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1.
The palaeomagnetism of 54 dykes sampled from the many swarms that intrude the Yilgarn Block of Western Australia shows that their directions of magnetization fall into five distinct groups.Preliminary Rb-Sr age determinations made on samples used in the study however, indicate that for one, and possibly two of those groups, the dykes belong to two widely different ages suggesting that the palaeomagnetic field has been sampled at two widely separated points in time but when its direction was essentially the same. The seven groups of directions thus obtained imply that the dykes belong to at least six, possibly seven periods of intrusion. Relative-age information relating to four of those periods, determined from cross-cutting and baked contact studies, agrees with that obtained radiometrically.The poles and ages of the groups are as follows: Group YA dykes (c. 2500 or c. 1700 m.y.) 21.7S 133.7E (A95 = 17.9°) Group YB dykes (750—700 m.y.) 19.9S 282.0E (A95 = 28.1°) Group YC dykes (1500 m.y., Group YB) 79.7N 2.7E (A95 = 13.0°) Group YD dykes (1700 m.y.) 23.5S 46.1E (A95 = 9.9°) Group YE dykes (c. 2500 m.y.) 28.3S 0.4E (A95 = 31.0°) Group YF dykes (c. 1700 m.y.) 24.7N 101.8E (A95 = 14.0°) Ravensthorpe dykes (2500 ± 100 m.y.) 38.3S 136.2E (A95 = 25.5°)Results from eight samples of the 1390 ± 140 m.y. Morawa Lavas of the Billeranga Hills yield a pole at 42.8N 22.4E (A95 = 14.7°).  相似文献   

2.
Along the northern part of the East Greenland coast the Caledonian structures are superimposed on an older fold system called the Carolinidian. Traces of this Carolinidian belt are preserved in a few isolated fragments within the Caledonian fold belt. According to Haller (1970) one of these fragments exhibiting the typical Carolinidian NNW to NW-trending infrastructural folds is the peninsula of Germania Land which is accessible near the Danish weather station Danmarkshavn. The rock sampled there is a banded gneiss of granodioritic composition with steeply inclined, NNW-trending layers. Isotopic age determinations yielded essentially two groups of ages: 1) 3,000±150 m.y. (zircon suite and Rb/Sr whole rock analyses of layers) and 2) 320–380 m.y. (Rb/Sr mineral isochrons, U-Th-Pb on sphene, K/Ar on hornblende and biotite). The egg-shaped zircons support a sedimentary origin of the banded gneiss and in conjunction with the Rb/Sr whole rock ages determine the age of formation of the banded gneiss (or its last high grade metamorphism) some 3,000 m.y. ago. No other Precambrian metamorphism or orogeny is recorded in the rock. The ages between 320–380 m.y. date a thermal event of lower amphibolite facies grade related to a late Caledonian spasm.The new isotopic data reveal the existence of very old rocks in the hinterland — away from the direction of thrusting—of the East Greenland Caledonian belt. With respect to the age of the Carolinidian fold system three geological interpretations are compatible with the results of this study:
1.  the Carolinidian fold system formed approximately 3,000 m.y. ago;
2.  the banded gneiss represents part of an old basement: the Carolinidian orogeny is younger than 3,000 m.y. Its marked structural imprint on the Danmarkshavn area was accompanied by very low grade metamorphism not recognised in the isotopic record;
3.  the fold structures observed in the Danmarkshavn area are not of Carolinidian age but belong to an earlier fold system preserved in the basement.
  相似文献   

3.
Early Aphebian dykes (lowermost Proterozoic) intrude the Archean terrain of the Slave Structural Province of the Canadian Shield and paleomagnetic results from them are reported. The Dogrib dykes, with an Rb/Sr age of 2692 ± 80 mm.y., have directions of magnetization directed toward the NW without reversals (16 sites; 309, + 37; α95 = 4°; pole 35S, 050W). The Indin dykes, with an Rb/Sr age of 2093 ± 86 mm.y., have magnetization directed toward the SE with reversals (13 sites; 131, + 58; α95 = 8°; pole 19N, 076W). Other, less well-documented data from a third dyke swarm (the “X” dykes) and a basic sill (the Duck Lake Sill), are also presented, and a very tentative polar path for the Slave Province in the earlier Proterozoic is given. This path is not greatly different from a similar very tentative early Aphebian polar path from the Archean Superior Province, considering the uncertainties in the paleomagnetic and age determinations. We interpret this to mean either that the intervening Hudsonian Structural Province (−1850 m.y.) was not the site of a wide plate-style opening and closing ocean, or if it was, the two bounding Archean cratons returned approximately to their original relative position.  相似文献   

4.
44 samples of the Jilin meteorite were analyzed by various laboratories for spallogenic, radiogenic, and trapped rare gases. A non-uniform distribution has been found for the rare gases of different origins. There have been found correlations among the spallogenic rare gases, with apparent depth effects. 43 samples were analyzed for their cosmogenic radionuclides60Co,26Al,36Cl,40K,53Mn,54Mn, and22Na. Correlations have been found between60Co and53Mn and between60Co and21Ne. The Jilin meteorite has a complex history of cosmic-ray irradiation. According to the two-stage model and the other fragments have a burying depth two stages,T 1=11 m.y. andT 2=0.3 m.y. The burying depth of all samples in the parent body can be obtained by the content of21Ne. Jilin meteorite No. 1 is located 20–142 cm from the surface, No. 4 ranges from 106–134 cm, and the other fragments have a burying depth between 15 and 150 cm. The equation of the reference plane for the surface of the 1-stage Jilin meteoroid is 0.24x+0.81y+0.53z+0.5=0. Use can also be made of60Co to determine the burying depth of all samples in the 2-stage Jilin meteoroid (under a geometry of 4π), and further to restore the preatmospheric form and size of the parent body. During its atmospheric passage, the Jilin had an ablation rate of ca. 30%. On the basis of the two-stage model and the concentration of21Ne and60Co in the samples, we propose a scheme to restore the relative position of all samples in the parent body. 12 sample-distribution regions can be sketched out. Also can be restored the relative position of all the samples in the parent body during the two stages.  相似文献   

5.
Stratigraphic and structural observations indicate that the Encounter Bay Granites concordantly intruded the youngest formations of the Kanmantoo Group in the Mount Lofty Ranges metamorphic belt prior to the culmination of the first phase of folding and associated schistosity development recorded during the early Palaeozoic Delamerian Orogeny. Metamorphic textures in the metasediments of the Kanmantoo Group suggest that cordierite crystallized locally near the granites prior to and during the F 1 folding, whereas andalusite crystallized on a regional scale during the F 1 folding and in the post‐F 1 and pre‐F 2 static phase.

Rb‐Sr isotope data for total‐rock, feldspar, and muscovite samples of the meta‐sediment‐contaminated border facies and the uncontaminated inner facies of the Encounter Bay Granites indicate that the granites were emplaced between 515 ± 8 m.y. and 506 ± 6 m.y. ago in the Late Cambrian epoch. Rb‐Sr and K‐Ar data for biotite from the granites record variable radiogenic Sr loss until about 469 m.y. ago and comparatively uniform radiogenic Ar loss until 460–475 m.y. ago. Rb‐Sr data for Kanmantoo Group metasediments and a metamorphic pegmatite indicate crystallization ages between 459–463 m.y. ago. Thus the regional andalusite‐grade temperatures and pressures, which appear responsible for the leakage of radiogenic Sr and Ar from biotite in the granites and the redistribution of Rb and Sr in the metasediments, seem to have persisted for some 50 m.y. after emplacement of the granites until the Early Ordovician epoch. There is evidence for further leakage of Sr and Ar from biotite in deformed granites from the margins of the intrusion more than 50 m.y. afterwards in the Late Silurian or Early Devonian, possibly during the F 2 folding.

Geological observations and radiometric data for other granitic rocks in southeastern South Australia, including the Palmer Granite, are consistent with this structural and metamorphic history of the Encounter Bay region.  相似文献   

6.
The preparation and characterisation of four chromium ore reference materials are described in this paper. The sample material for GCr‐1, GCr‐3 and GCr‐4 was collected from chromite deposits in Tibet, Qinghai province and Inner Mongolia. GCr‐2 is a composite sample from GCr‐1 and GCr‐4. Sample homogeneity was tested by WD‐XRF and the relative standard deviations were < 1.0%. An F‐test showed that all four materials were homogeneous. Thirteen laboratories involved in the inter‐laboratory programme provided 672 determinations (eighteen oxides and elements). Sixteen components were characterised as certified values, of which Cr2O3 ranged from 17.59 to 57.80% m/m. The contents of FeO and CO2 were taken as reference values.  相似文献   

7.
R.N. Thompson 《Lithos》1975,8(1):9-14
An intensely-welded ignimbrite has been identified in the upper part of the thick Palaeocene lava pile of Ubekendt Ejland, west Greenland. It consists of 2.3 volume present of phenocrysts and 2 percent of lithic fragments (basalt and trachyte) in a compact nitreous matrix of flattened and welded rhyolitic pumice fragments and glass shards. The phenocrysts are mostly of plagioclase (An17), together with minor amounts of sanidine (Or87), hydrothermally-altered olivine and augite, ilmenite and zircon. The major elements chemistry of the magmatic fraction of the rock is deduced from microprobe analyses of its constituent phases. It is suggested that this erupted pyroclastic rock may be a surface expression of high-level granite emplacement in southern Ubekendt Ejland. The source could have been an early acid member of the currently-exposed Sarqâta qáqâ plutonic complex. Recent Rb/Sr isotopic studies have shown that the acid and basic rocks of this intrusive centre, together with the surrounding basaltic lavas, define a single isochron (65 m.y.) with an initial 87Sr/86Sr ratio of 0.7045, appropriate to the upper mantle. The ultimate source of the Ubekendt Ejland ignimbr.es may therefore be sub-crustal.  相似文献   

8.
Fourty-four isotopic ages have been determined by K-Ar and U-Th-Pb methods for Late Palaeozoic granitic rocks in the Nanling Region, South China. All dating values vary within the range of 231–348 m.y. From the obtained dates, further evidence has been found that there do exist Late Palaeozoic granitic rocks, which can be subdivided into Late Devonian and Permian granitic rocks. Within a Late Devonian terrain, there is a granitic pluton, namely granodiorite with a zircon U-Th-Pb age of 348 m.y., while ten granitic plutons have been recognized within a Permian terrain where granites are predominant, yielding biotite K-Ar ages of 236–289 m.y. (λ β =4.72×10?10yr.?1,λ K=5.57×10?11yr.?1) and zircon U-Th-Pb ages ranging from 231 to 280 m.y., respectively. It is obvious from the dates that intrusive activity of granitic magma extensively took place in the Nanling Region during Late Palaeozoic, although no records of orogenie movements have been found, indicating that the faults are the main factor controlling the activity of granitic magma, whereas the orogenic movements are not the only prerequisite for the formation of granitic magma and the intrusive activity.  相似文献   

9.
U-Th-Pb isotopic data are reported for mineral fractions, individual chondrules and fractions of chondrule fragments from the equilibrated ordinary chondrite Richardton (H5). Chondrules and milligram-sized fractions of pyroxene-rich chondrule fragments contain highly radiogenic Pb and concordant or nearly concordant U-Th-Pb isotopic systems, and are suitable for precise Pb-Pb age determinations. Olivine and sulfide have low U concentrations and contain less radiogenic Pb. The ages of individual chondrules, pyroxene-rich and phosphate fractions are determined using U-Pb and Pb-Pb isochron and model date calculations. The Pb-Pb isochron date of 4562.7 ± 1.7 Ma of the Richardton chondrules and chondrule fragments is resolved from the Pb-Pb isochron date of 4550.7 ± 2.6 Ma obtained from multiple phosphate fractions. Possible biases of the isochron dates due to single-stage approximation of multi-stage evolution, contamination with modern common Pb, and disturbance to the system by reheating, are examined and are found to be insignificant. The chondrule and phosphate dates are interpreted as the timing of cessation of Pb diffusion during cooling following metamorphism in chondrite parent bodies. The difference in estimated closure temperatures, ∼950-1150 K for pyroxenes, and 700-800 K for phosphates (temperature estimates are based on published diffusion rates for Pb in pyroxenes and apatite), allows evaluation of the average cooling rate at 26 ± 13 K/million years for the Richardton parent body over the period of 4563-4551 my. Thermal modeling of the H-chondrite parent body (which is assumed to be asteroid 6 Hebe, heated by decay of 26Al) suggests a scenario in which accretion initiated at 1.7 m.y. after formation of calcium-aluminum-rich inclusions and continued for 3.5 m.y.  相似文献   

10.
U/Pb isotopic data for two zircon suites are presented:
  1. a pre D 1 tonalite gneiss gives an age of 443 ± 16 13 m.y.
  2. a post D 1 leucogranite gneiss gives 427 ± 11 10 m.y.
Both zircon suites contain a minor inherited pre-Cambrian component. The data confirm a lower Palaeozoic age for the major, fabric-forming D 1 event. Hercynian metamorphism which was sufficient to reset muscovite K/Ar ages to ca. 290 m.y. had little effect on the zircons. The possible importance of lower Palaeozoic orogeny in southern Europe and the uncertainties in regional palaeogeography are emphasised.  相似文献   

11.
Consider the problem of generating a realization y1 of a Gaussian random field on a dense grid of points 1 conditioned on field observations y2 collected on a sparse grid of points 2. An approach to this is to generate first an unconditional realization y over the grid =1 2, and then to produce y1 by conditioning y on the data y2. As standard methods for generating y, such as the turning bands, spectral or Cholesky approaches can have various limitations, it has been proposed by M. W. Davis to generate realizations from a matrix polynomial approximations to the square root of the covariance matrix. In this paper we describe how to generate a direct approximation to the conditional realization y1, on 1 using a variant of Davis' approach based on approximation by Chebyshev polynomials. The resulting algorithm is simple to implement, numerically stable, and bounds on the approximation error are readily available. Furthermore we show that the conditional realization y1 can be generated directly with a lower order polynomial than the unconditional realization y, and that further reductions can be achieved by exploiting a nugget effect if one is present. A pseudocode version of the algorithm is provided that can be implemented using the fast Fourier transform if the field is stationary and the grid 1 is rectangular. Finally, numerical illustrations are given of the algorithm's performance in generating various 2-D realizations of conditional processes on large sampling grids.  相似文献   

12.
The stable magnetizations of the Tasmanian Dolerites are shown to fall into two distinct groups depending upon their directions and the geographical region of the dolerites. It has been suggested that this could be a result of significant age differences between the dolerites of these groups. A series of K‐Ar determinations indicates that there is no detectable systematic age differences and the average of the five bodies dated is 170.5 ± 8.0 m.y. (not significantly different from previous K‐Ar dates from a single body). A re‐appraisal of the palaeomagnetic data, in the light of the distinct groupings of the directions, yields two significantly different pole positions‐ Lat 50.7°S, Long. 174.5°E (A9r, = 5.2°) and Lat. 47.7 °S, Long. 123.5° (A95 = 9.5°)’. The former of these is in excellent agreement with pole positions from other Lower to Middle Jurassic rocks of Australia but the significance of the latter remains obscure.  相似文献   

13.
Polymetamorphic rocks of Sifnos (Greece) have been investigated by Rb-Sr, K-Ar, and fission track methods. Critical mineral assemblages from the northern and southernmost parts of Sifnos include jadeite+quartz+3T phengite, and omphacite+garnet +3T phengite, whereas the central part is characterized by the assemblage albite+chlorite+epidote+2M 1 phengite.K-Ar and Rb-Sr dates on phengites (predominantly 3T) of the best preserved high P/itTmetamorphic rocks from northern Sifnos gave concordant ages around 42 m.y., indicating a Late Lutetian age for the high P/T metamorphism. Phengites (2M 1+3T) of less preserved high P/T assemblages yielded K-Ar dates between 48 and 41 m.y. but generally lower Rb-Sr dates. The higher K-Ar dates are interpreted as being elevated by excess argon.K-Ar and Rb-Sr ages on 2M 1 phengites from central Sifnos vary between 24 and 21 m.y. These ages date a second, greenschist-facies metamorphism which overprinted the earlier high-pressure metamorphic rocks.  相似文献   

14.
Large-scale structures, textures and mineral assemblages in the Precambrian rocks of the Banded Gneissic Complex and the overlying Delhi Group in north-central Aravalli Mountain reveal a complex deformational-crystallization history. In the basement Gneissic Complex at least three deformational events, D0, D1 and D2, and two separate episodes of metamorphism, M1 and M2, are recognized. The supracrustal Delhi Rocks display only two phases of deformation, D1 and D2, associated with a single protracted period of metamorphism, M2.The first phase of deformation (D1) of the Delhi orogeny (1650-900 m.y.) produced large isoclinal folds that are overturned towards the southeast and have gentle plunges in NE and SW directions. The second phase of deformation (D2) gave rise to tight open folds on the limbs and axial-plane surfaces of the D1 folds. These folds generally plunge towards the N and NNW at 30°–80°. In the Basement Complex one more deformation (D0) of the Pre-Delhi orogeny (> 2000 m.y.) is recorded by the presence of reclined and recumbent folds with W to WNW trending fold axes. The D0 folds were superimposed by D1 and D2 folds during the Delhi orogeny.The three deformational events have been correlated with the crystallization periods of minerals in the rocks and a setting in time is established for this part of the Aravalli range.  相似文献   

15.
K‐Ar total rock age determinations have been made on a sequence of metasedimentary rocks resting on a 2350 m.y.‐old basement in southern Eyre Peninsula, South Australia. The metasediments have an Rb‐Sr age of 1785 m.y., but K‐Ar isochrons suggest that relatively high temperatures persisted for a further 250 million years before the rocks became systems closed to K and Ar diffusion. A significant amount of 40Ar was trapped in the metasediments at the time of closure of the K‐Ar system, 1550 million years ago.  相似文献   

16.
《International Geology Review》2012,54(11):1928-1948
Many K-Ar ages have been accumulated in the world's geochronologidal laboratories but, as different decay constants are used in various countries for calculation of the formulae, it is difficult to compare the figures. Data from parallel K-Ar determinations on the one hand and from Rb-Sr and U-Pb figures often compare more favorably with the K-Ar ages calculated from the constants used in the Soviet Union. (λk - 0.557?10-10/year; λβ = 4.72?10-10/year). There follows a review of reference points in post-Precambrian time. A comparison of ages of individual geological boundaries with Kulp's 1961 scale is given. The Jurassic-Cretaceous and Triassic-Jurassic boundaries are identical in age on the basis of our new data and on Kulp's scale. The base of the Triassic cannot be older than 230-240 million years, and its duration is 40 m. y., which is more likely than the 50 m. y. suggested by Kul.P. We retain Kulp' s age of 280 m. y. for the Carboniferous- Permian boundary. The suggested age of the Devonian-Carboniferous boundary is 15 m. y. younger than Kulp's. The Silurian-Devonian boundary has been fixed on a single figure of 405 m. y. Kulp assesses the duration of the Silurian at 20 m. y., but we propose 25 m. y. The Proterozoic-Cambrian boundary cannot be older than 560 m. y. The 70 m. y. duration of the Cambrian is more realistic than Kulp's estimate which approaches 100 m. y. — J. E. Haun.  相似文献   

17.
Five deformational “episodes” (D1-D5) during which folds and associated cleavages formed, and a later period of faulting dominated by strike-slip movements, comprise the structural sequence in the Nambucca slate belt. D1 structures are most widespread and involved greatest strain; D2-D4 structures have affected progressively smaller areas and indicate progressively smaller strains. Strong compressive stresses during D1 produced horizontal shortening and vertical extension, and the D2-D4 structures result from adjustments to this initial strain. Regional metamorphism accompanied D1, and D1 strain is greatest in the more highly metamorphosed rocks. Some granitic bodies were probably emplaced at this time, but most plutons rose only after folding had ceased. Orogenesis, as indicated by folding and regional metamorphism lasted less than 10 m.y., but faulting continued for at least another 30 m.y.The slate belt accumulated close to a consuming plate margin, but deformation commenced only after subduction ceased, with compressive stresses generated by coupling across the former plate boundary. The development of a wrench regime during D5, and its continued existence during a long period of faulting, suggests either that the consuming plate boundary was replaced by a transform fault, or that subduction stepped oceanward and underthrusting was obliquely directed.  相似文献   

18.
Extensive exploration and mining at Kambalda, Western Australia has revealed a conformable mafic-ultramafic succession consisting of a sulphide ore bearing ultramafic layer located between metabasalt units. Geochemical and Rb-Sr, U-Pb isotopic analyses have been carried out on two 70–140 m sections of drill core from the metabasalts and U-Pb isotopic analyses have been made on sulphide ore samples. Greenschist metamorphism of the metabasalts is dated at 2610 ± 30 m.y. and was approximately isochemical except for addition of H2O and CO2 and a differential mobilization of K and Rb within the units. The addition of H2O and CO2 is believed to have taken place shortly after extrusion of the metabasalts in a submarine environment resulting in an early greenschist metamorphism. The later 2600 m.y. event is correlated with a high thermal regime also detected at Kalgoorlie 50 km to the north. A Pb-Pb isochron age of 2720 ± 105 m.y. may represent the metamorphic event or the time of emplacement of the metabasalts. New Sm-Nd data (Chauvelet al.; claqué--Longet al.) suggest the mafic volcanics are 3200 m.y. old. If true large scale homogenization of Pb isotopes is required. Alternatively the mafic sequence may be only slightly older than 2800 m.y. and the Sm-Nd data does not have time significance.  相似文献   

19.
U-Th-Pb, Pb-Pb, Rb-Sr and K-Ar radiometric relationships in the minerals from six selected Amîtsoq gneiss samples reveal a complicated history of variable mineral response to polymetamorphism.K-Ar dates on biotite range from 2170 to 3220 m.y. (excess argon present), on hornblende from 2340 to 2510, and on a single muscovite at 1670 m.y.Rb-Sr whole rock results give an apparent isochron of at least 4065 m.y., but this result is likely fortuitous from a small sample selection since Pb-Pb whole rock analyses give ~ 3600 m.y. and the zircons in these rocks yield a concordia-discordia intersection at 3600 m.y. Rb-Sr mineral analyses generally give a confusing and variable pattern of isotopic relationships; but hornblende, K-feldspar, apatite, allanite and sphene appear to have last responded to metamorphism at 2200–2600 m.y. Rb-Sr in biotite, epidote and, in part, plagioclase have been affected by an event at ~ 1550 m.y.U-Th-Pb data from sphene, apatite and allanite give almost concordant dates at 2500–2600 m.y. soul207Pb204Pb vs soul206Pb204Pb plots yield two separate lines for apatite (slope age 2435 m.y.) and for sphene + allanite (slope age 2530 m.y.), indicating apatite to have a different (less-radiogenic) ‘initial’ Pb than that for sphene and allanite. A similar pattern is found for the soul208Pb204Pb vs soul207Pb204Pb plot for sphene and apatite. The Pb-isotopic composition of the feldspars is very homogeneous and the least-radiogenic of all components, pointing towards a homogeneous parent material for the now lithologically diverse Amîtsoq gneisses. Using a0 = 9.307, b0 = 10.294, C0 = 29.476, t0 = 4.56 b.y., ω = 6.9 and soul232Th204Pb = 27.1; the feldspars give a model Pb age of 3500–3600 m.y. by either U-derived or Th-derived Pb. The segregation of the present Amîtsoq gneisses from the homogeneous parent material was apparently accompanied by a U and Th loss with preservation or enrichment of Pb at ~ 3600 m.y. ago. No consistent treatment of the present U-Th-Pb data will produce viable data indicating an age > 3600 m.y. for the parent materials of the Amîtsoq gneiss.Petrographie observations generally concur with radiometric results and permit the postulation of the reaction: Hbl + K-feld→ biotite + epidote + sodic plag, to account for some of the effects of the latest metamorphism.The total internal radiometric evidence indicates three major metamorphic events affected the Amîtsoq gneisses close to 3600, 2500 and 1550 m.y.  相似文献   

20.
A precise, accurate and rapid method for the sequential determination of FeO and Fe2O3 in rocks, soils and some non‐refractory minerals by 1,10‐phenanthroline spectrophotometry is described. Fe(II) and Fe(III) were leached from the sample (?200 mesh) using a mixture of NH4HF2 and H2SO4 at 40–80 °C for 10 min on a hot plate. Both Fe(II) and Fe(III) could be conveniently estimated sequentially from the same reaction mixture at the μg g?1 to percentage level. The method is better than the existing wet chemical methods, including the commonly used Pratt's titrimetric redox method, for Fe(II) and Fe(III) determinations in rock and soil samples in terms of precision, accuracy and rapidity. The throughput of the method was very high; at least forty to fifty samples could be estimated easily in a day. The results obtained compare favourably with those obtained by Pratt's method, as well as for certified/recommended values of a set of eleven certified reference materials having FeO and Fe2O3 contents in the range 0.21–14.63% and 0.58–8.48%, respectively. The optimised 1,10 phenanthroline method was found to be accurate to within 0.21% m/m FeO and 0.30% m/m Fe2O3 compared with the literature values of the certified reference materials studied.  相似文献   

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