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1.
提出了人工合成标样和化探样品经熔融处理后消除基体效应的影响,悬浮液进样ICP-AES测定化探样品中Cu、Mn,Ba、Sr、Zn、Ni、Co的分析方法,研究了悬浮液进样的最佳实验条件,经部分GBW标准物质验证分析结果与推荐值吻合。  相似文献   

2.
热电离质谱铀系法测定碳酸盐标样   总被引:5,自引:0,他引:5  
王兆荣  彭子成 《岩矿测试》1998,17(4):268-270
用高精度热电离质谱(TIMS)铀系法测定碳酸盐标样的年龄,测定结果与α谱仪铀系法进行比较,铀含量和年龄值均吻合。方法对U的回收率可达95%,Th为92%。TIMS铀系法具有样品用量少、测试时间短、精度高的优点。  相似文献   

3.
南京汤山洞穴石笋稳定同位素指示的气候与环境意义   总被引:16,自引:1,他引:15  
汪永进  许汉奎 《地质学报》2000,74(4):333-338
对南京汤山葫芦洞南壁钙板上一支长82mm石笋进行了高精度热电离质谱(TIMS)定年及氧碳同位素分析。结果表明,该支短石笋生长时段长达300ka左或(距今463~159ka),其底部年龄进一步证实南京直立人生存时代早于450kaBP。δ^13C值在MIS6/7界线上的显著漂移揭示了一次土壤侵蚀事件,结束了洞穴文化层的堆积历史。  相似文献   

4.
祁连山第四纪冰碛物的ESR测年研究   总被引:21,自引:7,他引:14  
论述了ESR测年的原理和方法,并利用ESR测年方法对祁连山的冷龙岭和走廊南山的摆浪河流域第四纪冰碛物进行了年代测定,结果表明,冰碛物样品的ESR年龄与野外地层对比推测的年龄和和^14C、TL测定的年龄基本一致,且同一冰碛物不同位位置采集的样品年龄也一致,说明本次测定的冰碛物年龄是可信及可靠的。  相似文献   

5.
刘颖  李献华 《岩矿测试》1998,17(2):112-116
用等离子体质谱(ICP-MS)对美国玄武岩标准物质BHVO-1、W-2和中国玄武岩标准物质GBW07105(GSR-3)进行了39种痕量元素分析。三个标准物质的大多数元素测定值与标准值在误差范围内一致。GSR-3中Cs、Pb、Y、Nb、Tm、Yb等元素的ICP-MS测定值与标准值存在不同程度的偏差。用同位素稀释法对GSR-3中的Pb做了进一步的精确测定,结合玄武岩的元素地球化学分析,认为GSR-3  相似文献   

6.
太平洋多金属结核及沉积物标准物质研制   总被引:8,自引:0,他引:8  
太平洋多金属结核及深海沉积物标准物质,GSPN-2,3和GSMS-2,3,4个样品已研制完成。GSPN-2,3和GSMS-2采自太平洋CC区,GSMS-3采自中太平洋海盆(CP区)。原样被加工成-200目(74μm)的均匀粉未,其均匀性采用高精度的X射线荧光光谱法检测。样品的特性值采用国内外多实验室协同分析的方式定值,有包括台湾大学在内的14个国内实验室和18个国外实验室参加了合作分析。测试组分分别达79和81个,定值组分63个。全组分的百分总和分别为:99.7%,99.5%,99.8%和99.7%。这4个标准物质已于1997年被国家技术监督局批准为国家一级标准物质,序号分别为GBW07295,GBW07296,GBW07315和GBW0731。  相似文献   

7.
WEBGEOGRAPHICINFORMATIONSYSTEMSongXianfengTheInstituteofGeography,ChineseAcademyofSciences,Beijing100101TanHaiqiaoChinaUniver...  相似文献   

8.
MID-PROTEROZOICMETAMORPHICROCKS,METAMORPHISMANDCRUSTALEVOLUTIONINTHEWESTOFLIAONINGPROVINCEYuLiangjunInstituteofGeology,Chines...  相似文献   

9.
作者对渭南黄土剖面连续采取的样品进行了系统的14C和TL年龄测定,测得的14C年龄做了δ13C校正和日历年龄校正,并与SPECMAP比较,取得了很好的结果。根据测得的年龄,S0底部143cm处的14C年龄为10300aB.P,即全新世起始于10300aB.P.;L1可划分五层,其中L(1-2)和L(1-4)为古土壤层,L(1-2)顶部14C年龄为22000aB.P.,深度为361cm,L(1-4).底部有一层明显的碳酸盐结核,其TL年龄为51910aB.P.,深度为640Cm;L1底部的TL年龄为73000aB.P.,深度为855cm,这便是马兰黄土的起始年龄;S1底部为134500aB.P.,深度为1216cm。与深海沉积物氧同位素阶段对比,马兰黄土相当于1—4阶段,S1相当于5阶段。  相似文献   

10.
郑存江  吴超 《地质实验室》1996,12(4):198-202
使用CO2激光器与ICP-AES联接,实现了地质样品的固体采样分析,加入一定量的聚三氟氯乙烯,可基本消除样品组成及元素赋存状态的影响,改善了分析结果的准确度。测定了地质样品中的Ba,Ce,Cu,Cr,La,Mn,Nb,Sc,Sr,Ti,Y,Yb和Zr等14种元素,检出限0.1×10^-6至10×10^-6,RSD一般在3%-7%,最大为10%,。  相似文献   

11.
Pant-y-ffynnon Quarry in South Wales yielded a rich cache of fossils in the early 1950s, including articulated specimens of new species (the small sauropodomorph dinosaur Pantydraco caducus and the crocodylomorph Terrestrisuchus gracilis), but no substantial study of the wider fauna of the Pant-y-ffynnon fissure systems has been published. Here, our overview of existing specimens, a few described but mostly undescribed, as well as freshly processed material, provides a comprehensive picture of the Pant-y-ffynnon palaeo-island of the Late Triassic. This was an island with a relatively impoverished fauna dominated by small clevosaurs (rhynchocephalians), including a new species, Clevosaurus cambrica, described here from a partially articulated specimen and isolated bones. The new species has a dental morphology that is intermediate between the Late Triassic Clevosaurus hudsoni, from Cromhall Quarry to the east, and the younger C. convallis from Pant Quarry to the west, suggesting adaptive radiation of clevosaurs in the palaeo-archipelago. The larger reptiles on the palaeo-island do not exceed 1.5?m in length, including a small carnivorous crocodylomorph, Terrestrisuchus, and a possible example of insular dwarfism in the basal dinosaur Pantydraco.  相似文献   

12.
Lithostratigraphy, physicochemical stratigraphy, biostratigraphy, and geochronology of the 77–70 Ma old series bracketing the Campanian–Maastrichtian boundary have been investigated by 70 experts. For the first time, direct relationships between macro- and microfossils have been established, as well as direct and indirect relationships between chemo-physical and biostratigraphical tools. A combination of criteria for selecting the boundary level, duration estimates, uncertainties on durations and on the location of biohorizons have been considered; new chronostratigraphic units are proposed. The geological site at Tercis is accepted by the Commission on Stratigraphy as the international reference for the stratigraphy of the studied interval. To cite this article: G.S. Odin, C. R. Geoscience 334 (2002) 409–414.  相似文献   

13.
Robert L. Linnen   《Lithos》2005,80(1-4):267-280
The solubilities of columbite, tantalite, wolframite, rutile, zircon and hafnon were determined as a function of the water contents in peralkaline and subaluminous granite melts. All experiments were conducted at 1035 °C and 2 kbar and the water contents of the melts ranged from nominally dry to approximately 6 wt.% H2O. Accessory phase solubilities are not affected by the water content of the peralkaline melt. By contrast, solubilities are affected by the water content of the subaluminous melt, where the solubilities of all the accessory phases examined increase with the water content of the melt, up to 2 wt.% H2O. At higher water contents, solubilities are nearly constant. It can be concluded that water is not an important control of accessory phase solubility, although the water content will affect diffusivities of components in the melt, thus whether or not accessory phases will be present as restite material. The solubility behaviour in the subaluminous and peralkaline melts supports previous spectroscopic studies, which have observed differences in the coordination of high field strength elements in dry vs. wet subaluminous granitic glasses, but not for peralkaline granitic glasses. Lastly, the fact that wolframite solubility increases with increasing water content in the subaluminous melt suggests that tungsten dissolved as a hexavalent species.  相似文献   

14.
15.
Calcite samples were extracted both from the rock matrix and the superficial coating of a karstified fault plane of an underground quarry, located in the eastern border of the Paris basin. The karstification is dated as Quaternary. Analysis of mechanical calcite twinning reveals that only the calcite matrix has also undergone a compression trending WNW that can be attributed to the Mio-Pliocene alpine collision. Both coating and matrix have undergone a strike-slip regime with σ1 roughly trending north–south, that could correspond to the regional present-day state of stress, a strike-slip compression rather trending NNW, modified by local phenomena. To cite this article: M. Rocher et al., C. R. Geoscience 335 (2003).  相似文献   

16.
正20141520 Bo Ying(Key Laboratory of Metallogeny and Mineral Assessment,MLR,Beijing 100037,China);Liu Chenglin Saline Spring Hydrochemical Characteristics and Indicators for Potassium Exploration in Southwestern and Northern Tarim Basin,Xinjiang(Acta Geoscientica Sinica,ISSN1006-3021,CN11-3474/P,34(5),2013,p.594-602,5 illus.,3 tables,28 refs.)  相似文献   

17.
正20141243Chen Ge(Hangzhou Research Institute of Petroleum Geology,PetroChina,Hangzhou 310023,China);Si Chunsong Study on Sedimentary Numerical Simulation Method of Fan Delta Sand Body(Journal of Geology,  相似文献   

18.
正20142599Chen Sanming(Guangxi Key Laboratory of Concealed Deposits Exploration,Guilin University of Technology,Guilin541004,China);He Yuzhou Block Model and Reserves Estimation of Panzhihua Iron Deposit Based on 3D Geological Modeling(Journal of Guilin University of Technology,ISSN1674-9057,CN45-1375/N,33(4),2013,p.610-615,9illus.,1table,15refs.)  相似文献   

19.
正20140594 Bai Daoyuan(Hunan Institute of Geology Survey,Changsha 410016,China);Zhong Xiang Faults in the Jingzhou Basin and Their Tectonic Settings(Geotectonica et Metallogenia,ISSN1001-1552,CN44-1595/P,37(2),2013,p.173-183,6illus.,59refs.)Key words:basin evolution,tectonic setting,South China In the Upper Paleozoic and Jurassic se-  相似文献   

20.
正20141912Cao Hui(State Key Laboratory for Continental Tectonics and Dynamics,Institute of Geology,Chinese Academy of Geological Sciences,Beijing 100037,China)Gravitational Collapse and Folding during Orogenesis:A Comparative Study of FIA Trends and Fold Axial Plane Traces(Geology in China,ISSN1000-3657,CN11-1167/P,40(6),2013,p.1818-1828,9illus.,35refs.,with  相似文献   

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