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1.
如何快速准确地建立老红砂剖面年代学标尺或区域年代学框架,是在实践中有待解决的问题。而标准生长曲线法(SGC)在减少样品测试时间、提高测年仪器的测试效率方面具有独特的优势,因此在内陆黄土及沙漠沉积年代测定中得到了广泛应用。在福建和海南海岸带老红砂分布区采集了4个剖面的测年样品共计20个,应用单片再生剂量法(SAR)及SGC法进行定年研究。结果表明:(1)福建和海南海岸带老红砂样品释光(OSL)信号均以快组分为主,在信号积分通道前0.64 s快组分的信号占据总体信号的80%以上,适合使用SAR及SGC方法测年;其快、中组分光电离截面分别为:福建老红砂2.62×10~(-17)cm~2和3.24×10~(-18)cm~2,海南老红砂2.66×10~(-17)cm~2和3.51×10~(-18)cm~2;2个区域样品的IRSL(红外激发释光信号)/OSL信号比值表明,较老样品的红外释光信号明显高于较年轻的样品,这可能是受到长石包裹体的影响,但其比值均小于10%,符合SAR与SGC测试要求。(2)SGC法在华南海岸地区老红砂OSL年代学研究中具有较好的适用性,不同样品之间的剂量生长曲线存在着相似的增长模式,可以建立标准生长曲线;但福建与海南老红砂样品之间的标准生长曲线具有较大的差异,因此在较大区域范围内运用标准生曲线法应当谨慎小心。 相似文献
2.
光释光(OSL)信号衰减曲线不同时段信号积分的选择, 直接影响到能否有效提取快组分信号, 从而影响等效剂量(De)计算的准确性。本文根据腾格里沙漠南缘古浪县附近的两个剖面的6个风成沉积物的共193个单片的单片再生剂量法(SAR)测试结果, 将石英OSL衰减曲线分解成快、中、慢与背景信号三个组分。利用分解出的OSL快组分信号建立再生曲线, 求取每个单片对应的De值, 并与4组选择OSL衰减曲线上不同时段信号积分的SAR法所计算的De值对比。结果表明, 腾格里沙漠南缘风成沉积物的De值对信号区间选择方式较为敏感; 使用通道1~2(0~0.32 s)作为快组分信号区间, 通道3~7(0.32~1.12 s)作为背景信号区间的早期背景信号扣除法获得的De值与快组分法计算的De值较一致; 晚期背景信号扣除法由于受中组分信号的显著影响, 计算的De值与真实De值之间存在较大差异。 相似文献
3.
本文以阿尔金造山带南缘出露的高镁赞岐质闪长岩为研究对象,通过系统的野外地质工作、显微岩相学、年代学和全岩地球化学分析,探讨其成因类型和源区性质,限定了阿尔金造山带构造演化格架。闪长岩LA-ICP-MS锆石U-Pb测年结果表明其形成年龄为(445±3) Ma,属晚奥陶世。地球化学数据显示:闪长岩Al2O3含量为15.11%~16.19%,且具有高MgO(3.93%~5.29%)和K2O(1.68%~2.67%)含量的特征,属于高镁钙碱性准铝质岩石;闪长岩具有较高的Cr(29.3×10-6~140×10-6)、Ni(27.1×10-6~43.5×10-6)、Ba(606×10-6~936×10-6)、Sr(513×10-6~734×10-6)和Y(26.4×10-6~31.1×10-6)含量,与典型的高镁赞岐岩类地球化学特征一致;稀土配分图和微量元素蛛网图显示闪长岩样品富集轻稀土元素和大离子亲石元素(如Rb和K),而亏损高场强元素(如Nb、Ti和Zr),表现出与俯冲带环境岩浆岩相似的性质;高Ti/Zr比值(48~60)与Mg#(46.74~53.06)、高Cr(29.3×10-6~140×10-6)与高Ni(27.1×10-6~43.5×10-6)含量等暗示闪长岩岩浆源区来自遭受俯冲组分交代过的富集岩石圈地幔。岩石成因分析表明,阿尔金造山带南缘晚奥陶世高镁赞岐质闪长岩是后碰撞构造环境下俯冲板片断离诱发地幔楔发生减压熔融而形成,代表了早古生代最强烈的区域性幔源基性岩浆侵入事件。 相似文献
4.
南海莺歌海盆地内地层普遍发育超压,东方区和乐东区是莺歌海盆地天然气成藏有利区的核心地带。其中,东方区位于底辟带中心,超压形成时间较早(9—5 Ma),主要物源来自西部昆嵩隆起区;乐东区位于莺东斜坡带,超压形成时间较晚(5—2 Ma),主要物源区为东部海南隆起区。本研究通过铸体薄片、荧光薄片、扫描电镜、电子探针、含烃包裹体微束荧光分析、流体包裹体激光拉曼成分与均一温度、X射线衍射黏土矿物等分析测试研究方法,对东方区和乐东区超压背景下黄流组砂岩储集层的岩石学与物性特征、烃类充注与成岩作用特征进行对比分析。结果显示: (1)东方区黄流组砂岩的压实作用、胶结作用较弱,物性较好(平均孔隙度17.68%,平均渗透率11.11×10-3 μm2),处于中成岩A期晚期;乐东区黄流组砂岩整体压实作用、胶结作用较强,物性较差(平均孔隙度8.94%,平均渗透率1.52×10-3 μm2),处于中成岩B期。(2)研究区储集层物性主要受沉积作用、超压背景和成岩作用的控制。物源、沉积中心与沉降中心、沉积相类型,超压形成时间和烃类充注规模共同影响了储集层的成岩作用特征及成岩—孔隙演化过程。(3)超压在一定程度上抵抗了压实作用强度,抑制了胶结作用,促进了溶蚀作用。 相似文献
5.
南海莺歌海盆地内地层普遍发育超压,东方区和乐东区是莺歌海盆地天然气成藏有利区的核心地带。其中,东方区位于底辟带中心,超压形成时间较早(9—5 Ma),主要物源来自西部昆嵩隆起区;乐东区位于莺东斜坡带,超压形成时间较晚(5—2 Ma),主要物源区为东部海南隆起区。本研究通过铸体薄片、荧光薄片、扫描电镜、电子探针、含烃包裹体微束荧光分析、流体包裹体激光拉曼成分与均一温度、X射线衍射黏土矿物等分析测试研究方法,对东方区和乐东区超压背景下黄流组砂岩储集层的岩石学与物性特征、烃类充注与成岩作用特征进行对比分析。结果显示: (1)东方区黄流组砂岩的压实作用、胶结作用较弱,物性较好(平均孔隙度17.68%,平均渗透率11.11×10-3 μm2),处于中成岩A期晚期;乐东区黄流组砂岩整体压实作用、胶结作用较强,物性较差(平均孔隙度8.94%,平均渗透率1.52×10-3 μm2),处于中成岩B期。(2)研究区储集层物性主要受沉积作用、超压背景和成岩作用的控制。物源、沉积中心与沉降中心、沉积相类型,超压形成时间和烃类充注规模共同影响了储集层的成岩作用特征及成岩—孔隙演化过程。(3)超压在一定程度上抵抗了压实作用强度,抑制了胶结作用,促进了溶蚀作用。 相似文献
6.
从湖南省北部赤山岛枫树嘴旧石器遗址剖面第2、第3和第4考古层位采集的3个沉积物样品中提取的细粒混合矿物,尝试对其红外释光(IRSL)信号进行研究。实验表明,虽然长石IRSL信号很弱,但仍可以测得信噪比足够高的红外激发后高温红外激发释光(post-IR IRSL)信号。与此同时,样品存在明显的红外激发后蓝光释光(post-IR OSL)信号,并且样品的IRSL与post-IR OSL信号均以快组分为主,这为该地区沉积物利用长石光释光信号定年提供了新的可能。鉴于长石IRSL信号较弱,根据剂量恢复实验结果,本研究采用post-IR IRSL SAR法(50℃红外激发后270℃高温红外激发,pIRIR270℃)进行等效剂量测量,同时也应用post-IR OSL SAR法定年进行比较。实验结果表明,细粒混合矿物的pIRIR270℃等效剂量分别为418.8±13.2 Gy、562.3±18.2 Gy和694.8±17.9 Gy,相对应的post-IR OSL SAR等效剂量结果为345.0±29.4 Gy、409.6±33.7 Gy和424.7±32.2 Gy。假设强烈化学风化未对沉积物的剂量率造成很大影响,基于长石pIRIR270℃信号的释光年龄为89±6 ka、118±8 ka和152±9 ka,比前人所得的石英OSL SAR法年龄老30%~55%(约20~55 ka)。通过对比不同测量条件下获得的等效剂量值来评估长石IRSL信号是否存在晒退问题,没有发现长石post-IR IRSL信号存在晒退不完全的证据。根据本研究post-IR IRSL SAR法测年结果,赤山岛枫树嘴旧石器遗址似阿舍利技术类型的石器出现在倒数第二次冰期(MIS 6)后期至末次间冰期(MIS 5)前期,比湖南道县福岩洞现代人类牙齿化石年龄(80~120 ka)稍老。作为似阿舍利技术石器制造者的赤山岛古人与福岩洞现代人的关系将是我国旧石器时代考古学和古人类学研究的一个重要课题。 相似文献
7.
准噶尔盆地沙湾凹陷西斜坡二叠系佳木河组物源体系一直备受争议,导致沉积体系“众说纷纭”。利用聚类分析、多维尺度分析及主成分分析等方法,对重矿物含量、微量元素进行分析,明确了沙湾凹陷西斜坡二叠系佳木河组砂砾岩碎屑颗粒富石英(35.41%)、长石(43.2%),贫岩屑(18.71%)。稀土元素总量(ΣREE)平均值139×10-6接近大陆上地壳(UCC)的平均值148.14×10-6,Hf-La/Th微量元素物源判别图解和La/Sc-Co/Th值表明佳木河组属于酸性岛弧区。稀土配分模式表现为右倾分布模式,整体上具有“轻稀土元素富集、重稀土元素亏损”的特征,指示源岩以长英质火山岩为主,即“一源”。在同一物源下,又可以分为4个物源区:新光1井—中佳6井物源区,车排10井—中佳5井—中佳4井—中佳3井物源区,车排7井—车排005井体系物源区,车排5井物源区,即“四区”。构造背景判别图解揭示了佳木河组形成于大陆岛弧环境。该研究将有助于对沙湾凹陷西斜坡的沉积体系及古水系的准确恢复和远景区油气储集层的准确预测。 相似文献
8.
现代暖期(Current Warm Period,CWP,1850—至今)以来全球气温升高,南海北部陆坡底层海水温度升高、海平面上升影响海底天然气水合物稳定性。为探究现代暖期气候变暖对南海北部陆坡水合物分解影响,本文模拟计算了东沙海域、神狐海域、西沙海域、琼东南海域水合物赋存水深最浅处水合物的饱和度在1 000年内变化情况,评估了受现代暖期气候变暖影响水合物赋存水深范围,讨论了水合物分解量及其对环境影响。结果发现:(1)受现代暖期气候变暖影响,东沙海域、西沙海域、琼东南海域水合物分解,神狐海域水合物不分解;当东沙海域、西沙海域、琼东南海域水深分别超过665、770、725 m,水合物不分解;(2)现代暖期自始以来,南海北部陆坡水合物分解量为9.36×107~3.83×108 m3,产生的甲烷量为1.54×1010~6.28×1010 m3;(3)受现代暖期气候变暖影响,南海北部陆坡每年水合物分解量为5.5×105~2.25×106 m3,产生的甲烷量为9.02×107~3.69×108 m3,这些甲烷中3.61×105~1.48×106 m3能够进入大气,对温室效应贡献度为每年我国人类生活的0.01%~0.06%;与此同时,1.77×107~7.23×107 m3甲烷可能会在海水中被氧化形成弱酸,加重南海北部陆坡海水酸化。 相似文献
9.
对辽东岫岩地区锉草沟黑云母二长花岗岩、刘家堡子二云母二长花岗岩进行了岩相学观察、LA-ICP-MS锆石U-Pb年代学和地球化学测试。测年结果显示锉草沟黑云母二长花岗岩的锆石年龄为(162.7±2.5) Ma,刘家堡子二云母二长花岗岩锆石年龄为(156.9±1.1) Ma,均形成于晚侏罗世。两个岩体具有相似的地球化学特征,主量元素具有富Si、Al和K以及贫Fe、Mg和Ca的特征,A/CNK值为1.01~1.15,A/NK值为1.13~1.33;微量元素亏损Nb、P和Ti等高场强元素,富集Rb、K和Hf等不相容元素,(La/Yb)N为7.10~41.13,Eu无负异常,具有高Sr (128×10-6~454×10-6)、低Y(3.03×10-6~12.10×10-6)和Yb(0.40×10-6~1.32×10-6)特征,表现为具有埃达克质亲和性的过铝质I型花岗岩。结合两个岩体的时空特点分析认为,在晚侏罗世时期,辽东岫岩地区花岗质岩浆作用的发生是太平洋Izanaqi板块向西俯冲、西伯利亚板块与华北板块碰撞挤压造成地壳增厚,进而引发下地壳物质部分熔融的结果。 相似文献
10.
以4 000 m以浅的主要热储层为研究对象,通过总结天津地热资源特征及勘查现状,利用热储法结合水均衡法和数值耦合优化管理模型计算天津市主要热储层30 a热流体可采资源量及可采热量。结果表明: 到2045年底,热储法结合水均衡法计算的热流体可采资源量和可采热量分别为27.012×1018 m3和47.0×1016 J; 数值耦合优化管理模型计算的热流体可采资源量和可采热量分别为26.6×1018 m3和49.74×1016 J; 2种方法计算结果基本一致。该计算结果可为天津市地热资源合理开发及科学管理提供依据。 相似文献
11.
High-resolution loess deposits are widely distributed in Arid Central Asia (ACA) and provide important records associated with dust transportation, paleoenvironmental and paleoclimatic evolution. The chronology is the foundation of the research into loess deposits as an environmental archive. In recent decades, the gradually developed optical dating method has been increasingly matured and become an important approach to establishing the loess-paleosol sequences. Here, we summarized and discussed previous work on loess chronology mainly based on optical dating approach in ACA. The following understandings have been listed: ① In comparison with optical dating method, the suitable material for 14C dating is uncommon in ACA. However, the dating range of luminescence dating is more extensive, and the dating materials are accessible. Thus, the optical dating is widely applicable in the establishment of loess framework in this area. ② Until now, the quartz Single Aliquot Regeneration (SAR) method can be applied to the establishment of loess-paleosol sequence since last glacial period. But several issues remain unaddressed. For example, the Optically Stimulated Luminescence (OSL) signal sensitivity of quartz grains are low in some areas. Furthermore, the results of OSL dating of different grain sizes within a single sample are inconsistent in some areas. The solution of these problems still requires more methodological research. ③ The post-IR IRSL (pIRIR) and multiple elevated temperature stimulation (MET-pIRIR) protoCols of feldspar have basically overcome the anomalous fading issue in the traditional IRSL dating process. In ACA, the framework since MIS 7 can be established with K-feldspar luminescence dating method. Compared with quartz luminescence characteristics, the K-feldspar luminescence signals are more sensitive and exhibit a high saturation level. In specific applications, it is necessary to establish the age frame according to the luminescence sensitivity, the age of samples or other factors. 相似文献
12.
JAN‐PIETER BUYLAERT SÉBASTIEN HUOT ANDREW S. MURRAY PETER VAN DEN HAUTE 《Boreas: An International Journal of Quaternary Research》2011,40(1):46-56
Buylaert, J.‐P., Huot, S., Murray, A.S. & Van den haute, P.: Infrared stimulated luminescence dating of an Eemian (MIS 5e) site in Denmark using K‐feldspar. Boreas, 10.1111/j.1502‐3885.2010.00156.x. ISSN 0300‐9483. Infrared stimulated luminescence (IRSL) dating of K‐feldspars may be an alternative to quartz optically stimulated luminescence (OSL) dating when the quartz OSL signal is too close to saturation or when the quartz luminescence characteristics are unsuitable. In this paper, Eemian (MIS 5e) coastal marine sands exposed in a cliff section on the coast of southern Jutland (Denmark) are used to test the accuracy and precision of IRSL dating using K‐feldspars. This material has been used previously to test quartz OSL dating ( Murray & Funder 2003 ): a small systematic underestimation of <10% compared to the expected age of ～130 ka was reported. In our study, a single‐aliquot regenerative‐dose (SAR) IRSL protocol is used to determine values of equivalent dose (De) and the corresponding fading rates (g values). A significant age underestimation (of up to ～35%) is observed; this is attributed to anomalous fading. Using a single site‐average fading rate of 3.66 ± 0.09%/decade to correct the IRSL ages for all samples provides good agreement between the average fading‐corrected K‐feldspar age (119 ± 6 ka) and the independent age control (132–125 ka). This is despite the reservations of Huntley & Lamothe (2001) that their fading correction method is not expected to work on samples older than ～20–50 ka. This fading‐corrected feldspar result is not significantly different from the overall revised quartz age (114 ± 7 ka) also presented here. We conclude that fading‐corrected IRSL ages measured using K‐feldspar may be both precise and accurate over a greater age range than might be otherwise expected. 相似文献
13.
Optically stimulated luminescence (OSL) dating of polymineral fine-grained loess samples collected from the southern Loess
Plateau of China was conducted using the single-aliquot regenerative-dose (SAR) protocol. A ‘Double-SAR’ procedure in which
aliquots are subjected to both infrared (IR) and blue stimulations was used, and two sets of equivalent dose (D
e
) determinations were produced. These doses are assumed to be predominantly related to the feldspathic and quartz fine grain
populations, respectively. The results revealed that the OSL ages estimated by infrared stimulated luminescence (IRSL) signals
and those estimated by [post-IR] stimulated luminescence ([post-IR] OSL) signals disagreed. Specifically, the ages estimated
using the IRSL signals were smaller than those estimated using [post-IR] OSL signals. The results of an anomalous fading test
of the two types of OSL signals revealed that the [post-IR] OSL signals from the etched sub-sample (by H2SiF6 and HF) and the un-etched sub-sample did not fade significantly. However, the IRSL signals from the un-etched sub-sample
showed obvious signs of fading. These findings indicate that the lower age estimated by IRSL is due to the anomalous fading
of feldspar IR signals in the polymineral fine grains. For samples collected from greater than 100 cm, the estimates of their
OSL ages using two types of luminescence signals generally agreed with their pre-estimated ages, especially those of the [post-IR]
OSL signals. However, for the three samples that were collected from a depth of less than 100 cm, their OSL ages were remarkably
underestimated, possibly due to the enhanced human activity (such as soil cultivation) that has occurred in the region since
3000 a B.P. 相似文献
14.
甘肃玉门地区第四纪晚期构造阶地的红外释光测年 总被引：4，自引：0，他引：4
光释光（ＯＳＬ）测年是近几年从热释光（ＴＬ）测年基础工起来的测定第四纪沉积物年龄的一种新技术，其原理与ＴＬ测年类似。不同的是：ＯＳＬ是单色光束激发品体中储存的电离辐射能使其以光的形式释放出来。当用近红外线束作为激光光源时称之为红外释光测年。与ＴＬ测年相比，ＩＳＬ测年可以不考虑残留的ＯＳＬ信号，而且测量具有简便，迅速且准确等优点。本文用细颗粒红外释放技术对玉门地区的构造阶地进行了年龄测定，初步结果表 相似文献
15.
4He是测定地下水年龄理想的示踪剂之一,由于测年时间尺度及多成因等问题,其测年结果通常与14C测年结果缺乏一致性。通过采集河北平原第四系承压水中的惰性气体（He、Ne、Ar、Kr、Xe）及14C样品,利用CE（封闭系统平衡）模型分离出地下水中的放射性成因4Herad浓度为（5.43～8 994）×10-8 cm3·STP/g,进而得到地下水的4He年龄为8.8～55.9 ka;相应样品的14C测年结果为7.7～35.2 ka。结果表明,2种测年结果在河北平原具有很好的一致性。 相似文献
16.
松辽盆地中二叠统哲斯组发育一套暗色泥岩、灰色砂砾岩与灰岩沉积组合,灰岩中产海相腕足类和双壳类化石。由于受钻井进尺和取心资料限制,前人对盆地覆盖区晚古生代地层及其沉积环境研究较少。对采自松辽盆地杜101井、杜103井剖面哲斯组的白云质灰岩进行了系统的稳定同位素和微量元素、稀土元素分析,首次获取了盆地覆盖区中二叠统灰岩元素地球化学资料。测试结果显示碳同位素δ13CPDB值一般>0(均值为1.68‰),氧同位素δ18OPDB值全部<-15‰(均值为-19.98‰),碳、氧稳定同位素关系图解显示二者呈正相关关系,表明白云岩化作用对灰岩同位素改造作用明显。稀土元素(REE+Y)总量为56.88×10-6~143.72×10-6,均值为108.92×10-6,PAAS标准化后显示具有轻稀土相对于中稀土和重稀土亏损、δEu(均值0.94,最大值1.57)负异常、δCe(均值0.87,最大值1.06)普遍负异常和相对高的Y/Ho均值(均值34.59)等特点,与正常海相具有大体相同的稀土元素配分模式;而微量元素Ba(均值281.55×10-6)、Zn(均值71.91×10-6)、Y(均值17.44×10-6)、Zr(均值117.75×10-6)和Rb(均值66.84×10-6)等元素含量整体较高,Sr/Ba(均值2.91)、Th/U(均值2.75)、V/Cr(均值1.45)和V/(V+Ni)(均值0.66)等比值适中,指示研究区哲斯组沉积时期主体为一种频繁受陆源碎屑混染作用影响的碳酸盐台地或滨海岸环境。 相似文献
17.
A robust feldspar luminescence dating method for Middle and Late Pleistocene sediments 总被引：2，自引：0，他引：2
Jan‐Pieter Buylaert Mayank Jain Andrew S. Murray Kristina J. Thomsen Christine Thiel Reza Sohbati 《Boreas: An International Journal of Quaternary Research》2012,41(3):435-451
Luminescence dating is used extensively to provide absolute chronologies for Late Pleistocene sediments. Nowadays, most optical dates are based on quartz optically stimulated luminescence (OSL). However, the application of this signal is usually limited to the last ～100 ka because of saturation of the quartz luminescence signal with dose. In contrast, the feldspar infrared stimulated luminescence (IRSL) dose–response curve grows to much higher doses; this has the potential to extend the datable age range by a factor of 4–5 compared with quartz OSL. However, it has been known for several decades that this IRSL signal is unstable, and this instability often gives rise to significant age underestimation. Here we test against independent age control the recently developed feldspar post‐IR IRSL approach to the dating of sediments, which appears to avoid signal instability. A physical model explaining our observations is discussed, and the method is shown to be accurate back to 600 ka. The post‐IR IRSL signal is reduced by exposure to daylight more slowly than that from quartz and low‐temperature IRSL, preventing its general application to young (e.g. Holocene) sediments. Nevertheless, this new approach is widely applicable (feldspar of appropriate luminescence behaviour is even more ubiquitous than quartz). These characteristics make this a method of great importance for the dating of Middle and Late Pleistocene deposits. 相似文献
18.
小狐狸山钼多金属矿床位于内蒙古北山地区的东北部,矿区内出露的地层主要为奥陶系咸水湖组火山岩。本次工作显示,小狐狸山矿床赋矿火山岩地层存在安山玢岩呈岩株状侵位于奥陶系咸水湖组安山岩中,测得该安山玢岩(XHLS-01)的锆石LA-ICP-MS U-Pb同位素年龄为(419±5) Ma,对应晚志留世,晚于奥陶纪安山岩的成岩年代(489±11) Ma,研究成果更正了对矿区仅发育奥陶纪火山岩的传统认识。小狐狸山矿区晚志留世安山玢岩w(SiO2)为57.18%~58.19%,w(K2O+Na2O)为5.78%~6.97%,w(TiO2)为0.57%~0.90%,为富钾贫钠、准铝质岩石,与奥陶纪低钾钙碱性的安山岩不同;微量元素显示安山岩和安山玢岩均呈大离子亲石元素富集、高场强元素亏损特征,安山玢岩稀土总量(∑REE含量)为71.9×10-6~72.24×10-6,低于安山岩96.89×10-6,Eu呈较弱负异常。以上显示小狐狸山矿区晚志留世安山玢岩的母岩浆来自俯冲洋壳板片交代的亏损地幔源区,上升过程中经历了较弱的分离结晶和同化混染作用。小狐狸山志留纪安山玢岩和奥陶纪安山岩均形成于岛弧环境。综合区域地质、年代学和地球化学研究显示,内蒙古北山地区早古生代具有相似的构造演化过程,同属西伯利亚板块与塔里木板块之间的岛弧增生带。 相似文献