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1.
In this paper we report progresses in the realization of self-standing bent crystals, which are suitable as optical elements for Laue lenses, i.e. for optic to focus hard X-rays in the 100–1000 keV energy range. The curvature of the crystals is a key factor to enhance diffraction efficiency and energy bandpass for such an optic. In particular, two bent crystals featuring a thickness of 5 mm, made of Si and Ge respectively, were produced at the Sensor and Semiconductor Laboratory in Ferrara, Italy. The crystals were bent through the application of a carbon fibre composite. This proved to be a relatively low cost method for crystal bending, suitable for mass production. The manufactured samples were characterised via optical interferometry, and showed a fairly uniform curvature. Finally, the samples were tested exploiting hard X-ray diffraction at the ID11 facility of the European Synchrotron Radiation Facility (ESRF) in Grenoble, France. A careful analysis of the experimental data highlighted that the samples feature large energy bandpass, wide geometrical acceptance for incoming hard X-rays, and high diffraction efficiency. We therefore conclude that such self-standing crystals are good candidates as Laue lens components for astrophysics applications.  相似文献   

2.
Based on the laws of X-ray diffraction in crystals, Laue lenses offer a promising way to achieve the sensitivity and angular resolution leap required for the next generation of hard X-ray and gamma-ray telescopes.The present paper describes the instrumental responses of Laue diffraction lenses designed for nuclear astrophysics. Different possible geometries are discussed, as well as the corresponding spectral and imaging capabilities. These theoretical predictions are then compared with Monte-Carlo simulations and experimental results (ground and stratospheric observations from the CLAIRE project). PACS 95.55.Ka, 61.50.Ah, 61.10.−i, 41.50.+h  相似文献   

3.
A major goal of the MAX program is to detect and measure gamma rays produced following the nuclear reactions that take place in a supernova explosion. To detect a reasonable number of supernovae, sensitivities of the order of a few times 10-7 γ cm-2sec-1 are needed – much better than possible with current instruments. The approach in the MAX program is to use a crystal diffraction lens to collect photons over a large area and concentrate them on a small well-shielded detector, greatly improving the signal to noise ratio. The crystals need to have both high diffraction efficiency and a relatively broad energy bandwidth. With mosaic crystals there is a trade-off between bandwidth and diffraction efficiency – one can have either high efficiency or large bandwidth, but not both without losing too much intensity through atomic absorption. A recent breakthrough in our understanding of crystal diffraction for high-energy gamma rays has made it possible to develop crystals that have both high diffraction efficiency and a relatively broad energy bandwidth. These crystals have near perfect crystal structure, but the crystalline planes are slightly curved. Such curved planes can be obtained in 3 different ways, by using mixed crystals with a composition gradient, by applying a thermal gradient, and by mechanically bending a near perfect crystal. A series of experiments have been performed on all three types of crystals using high-energy x-ray beams from the Advanced Photon Source at the Argonne National Laboratory. Experiments performed at 3 energies, 93 keV, 123 keV and 153 keV, with both the thermal gradient Si crystals and with the mechanically bent Si crystals, demonstrated that one can achieve diffraction efficiencies approaching 100% with moderate energy bandwidths (ΔE/E = 1.4%) and low atomic absorption (transmission = 0.65), in excellent agreement with theory. The use of this type of diffraction crystal is expected to increase the sensitivity of gamma ray telescopes by a factor of 5 over that possible with normal mosaic crystals.  相似文献   

4.
Beyond the present technologies, Laue diffraction lenses are very promising tools in the field of gamma-ray astrophysics. The theoretical concepts of this kind of instruments are based on the Laue diffraction in crystals, discovered almost 100 years ago. Though they are commonly used in crystallography, their application to γ-ray focusing in astrophysics requires some specific developments, e.g. in terms of energy and imaging responses. The present article describes the physics of X-ray diffraction in crystals. In the context of the Darwin model of mosaic crystals, some peculiar aspects, relevant to the astrophysical observation, are discussed. The evaluation and optimization of diffraction efficiency are discussed, especially with rigards to the crystal’s mosaicity and thickness, its spatial extent and deviations to the “ideally imperfect” Darwin model. PACS 95.55.Ka, 61.50.Ah, 61.10.−i, 41.50.+h  相似文献   

5.
Large single crystals of copper with an uniform and very narrow mosaic spread between 25 seconds and 1 minute of arc are now available at I.L.L. This result is of great interest in the construction of a Laue lens for astrophysical applications for which such quality copper single crystals may be used. The X-ray diffraction properties of copper single crystals produced at I.L.L. were studied for x-ray energies ranging from 100 keV to 400 keV. Several monocrystalline plates with different thicknesses and mosaic distributions were then prepared from the as-grown crystals in order to measure their diffraction efficiency as a function of energy. As expected, the value of the peak reflectivity depends on the crystal thickness. Reflectivity measurements show the excellent properties of copper crystals for gamma-ray diffraction. A peak reflectivity of 24% was measured at 220 keV from a copper single crystal of 3.75 mm thickness having a mosaic spread of 1.5 minutes of arc. Some technical aspects on the preparation of copper single crystal plates are also discussed.  相似文献   

6.
Silicon mono-crystals have been bent thanks to a series of parallel superficial indentations on one of the largest faces of the crystals. This technique relies on irreversible compression of the crystal beneath and beside the indentations. This latter causes deformation with no need for external device, resulting in a uniform self-standing curvature within the crystal. Indented Si crystals have been characterized at European Synchrotron Radiation Facility using a monochromatic beam ranging from 150 to 700 keV. Crystals exhibited very high diffraction efficiency over a broad range of energy, peaking 95% at 150 keV. Measured angular spread of the diffracted beam was always very close to the morphological curvature of the sample under investigation, proving that the energy passband of bent crystals can be controlled by simply imparting a selected curvature to the sample. The method of superficial indentations was found to offer high reproducibility and easy control of diffraction properties of the crystals. Moreover the method is cheap and simple, being based on mass production tools. A Laue lens made of crystals bent by superficial indentations can provide high-efficiency concentration of hard x-ray photons, leading significant improvement in many astrophysical applications.  相似文献   

7.
The Mungindi Iron Nickel Meteorite was investigated by neutron diffraction. All layers of the γ-phase (separated from each other by α-phase bars) form, from the crystallographic point of view, the same, big single crystal. The perfection of this single crystal is very high. In the kamacite phase each individual “single crystal” is broken into a group of crystals.  相似文献   

8.
If sensitive enough, future missions for nuclear astrophysics will be a great help in understanding supernovae explosions. In contrast to coded-mask instruments, both crystal diffraction lenses and grazing angle mirrors offer a possibility to construct a sensitive instrument to detect γ-ray lines in supernovae. We report on possible implementations of grazing angle mirrors and simulations carried out to determine their performance.  相似文献   

9.
Both Ge1−x Si x mosaic crystals and Si1−x Ge x crystals with gradient of composition could be grown using the modified Czochralski technique to produce the diffracting elements for the MAX gamma ray telescope. Although many elements cut from the mosaic crystal and used before for CLAIRE gamma ray telescope had an efficiency up to 20%, the overall efficiency of the lens was about 8.1 ± 0.7 %, which is more than twice lower than the theoretically predicted efficiency. Some causes of this behaviour are discussed. In addition to mosaic crystals, the growth of Si1−x Ge x crystals with a gradient of composition and their properties are analysed. Such composition-gradient crystals could be a promising way to improve the diffraction efficiency of Laue lens for MAX.  相似文献   

10.
Abstract— We have studied carbonate and associated oxides and glasses in a demountable section of Allan Hills 84001 (ALH 84001) using optical, scanning, and transmission electron microscopy (TEM) to elucidate their origins and the shock history of the rock. Massive, fracture‐zone, and fracture‐filling carbonates in typical locations were characterized by TEM, X‐ray microanalysis, and electron diffraction in a comprehensive study that preserved textural and spatial relationships. Orthopyroxene is highly deformed, fractured, partially comminuted, and essentially unrecovered. Lamellae of diaplectic glass and other features indicate shock pressures >30 GPa. Bridging acicular crystals and foamy glass at contacts of orthopyroxene fragments indicate localized melting and vaporization of orthopyroxene. Carbonate crystals are >5 mm in size, untwinned, and very largely exhibit the R3c calcite structure. Evidence of plastic deformation is generally found mildly only in fracture‐zone and fracture‐filling carbonates, even adjacent to highly deformed orthopyroxene, and appears to have been caused by low‐stress effects including differential shrinkage. High dislocation densities like those observed in moderately shocked calcite are absent. Carbonate contains impactderived glasses of plagioclase, silica, and orthopyroxene composition indicating brief localized impact heating. Stringers and lenses of orthopyroxene glass in fracture‐filling carbonate imply flow of carbonates and crystallization during an impact. Periclase (MgO) occurs in magnesite as 30–50 nm crystals adjacent to voids and negative crystals and as ?1 μm patches of 3 nm crystals showing weak preferred orientation consistent with (111)MgO//(0001)carb, as observed in the thermal decomposition of CaCO3 to CaO. Magnetite crystals that are epitaxially oriented at voids, negative crystals, and microfractures clearly formed in situ. Fully embedded, faceted magnetites are topotactically oriented, in general with (111)mag//(0001)carb, so that their oxygen layers are aligned. In optically opaque rims, magnetites are more irregularly shaped and, except for the smallest crystals, poorly aligned. All magnetite and periclase crystals probably formed by exsolution from slightly non‐stoichiometric, CO2‐poor carbonate following impact‐induced thermal decomposition. Any magnetites that existed in the rock before shock heating could not have preserved evidence for biogenic activity.  相似文献   

11.
SEM photographs were taken of euhedral olivine grains from the Murchison C2 chondrite and several terrestrial and lunar occurrences. In general, the crystal faces of the meteorite grains are rough and uneven, with irregular growth patterns. They are very similar to crystal faces on terrestrial olivine grains that formed by sublimation from a vapor phase. They are very different from the relatively smooth and featureless surfaces of magmatic olivine crystals that precipitated from igneous melts. Qualitatively, the surface morphology of the crystal supports the contention that many euhedral crystals of olivine in C2 meteorites condensed from a gas phase.  相似文献   

12.
Abstract Small crystals of an optically uniaxial Ti-bearing calcium aluminosilicate were discovered in a mixer furnace slag consisting mostly of åkermanitic melilite. The crystals have the same unit cell as those observed for a phase crystallized from slowly-cooled melts used to simulate the formation of aluminous inclusions in meteorites. Moreover, compositions of synthetic and meteoritic occurrences of the phase are all very similar and can be expressed in terms of a binary solid solution between the end-members Ca3TiAl2Si3O14 and Ca3Ti(AlTi)(AlSi2)O14. Thus, crystallographic and crystallochemical information obtained from crystals in the mixer furnace slag can be used to constrain the origin of similar crystals found in meteoritic inclusions. We separated crystals from the mixer furnace slag by acid leaching; some were used for EPMA analysis, others were crushed for study by TEM methods or X-ray powder diffraction. Convergent beam electron diffraction shows that the crystals belong to the trigonal (rhombohedral) class and have point group symmetry 3m. X-ray powder diffraction gives the unit cell parameters a = 0.791 ± 0.009 nm, c = 0.492 ± 0.006 nm. The results suggest that the mineral has space group symmetry P3ml or P31m.  相似文献   

13.
The existence of noctilucent clouds probably indicates that there are submicron ice crystals in the upper atmosphere at altitudes of 80–85 km. For ice crystals to form at all, the temperature in the cloud region must be very low. The pressure at these heights is such that the ice crystals have relatively large settling speeds and growth has to be rapid enough for the crystals to reach observable size before they drop clear of the saturated region. The mesosphere is thought to be rather dry, with water vapour mixing ratios of a few parts per million only and it becomes difficult to envisage conditions where the growth rate is large enough to give crystals of observable size. In this paper, the results of numerical calculations of crystal sizes are discussed to provide a guide to the interpretation of observational data.  相似文献   

14.
Abstract— Calcite crystals within the Kaibab limestone in Meteor Crater, Arizona, are examined to understand how calcite is deformed during a meteorite impact. The Kaibab limestone is a silty finegrained and fossiliferous dolomudstone and the calcite crystals occur as replaced evaporite nodules with impact‐induced twinning. Twinning in the calcite is variable with deformational regimes based on abundances of crystals with twins and twin densities within crystals. The twins are similar to those that are seen in low tectonically deformed regimes. Low levels of shock are inferred from minor peak broadening of the X‐ray diffraction patterns (XRD) of the calcite crystals. In addition, electron spin resonance (ESR) spectroscopy data also indicates low shock levels (<3.0 GPa). Quantitative shock pressures and correlation between the XRD and ESR results are poor due to the inferred low shock levels in conjunction with the analytical error associated in calculation of the shock pressures.  相似文献   

15.
X-ray diffraction is a widely used technique for measuring the crystal structure of a compressed material. Recently, short pulse x-ray sources have been used to measure the crystal structure in-situ while a sample is being dynamically loaded. To reach the ultra high pressures that are unattainable in static experiments at temperatures lower than using shock techniques, shockless quasi-isentropic compression is required. Shockless compression has been demonstrated as a successful means of accessing high pressures. The National Ignition Facility (NIF), which will begin doing high pressure material science in 2010, it should be possible to reach over 2 TPa quasi-isentropically. This paper outlines how x-ray diffraction could be used to study the crystal structure in laser driven, shocklessly compressed targets the same way it has been used in shock compressed samples. A simulation of a shockless laser driven iron is used to generate simulated diffraction signals, and recent experimental results are presented.  相似文献   

16.
We will report on the current configuration of the X-ray facility of the University of Ferrara recently used to perform reflectivity tests of mosaic crystals and to calibrate the experiment JEM–X aboard Integral. The facility is now located in the technological campus of the University of Ferrara in a new building (named LARIX laboratory= ̳LARge ̳Italian ̳X-ray facility) that includes a tunnel 100 m long with, on the sides, two large experimental rooms. The facility is being improved for determining the optical axis of mosaic crystals in Laue configuration, for calibrating Laue lenses and hard X-ray mirror prototypes.  相似文献   

17.
The status of dark matter searches with inorganic scintillator detectors at Boulby mine is reviewed and the results of tests with a CsI(Tl) crystal are presented. The objectives of the latter experiment were to study anomalous fast events previously observed and to identify ways to remove this background. Clear indications were found that these events were due to surface contamination of crystals by alphas, probably from radon decay. A new array of unencapsulated NaI(Tl) crystals immersed either in liquid paraffin or pure nitrogen atmosphere is under construction at Boulby. Such an approach allows complete control of the surface of the crystals and the ability to remove any surface contamination. First data from the unencapsulated NaI(Tl) do not show the presence of anomalous fast events.  相似文献   

18.
Happy Canyon [found: 1971, 34° 46.5′N, 101° 33.6′W, Texas] consists of about 85 vol. % enstatite (Fs 0.4%), 5 to 10 vol % plagioclase (An 26%), and 5 vol % diopside (Fs 0.9%). In addition, there are minor remnants of metal (Ni 6.35 wt %, Si-free) and troilite (with 5.10 wt % Cr and 1.15 wt % Ti) that have survived extensive terrestrial weathering. The meteorite has a cumulate texture, uniform-size euhedral, prismatic crystals of enstatite (0.3 to 0.4 mm long) with interstitial plagioclase, diopside, troilite, and metal. The enstatite crystals are dominantly disordered and occur in alignments that suggest flow. There are no chondrules or remnants of chondrules. The enstatite crystals contain internal negative crystal voids, which are charactieristic of enstatite achondrites, as well as internal branching submicron rivulet dislocations. The bulk composition is that of an E6 enstatite chondrite, however, it has the texture of a crystal cumulate; achondritic, but unlike that of enstatite achondrites. Glass of a granitic composition occurs mainly in the mesostasis and is compositionally like the glass found inside pyroxene crystals in the Cumberland Falls enstatite achondrite. Happy Canyon is most simply explained as an E6 composition that has melted and reprecipitated at a slightly higher oxidation state, at some depth (> 7 km), possibly in the core volume of a small, asteroidal-size parent body. In terms of classification, it occupies the gap between the recrystallized enstatite chondrites and the igneous, crystalline, unbrecciated enstatite achondrites like Shallowater. Happy Canyon is a new type of enstatite achondrite  相似文献   

19.
With ESA’s INTEGRAL mission gamma-ray astronomy has advanced to the point where major scientific advances must be expected from detailed studies of the many new point sources. The interest in developing focusing telescopes operating in the soft gamma-ray regime up to 1 MeV is therefore mounting rapidly. Telescopes based on Laue diffraction of gamma-rays from crystals appear as one promising route, although the practical difficulties of realizing a large scale Laue lens are certainly not small. In this paper I have attempted to develop an optimized lens design considering the size and mass constraints of a specific medium size launch vehicle. The introduction of the lens mass as a primary design driver has some surprising effects for the choice of material for the crystals and new tradeoff considerations are introduced.  相似文献   

20.
Abstract— The matrix of the CM2 carbonaceous chondrite Murray contains rare micrometer‐sized prismatic crystals of aragonite that formed during late‐stage parent body aqueous alteration. The aragonite was identified by X‐ray microanalysis coupled with electron backscatter diffraction (EBSD), TEM selected area electron diffraction and cathodoluminescence spectroscopy. The sixteen crystals found all occur within loose and elongate submillimeter‐sized clusters and one cluster is present in each of the two thin sections studied. Orientation determinations using EBSD show that the c axes of aragonite crystals within each cluster lie roughly in a plane, itself aligned approximately parallel to the long axis of the host cluster. Aragonite is inferred to have crystallized after calcite but before completion of static/impact‐related compaction. The clusters developed by growth of aragonite within films of aqueous fluids that had a relatively high Mg/Ca ratio. These fluids were focused within zones of high porosity and permeability along a weak compactional fabric in the matrix and this fabric is also likely to have influenced the orientations of aragonite crystals as they grew. These results suggest that aragonite probably occurs in most of those carbonaceous chondrites that have undergone moderate degrees of parent body aqueous alteration and may provide further insights into the evolution of pore fluid compositions and volumes and the chronology of asteroidal evolution.  相似文献   

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