distribution in the profiles does not show the same degree of leaching as does uranium. This is ascribed to the fact that samples from a percussion drill would include both the rock fragments from which tin has been leached and the clay-rich alteration products in which it has been trapped. Tin is generally immobile when present as cassiterite, but when enclosed in biotite, and when the groundwater is enriched in chlorine and fluorine, it leaches readily from the biotite.  相似文献   

19.
Deformed conglomerates and ooidal/oncoidal packstones are commonly used to evaluate finite strain in deformed sedimentary successions. In order to obtain a correct estimate of finite strain, it is necessary to consider not only the different behaviour of matrix and objects, but also object concentration. The analysis of two-component rocks characterised by high values of packing commonly results in a substantial underestimate of bulk strain and of viscosity contrast between objects and matrix. In this study, the effects of the volumetric fraction of competent inclusions on both object and bulk measured finite strain, as well as on apparent viscosity contrast, have been investigated in naturally deformed packstones characterised by variable object concentration on the scale of the hand specimen (and hence for homogenous viscosity contrast). Object finite strain has been obtained by Rf/ analysis, whereas the Fry method provides a measure of whole-rock strain that is also a function of inclusion concentration. Therefore, the finite strain measured by the Fry method is better termed effective bulk strain. In order to investigate the role of object concentration, this parameter has been plotted against object and effective bulk strain, and also against viscosity contrast. These diagrams show that: (i) for high values of packing, measured object and effective bulk strain show values that are significantly lower with respect to the calculated maximum value (that would result in the ideal case of no particle interaction and represents therefore the real bulk strain of the samples); (ii) the viscosity contrast shows lower values with respect to the calculated maximum one (that is equal for the three principal sections of the finite strain ellipsoid), and as packing reaches the maximum value, the viscosity contrast approaches a unit value. Empirical equations have also been found that link object concentration with both object and effective bulk finite strain.  相似文献   

20.
Based on the maximum entropy concept, optimal numbers of class intervals(K) for a closed array of samples has been determined. From the analysis, two values ofK (8 and 19) are selected as the most appropriate. ForK=8, the probability of occurrence on each unequal-size interval isp i=0.125, whereasK=19 results inp i=0.0526. An objective method for determining interval limits, modified from a previous method by Full et al. (1984), is also included.Contribution 114, Instituto Argentino de Oceanografia.  相似文献   

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