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1.
容量法测定方铅矿中高含量银   总被引:1,自引:0,他引:1  
刘茂荣 《岩矿测试》2001,20(2):147-149
报道了采用HNO3-H2SO4-HF溶样,KI容量法测定硅、铅含量较高样品中高含量银的方法。试验了滴定反应的酸度条件。在1.6mol/L HNO3介质中,银与碘化钾反应,生成碘化银沉淀。银的标准加入回收率为97.8%-100.4%。精密度试验,相对标准偏差为0.92%(n=11)。该法可溶解含硅银矿及角银矿中的银。方法已被用于测定矿石中高含量银。  相似文献   

2.
用ICP-AES法测定银精矿中银铜铅锌砷   总被引:3,自引:0,他引:3  
研究了在王水介质中用ICP-AES法同时测定银精矿中银、铜、铅、锌、砷的分析方法,进行了加标回收试验,回收率为92%-107%,相对标准偏差2.3%-11%,确定了各元素的测定下限,与行业标准进行了方法对照实验。本方法已用于矿样的测定。  相似文献   

3.
北岭金矿中的针碲银金矿的研究   总被引:2,自引:0,他引:2       下载免费PDF全文
针碲银金矿产于北岭金矿的晚期矿化阶段,赋存于梳状排列网脉状的石英中,与自然金伴生。矿物组合为针碲银金矿-自然碲-碲铅矿-自然金-石英和针碲银金-碲镍矿-碲铅矿-石英,自然碲,碲镍矿,碲铅矿在针碲银金矿中呈包裹体产出。针碲银金矿呈柱状,板状,粒状晶形,聚片双晶,具强非均质性及双反射和反射多色性,HV50=216-219kg/mm^2,其化学成分:Ag10.58%-12.36%,Au23.70%-24  相似文献   

4.
发展了一种可在野外快速测定0.010—50μg/g银量的新方法。此法由两个各自独立而又配套的部分组成。一是直接测定0.25—50μg/g银量的Ag-TMK-SDS三元络合物光导比色测定法;二是测定0.010—0.25μg/g银量的巯基棉分离富集微珠析出比色法。可在同一份试液中依次完成。前者检出限为0.006μg/ml(K=3);测定铜、铅和锌矿石标样GSO-Cu-1(含银3.87μg/g)、GSO-Ph-1(含银14.7μg/g)和GSO-Zn-1(含银13.5μg/g)中的银,RDS(n=11)分别为1.6%、3.7%和3.4%;后法可检出5ng/g银;测定地球化学标样GSD-3(含银0.59μg/g)中的银,RSD(n=11)为6.t%。方法较为简便、快速、准确和灵敏。用光导比色计测定,结果准确度、精度均有较大改善,且与室内原子吸收法相当。故所定方法具有广阔的应用前景。  相似文献   

5.
研究了利用二苯硫脲-甲基异丁酮泡塑振荡吸附富集Au、Ag的条件,并采用金试剂-TBP液珠萃取比色法测定地质样品中的金、银。方法的检出限:Au为0.5×10-9,Ag为5×10-9。  相似文献   

6.
原子吸收法测定炼银炉渣中的金   总被引:6,自引:1,他引:6  
刘茂荣 《岩矿测试》2001,20(1):68-70
采用HF-H2SO4除硅,萃取-原子吸收法测定炼银炉渣中的金。样品加标回收率为92.0%-104.0%,相对标准偏差为3.8%(n=11)。将该法应用到炼银炉渣中金的测定,结果符合分析质量要求。  相似文献   

7.
澜沧铅锌银铜矿床矿物包裹体及成矿物化条件的研究   总被引:4,自引:0,他引:4  
李虎杰  田煦 《矿产与地质》1995,9(2):107-111
矿物流体包裹体的研究表明,澜沧铅锌银铜矿床成矿流体的温度为160 ̄350℃,压力69000kPa,盐度4.6 ̄17.0NaClwt%,密度0.85 ̄1.0g/cm^3,fs210^-9.3 ̄10^-11.0Pa,fo210^-35 ̄10^-37Pa,Ph值5.1 ̄5.7。成矿元素主要以氯化物络合物的形式迁移、温度降低,fs2和pH值的升高是引起矿物质沉淀的主要因素。  相似文献   

8.
薛光 《黄金地质》1995,1(1):68-72
研究了利用二苯硫脲-甲基异丁酮泡塑振荡吸附富集Au,Ag的条件,并采用金试剂-TBP液珠萃取比色法测定地质样品中的金,银,方法的检出限:Au为0.5×10^-9,Ag为5×10^-9。  相似文献   

9.
中国周边国家银矿床主要分布于原苏联、蒙古、日本、朝鲜、菲律宾、缅甸、印尼等国家。有5种类型银矿床可与中国相应地区银(含银)矿床进行类比,即(1)大陆边缘带陆相火山岩型(金-)银(-多金属)矿床;(2)火山(一次火山)热液型含银黄铁矿型铜或多金属矿床;(3)斑岩型银或含银金-铜(铅-锌-锡)矿床;(4)变质热液交代型金-银矿床或银-铅-锌矿床;(5)矽卡岩型含银磁铁矿或多金属矿床;并提出我国相应地区  相似文献   

10.
福建碧田铜金银矿床中的含银黄铜矿研究   总被引:2,自引:0,他引:2  
陈殿芬  韩秀伶 《地质论评》1997,43(5):529-534
福建碧田矿床是成因上与燕山晚期次火山岩有关的铜金银矿床。含银黄铜矿产于该矿床的金银矿石和银矿石中。含银黄铜矿呈粒度约0.004-0.07mm的他形粒状与银金矿,金银矿,自然银,辉银矿,黄铜矿,闪锌矿等共生,在空气中极易氧化。含银黄铜矿的银含量变化在1.045%-14.273%之间,平均值为4.37%。与黄铜矿比较,含银黄铜帮中硫含量变化不大,但铁与银有反消长关系。  相似文献   

11.
Pant-y-ffynnon Quarry in South Wales yielded a rich cache of fossils in the early 1950s, including articulated specimens of new species (the small sauropodomorph dinosaur Pantydraco caducus and the crocodylomorph Terrestrisuchus gracilis), but no substantial study of the wider fauna of the Pant-y-ffynnon fissure systems has been published. Here, our overview of existing specimens, a few described but mostly undescribed, as well as freshly processed material, provides a comprehensive picture of the Pant-y-ffynnon palaeo-island of the Late Triassic. This was an island with a relatively impoverished fauna dominated by small clevosaurs (rhynchocephalians), including a new species, Clevosaurus cambrica, described here from a partially articulated specimen and isolated bones. The new species has a dental morphology that is intermediate between the Late Triassic Clevosaurus hudsoni, from Cromhall Quarry to the east, and the younger C. convallis from Pant Quarry to the west, suggesting adaptive radiation of clevosaurs in the palaeo-archipelago. The larger reptiles on the palaeo-island do not exceed 1.5?m in length, including a small carnivorous crocodylomorph, Terrestrisuchus, and a possible example of insular dwarfism in the basal dinosaur Pantydraco.  相似文献   

12.
Robert L. Linnen   《Lithos》2005,80(1-4):267-280
The solubilities of columbite, tantalite, wolframite, rutile, zircon and hafnon were determined as a function of the water contents in peralkaline and subaluminous granite melts. All experiments were conducted at 1035 °C and 2 kbar and the water contents of the melts ranged from nominally dry to approximately 6 wt.% H2O. Accessory phase solubilities are not affected by the water content of the peralkaline melt. By contrast, solubilities are affected by the water content of the subaluminous melt, where the solubilities of all the accessory phases examined increase with the water content of the melt, up to 2 wt.% H2O. At higher water contents, solubilities are nearly constant. It can be concluded that water is not an important control of accessory phase solubility, although the water content will affect diffusivities of components in the melt, thus whether or not accessory phases will be present as restite material. The solubility behaviour in the subaluminous and peralkaline melts supports previous spectroscopic studies, which have observed differences in the coordination of high field strength elements in dry vs. wet subaluminous granitic glasses, but not for peralkaline granitic glasses. Lastly, the fact that wolframite solubility increases with increasing water content in the subaluminous melt suggests that tungsten dissolved as a hexavalent species.  相似文献   

13.
Calcite samples were extracted both from the rock matrix and the superficial coating of a karstified fault plane of an underground quarry, located in the eastern border of the Paris basin. The karstification is dated as Quaternary. Analysis of mechanical calcite twinning reveals that only the calcite matrix has also undergone a compression trending WNW that can be attributed to the Mio-Pliocene alpine collision. Both coating and matrix have undergone a strike-slip regime with σ1 roughly trending north–south, that could correspond to the regional present-day state of stress, a strike-slip compression rather trending NNW, modified by local phenomena. To cite this article: M. Rocher et al., C. R. Geoscience 335 (2003).  相似文献   

14.
HYDROGEOLOGY     
正20141756 Chen Ruige(Mathematical College,China University of Geosciences,Beijing100083,China);Zhou Xun Numerical Simulation of Groundwater Level Fluctuation in a Coastal Confined Aquifer with Sloping Initial Groundwater Level Induced by the Tide(Geological Bulletin of China,ISSN1671-2552,CN11-4648/P,32(7),2013,p.1099-1104,6 illus.,16 refs.) Key words:confined water,groundwater level  相似文献   

15.
正20141408 Cai Jia(Institute of Geology,Chinese Academy of Geological Sciences,Beijing100037,China);Liu Fulai Petrogenesis and Metamorphic P-T Conditions of Garnet-Spinel-Biotitebearing Paragneiss in Danangou Area,Daqingshan-Wulashan Metamorphic Complex Belt(Acta Petrologica Sinica,ISSN1000-0569,CN11-1922/P,29(7),  相似文献   

16.
17.
正20142386An Guoying(China Aero Geophysical Survey and Remote Sensing Center for Land and Resources,Beijing 100083,China)Application of Satellite Remote Sensing in Regional Hydrogeological Investigation:Taking Cenozoic Strata in Wenquan Sheet(1∶250 000)of Karakoram Range as an Example(Geosci-  相似文献   

18.
正20141016An Chengbang(Key Laboratory of Western China’s Environmental Systems,Ministry of Education,Lanzhou University,Lanzhou 730000,China);Zhao Yongtao Lake Records during the Last Glacial Maximum from Xinjiang,NW China and Their Climatic Impli-  相似文献   

19.
正20141538 Cao Qing(School of Earth Sciences and Engineering,Xi’an Petroleum University,Xi’an 710065,China);Zhao Jingzhou Characteristics and Significance of Fluid Inclusions from Majiagou Formation,Yichuan Huangling Area,Ordos Basin(Advances in Earth Science,ISSN1001-8166,CN62-1091/P,28(7),2013,p.819-828,7 illus.,3 tables,43 refs.)  相似文献   

20.
GEOCHEMISTRY     
正20142002 Wei Hualing(Institute of Geophysical and Geochemical Exploration,Chinese Academy of Geological Sciences,Langfang065000,China);Zhou Guohua Element Content and Mineral Compositions in Different Sizes of Soil in Tongling Area,Anhui Province(Geological Bulletin of China,ISSN1671-2552,CN11-4648/P,32(11),2013,p.1861  相似文献   

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