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晚第四纪细颗粒河流阶地沉积物的准确定年是当前光释光测年研究中的一个难点。利用简单多片再生法(SMAR)、单片再生法(SAR)等对新疆西南天山喀什前陆盆地明尧勒背斜喀浪勾律克河阶地沉积物样品的细颗粒石英光释光(BLSL)信号、混合矿物红外释光信号(IRSL)和红外后蓝光释光信号([Post-IR]OSL)进行测量。通过对比同一样品的细颗粒石英BLSL、混合矿物IRSL和[Post-IR]OSL的等效剂量值,认为细颗粒石英简单多片再生法是河流阶地沉积物释光测年最为适用的方法之一。对于细颗粒混合矿物而言,由于长石矿物的异常衰退,对于等效剂量De>70Gy的样品,其IRSL等效剂量值均偏小;其[Post-IR]OSL等效剂量值仍需慎重使用。通过对同一样品细颗粒石英多个测片的单片再生法等效剂量值分布以及简单多片再生法多个测片校正后天然释光信号强度的一致性判断,认为样品LEDL03-87q,LEDL03-86q和LEDL04-54q在沉积时的光晒退是不均匀的,采用最小等效剂量组分来计算沉积年龄 相似文献
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等效剂量预热温度坪实验是光释光(OSL)测年中确定预热温度的常用手段,一般选择坪区温度作为OSL测年的预热温度。对于黄土细颗粒石英,无论采用单片再生法(SAR)还是简单多片再生法(SMAR),以10s为预热时间,其天然和再生剂量预热温度坪区间均为250～280℃,试验剂量的预热温度分布较广,如180～260℃。常规等效剂量预热温度坪实验需要耗费较长的实验室时间。通过对SMAR法测试数据的再分析发现,天然与再生剂量OSL信号校正强度的比值(N/R)随预热温度的变化与常规等效剂量坪实验中等效剂量随预热温度的变化有着相似的趋势,这样,N/R预热温度坪就可作为黄土样品细颗粒石英等效剂量预热温度坪的替代,为实验室OSL测年确定预热温度提供一个简捷途径 相似文献
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通过对滹沱河冲洪积物、阳原盆地湖相地层细颗粒石英天然热转移光释光(TT-OSL)信号测量、回授剂量恢复测试以及简单多片光释光(OSL)与回授光释光(Re-OSL)测量结果对比等,探讨了细颗粒石英回授光释光在水成沉积物测年中应用的可能性。结果表明,冲积样品回授光释光信号没有随深度逐步增加的规律,而湖相样品热转移光释光信号随深度逐渐增大;冲洪积物细颗粒石英样品回授光释光不能得出剂量值,剂量不能恢复;而湖相样品回授实验室附加剂量与测得的剂量在2%的误差范围内一致,说明回授光释光测年在一定时间范围内对于湖相样品测年是可行的;细颗粒石英回授释光在测量>10万a的湖相样品年龄方面具有很大的潜力 相似文献
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古湖岸堤沉积物石英光释光测年研究:以中国东北兴凯湖为例 总被引：1，自引：0，他引：1
古湖岸堤是湖面波动的地貌证据,可以用来重建古湖泊演化.古湖岸堤沉积物的准确测年是应用此地貌学证据重建湖泊演化的关键.以我国兴凯湖最低一级湖岸堤——大湖岗为研究对象,采用石英小片技术,应用单片再生剂量法(SAR)对大湖岗2个不同位置的剖面风成砂质沉积物(共13个样品)进行了光释光(OSL)测年.样品石英组分的光释光衰减曲线特征表明,样品的释光信号以快组分为主,预热坪和实验室剂量恢复实验结果表明,SAR法可以用来测量兴凯湖古湖岸堤样品的等效剂量.通过分析样品等效剂量分布情况和比较3种年龄模型(平均值模型、中值模型和最小值模型),认为大湖岗湖滨砂质沉积物在沉积埋藏前石英光释光信号晒退完全,获得的OSL年龄是可信的.年代结果表明,大湖岗采自不同位置的2个剖面的年代范围一致,且各个剖面中所有年代均随地层顺序变化;另外,2个样品的OSL年龄与同层位的炭屑样品的14C年代结果在误差范围内一致,进一步表明OSL测年技术可以获得可靠的兴凯湖岸堤沉积物的年龄.尽管与前人使用热释光(TL)测年方法研究大湖岗形成年代有较大差别,本文认为兴凯湖最低一级古湖岸堤——大湖岗形成于距今约1.24-0.50 ka. 相似文献
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水成相沉积物细颗粒石英光释光综合生长曲线的建立与应用 总被引：1，自引：0，他引：1
选择中国不同地区的冲洪积相等水成相沉积物样品,根据其简单多片再生法(SMAR)测量数据建立了细颗粒石英光释光信号的综合生长曲线(Standardised growth curves,SGC)。对未知年龄的水成相沉积物细颗粒石英样品,通过测量其天然光释光信号和试验剂量响应信号,并利用上述SGC方程可计算出其等效剂量值。将此值与简单多片再生法(SMAR)测量结果相比较,统计得出对于天然等效剂量为12~65Gy的样品,其误差可达19%;对于天然剂量>65Gy的样品,其误差更大;对于等效剂量<12Gy的样品,最大误差也达25%。实验表明,应用这个SGC估计未知年龄样品的等效剂量值范围,再对样品采用简单多片再生法(或单片再生法)进一步测量,可大大节省测量时间 相似文献
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文中报道了细颗粒石英光释光测年中测量等效剂量的一种可靠技术——简单多片再生法。该技术的核心是引入单片再生法中试验剂量校正感量变化的功能,即在天然和再生多测片光释光信号测量后,再对各测片辐照以试验剂量,利用试验剂量的光释光信号响应对各测片归一化,同时校正可能发生的感量变化。从方法学上,这一技术具有以下优点1)试验剂量可以校正各测片的感量变化;2)对各测片归一化,克服了实验数据分散度的问题;3)通过对比简单多片再生法与单片再生法在测年中的表现,证实简单多片再生法可以克服单片再生法中可能发生的光释光信号的积累问题。最后,文中通过测定参考年龄样品,即洛川剖面末次冰期马兰黄土(L1)的开始堆积年龄,验证了简单多片再生法的可靠性,即在提高测量准确度和精度的同时,更节约时间 相似文献
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采集来自毛乌素沙地东南缘巴图湾、大沟湾和三岔河等3处典型湖相地层出露点的3个样品,分别提取石英和钾长石矿物组分,采用小片技术(样品直径2 mm)进行释光年代测试,并将两种矿物年代结果进行对比研究.应用单片再生剂量(SAR)流程测试了石英样品的等效剂量(预热温度选为260℃).剂量恢复实验和光释光特性显示,SAR流程测试条件选择合适,样品沉积前光释光信号晒退完全,说明石英年代结果可靠.另外,应用两步红外激发(激发温度分别为50℃和150℃)的单片再生剂量流程(post-infrared infrared-stimulated luminescence,简写为p IRIR流程)测试钾长石样品的等效剂量,剂量恢复实验和释光特性等各项检验均符合要求,剩余剂量在-0.2~0.026 Gy之间,可忽略不计.钾长石的p IRIR150信号异常衰减速率为0.55~1.71(%/decade),因造成的误差较小,故无需对年代结果进行校正.3处湖相地层的石英年代分别为11.3±0.9、6.5±0.6、2.7±0.2 ka BP,钾长石p IRIR150年代分别为10.0±0.7、6.9±0.5、2.4±0.2 ka BP,两者在误差范围内一致,说明毛乌素沙地东南缘的全新世湖相沉积物适合用钾长石p IRIR150流程进行释光测年.本研究为毛乌素沙地部分样品因石英信号较弱而无法测年问题提供了解决办法,也为该区域全新世,尤其是历史时期(近2000年)以来的环境变化研究提供了年代学支撑. 相似文献
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对新疆阜康断裂带中段大黄山探槽的23个样品进行了细颗粒石英光释光简单多片再生法测年。样品LED12-297等效剂量的预热坪实验结果表明,在220~260℃的预热温度范围内均能获得基本一致的等效剂量值。测年结果显示,样品年龄与地层的时序性一致,表明阜康断裂带为全新世活动断层。根据探槽剖面错断的最新地层及其上覆地层的光释光年龄判断,断层的最新1次古地震事件发生在距今(1.90±0.14)ka~(3.47±0.17)ka。根据地层的垂直位移量与测年结果得到,阜康断层大黄山段的垂直滑动速率为0.17mm/a。 相似文献
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The loess deposits surrounding the high mountainous regions of Central Asia play an important role in understanding environmental changes in Eurasia on orbital and sub-orbital timescales. However, problems with dating Central Asian loess have limited the interpretation of climatic and environmental data, especially on sub-orbital timescales. We selected a controversial loess section, Zeketai (ZKT, with a thickness of 23 m), in the Yili basin in Xinjiang Province in western China, to establish a detailed and systematic Optically Stimulated Luminescence (OSL) chronology. Quartz grains of 38–63 μm were isolated from 15 samples and the single-aliquot regenerative-dose (SAR) protocol was employed for De determination. OSL ages are in stratigraphic order and range from 13.8 ± 1 to 72 ± 6 ka, suggesting continuous loess accumulation during the last glaciation. We compared these dating results with that of the previously published fine-grain sized quartz (4–11 μm) using simplified multiple aliquot regenerative-dose (SMAR) protocol, and with the previous published radiocarbon dating (14C) ages on snail shells. With the exception of three young samples from the upper 6 m of the section, the SMAR dating results are basically consistent with the results using the SAR protocol. Both the SMAR and SAR OSL ages are consistently older than the 14C ages, and the radiocarbon date results should be used with caution since they appear to have been underestimated. 相似文献
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2008年5月12日四川汶川发生MS8.0大地震,形成了200多km长的地震地表破裂带。破裂带的古地震研究对于认识龙门山断裂带的活动习性和大地震的发生规律具有重要的理论和现实意义。文中用光释光(OSL)测年中的校正感量简单多片再生法(SMAR),对映秀-北川地震地表破裂带擂鼓探槽样品进行了光释光测年,并对探槽中含有的炭屑进行了AMS14C测年。样品的光释光年龄和校正的AMS14C年龄吻合,该地区与汶川地震类似规模的上一次古地震事件发生在距今约(2.1±0.2)ka至(1.1±0.2)ka间 相似文献
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Quartz optically stimulated luminescence (OSL) dating has been applied to sandy beach ridge systems from the Magdalen Islands in the center of the Gulf of St. Lawrence (Quebec, Canada) to provide the first chronological framework for these features. Nineteen beach ridges (22 samples) from four different sites throughout the archipelago were investigated. At one of the sites, samples were taken at 9 m and 7.5 m depth using a vibracore. The quartz is dominated by the fast OSL component and a single-aliquot regenerative-dose (SAR) protocol was used to measure the equivalent doses; a low preheat (180°C/10 s) was chosen to avoid the influence of thermal transfer. The average dose recovery ratio of all samples is 1.02 ± 0.02 (n = 130) suggesting that the SAR protocol works satisfactorily on this material. The OSL ages are internally consistent and supported by independent age control (radiocarbon). The OSL ages indicate that the ridges were built between 2.6 ± 0.2 ka and 0.40 ± 0.10 ka, i.e. during a period of sea level rise. This rise eroded adjacent sandstone cliffs, which contributed a significant sediment supply to the littoral drift and beaches. Some low-lying coasts in the archipelago are still prograding, despite a relative sea level increase of ∼1.6 mm/a over the last 600 years. The late Holocene ages obtained in this study indicate that these processes have been active for at least the past two thousand years. This study demonstrates for the first time that OSL dating using quartz has great potential in this area, and is an appropriate method for establishing precise chronologies for coastal sediments in this region of the Gulf of St. Lawrence. 相似文献
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《Quaternary Geochronology》2008,3(1-2):114-136
We present chronological constraints on a suite of permanently frozen fluvial deposits which contain ancient DNA (aDNA) from the Taimyr Peninsula of north-central Siberia. The luminescence phenomenology of these samples is first discussed, focusing on the optically stimulated luminescence (OSL) decay curve characteristics, thermoluminescence (TL) properties, and signal compositions of quartz from these previously unstudied deposits. Secondly, we assess the suitability of these samples for OSL dating and present the OSL chronologies obtained using both single-grain and multi-grain equivalent dose (De) measurements. The results of our analyses reveal a large amount of inter-aliquot variability in OSL decay curve shape that is directly related to differences in the size of the 280 °C TL peak and the associated slowly bleached ‘S2’ OSL component. Longer OSL stimulation durations are adopted in the De measurement procedure to prevent the progressive build-up of slowly bleached signal components throughout successive single-aliquot regenerative-dose (SAR) measurement cycles. The use of low preheat temperatures in the SAR procedure also reduces the deleterious effects of these slowly bleached signal components. The resultant single-grain and multi-grain OSL chronologies obtained using this approach are stratigraphically consistent and are in close agreement with independently established 14C ages at our sites. The findings of this research reveal the potential of OSL dating as a means of providing a reliable chronometric framework for sedimentary aDNA records in permafrost environments. 相似文献
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Edward J. Rhodes Patricia C. Fanning Simon J. Holdaway 《Quaternary Geochronology》2010,5(2-3):348-352
Research conducted by the Western New South Wales Archaeology Program (WNSWAP) provides the opportunity to assess the reliability of optically stimulated luminescence (OSL) dating of late Pleistocene and Holocene fluvial sediments and burnt stone samples from arid zone geoarchaeological contexts. A large number of radiocarbon age determinations of charcoal preserved in heat retainer hearths provides independent chronological control at these contexts. We describe a rapid OSL methodology for dating burnt hearth stones to complement previously applied radiocarbon methods, which we have tested using 37 samples from hearths with radiocarbon determinations. We propose a geoarchaeological model in which these hearths were constructed by people whose activity took place on an archaeological surface, formed by the earlier deposition of fluvial sediments. Here we demonstrate the veracity of this model by dating sediments lying stratigraphically below the hearths, and use the radiocarbon age control and chronological consistency to assess the accuracy and reliability of both small aliquot and single grain single aliquot regenerative-dose (SAR) OSL dating. While small aliquot age estimates are in most cases in agreement with independent control, the single grain determinations using a finite mixture model (FMM) appear to provide improved chronological resolution. Using single grains, we note some problems in the application of the FMM and in the dating of young samples in the range of 1–100 years. As many samples may have resided close to the surface since deposition, we have developed a mathematical function to describe gamma and cosmic dose rate contributions at burial depths down to 40 cm. These OSL age estimates allow us to reject the model of intensification of human activity as responsible for the observed pattern of archaeological radiocarbon determinations in this part of the Australian arid zone. 相似文献
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Whilst optically stimulated luminescence (OSL) is commonly more suitable for sediment dating because of faster signal resetting, thermoluminescence (TL) remains important for dating burnt material, e.g. in archaeological contexts, or for studying the luminescence properties of different materials. A lack of user-optimized analysis software for TL data has exacerbated the decline of TL dating in comparison to OSL. However, exciting developments in TL dating of flint and calcite indicate a rise in application of this underused method.R is a programming language and environment for statistical computing and graphics. It provides a wide variety of statistical and graphical techniques and is highly extendable. A package specifically designed for luminescence data analysis is available. However, it mainly includes functions for the analysis of OSL data. The TLdating package is a new R package specifically dedicated to TL dating. This package is designed to be fully compatible with the existing Luminescence package and is user-friendly. It includes functions for TL data pretreatment and palaeodose estimation using the MAAD and the SAR protocols. The functionality of the TLdating package is evaluated using heated flints from Taibeh, Jordan. 相似文献