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1.
After the Salawusu and Shuidonggou sites, the Wulanmulun site found in 2011 is another important Paleolithic site in Ordos, China, due to its numerous stone artifacts and animal fossils. Here, we carry out a combined luminescence and radiocarbon dating of the site. The luminescence dating was done on coarse-grained quartz from 24 sediment samples using a single-aliquot regenerative-dose (SAR) protocol. The radiocarbon dating was performed on ten charcoal samples and one bone sample using acid-base-acid (ABA) and acid–base-wet oxidation-stepped combustion (ABOx-SC) pretreatments. The results showed that: (i) although some samples show relative large (>20%) overdispersion in De distribution (small aliquots), the quartz grains are considered to be sufficiently bleached before burial; (ii) the quartz OSL ages of ∼4–65 ka obtained for the samples are generally stratigraphically consistent and reliable; (iii) the radiocarbon ages obtained using the ABA pretreatment procedure are much younger than the corresponding OSL ages, and the radiocarbon ages obtained using the ABOx-SC method are beyond or close to the laboratory background. The radiocarbon ages obtained using the ABA treatment were considered to be underestimated. This implication is that caution must be taken for dating Chinese Paleolithic (>25 ka) using the ABA pretreatment procedure on carbon samples. Finally, the cultural layers from the Wulanmulun site are deduced to be between 50 and 65 ka. 相似文献
2.
Sediments of river deltas provide valuable records of past coastal environments. Optically-stimulated luminescence (OSL) dating has become an alternative to radiocarbon dating for constraining the sediment chronology in large deltas that allow for sufficient sunlight bleaching of sediments during the fluvial transport. However, its applicability to smaller deltas with mountainous riverine systems has not been confirmed yet. To check this, we examine multiple signals from two Holocene sediment cores in the wave-dominated Thu Bon River delta in central Vietnam. Two cores were collected, respectively, 3.9 km and 1.2 km inland from the present shoreline and both show a >-25-m thick succession of coarsening-upward mud to sand deposits. Coarse grains (180–250 μm in diameter) of quartz and K-feldspar, and fine grains (4–11 μm in diameter) of quartz and polymineral were extracted from the upper and lower parts of the cores for multi-grain measurements of quartz OSL, and of feldspar infrared-stimulated luminescence (IRSL) at 50 °C (IR50) and post-IR IRSL at 175 °C (pIRIR175) to determine burial ages. In addition, facies analysis and radiocarbon dating were conducted. The landward core consists of transgressive to early regressive estuarine and prodelta facies, which is overlain by a sandy beach-shoreface facies. The seaward core consists of a relatively simple shallowing-upward succession from muddy prodelta facies to sandy beach-shoreface facies. All luminescence ages except for pIRIR175 of fine grains are mostly consistent with the radiocarbon ages. Instead, pIRIR175 ages of fine grains are significantly overestimated with variable offsets. OSL and IR50 of fine grains provide reasonable age estimates, as these grains were likely well bleached during the transport even along a short and steep mountainous river. Consistent age estimates of all signals from sand indicate that sand was well-bleached in the beach and shoreface owing to the frequent sediment reworking by waves and currents. These results support the hypothesis that luminescence dating is applicable to Holocene wave-dominated deltas and reiterate that comparing different luminescence signals is an effective way to check reliability of the age estimates in environments where the sunlight bleaching is not ensured. 相似文献
3.
The paleogeography of Amazonia lowlands during the Pleistocene remains hampered by the lack of reliable absolute ages to constrain sediment deposition in the hundred thousand to few million years timescales. Optically stimulated luminescence (OSL) dating applied to quartz has provided important chronological control for late Quaternary sediments, but the method is limited to the last ∼150 ka. In order to extend the age range of luminescence dating, new signals from quartz have been investigated. This study tested the application of isothermal thermoluminescence (ITL) and thermally transferred optically stimulated luminescence (TT-OSL) signals of quartz for dating of fluvial terraces from eastern Amazonia. ITL and TT-OSL signals measured in a modern fluvial sediment sample have shown small residual doses (4 and 16 Gy), suggesting adequate bleached sediments for the target dose range (>150 Gy). This sample responded well to dose recovery test, which showed that the ITL and TT-OSL signals grow to higher doses compared to the doses estimated by the conventional OSL signal. The ITL signal saturated for doses significantly lower than doses reported in the literature. Most dating samples were beyond the ITL saturation doses and only TT-OSL signals were suitable to estimate equivalent doses. Burial ages ranging from 107 to 340 ka were estimated for the fluvial terraces in the lower Xingu River. The main ages uncertainties are related to dose rate changes through time. Despite the uncertainties, these ages should indicate a higher channel base level during the Middle Pleistocene followed by channel incision, possibly due to episodes of increased precipitation in the Xingu watershed. 相似文献
4.
A comparative study using quartz optically stimulated luminescence (OSL) and feldspar post-infrared infrared stimulated luminescence (post-IR IRSL) was undertaken on Quaternary fluvial sediments from an unnamed tributary of the Moopetsi River in South Africa. The aim is to assess whether the post-IR IRSL signal can be used to date incompletely bleached sediments. Several post-IR IRSL signals using varying stimulation and preheat temperatures were investigated; of these the post-IR IRSL225 signal was deemed most appropriate for dating because it bleached most rapidly. The feldspar post-IR IRSL225 equivalent dose (De) values from this site are consistently larger than those from quartz OSL, probably due to differences in the bleaching characteristics of the two signals. Additionally, the post-IR IRSL225 De values within a sample showed less variation in precision than the quartz De data, possibly due to greater averaging between grains in the feldspar small aliquots. The agreement between ages based on the OSL and post-IR IRSL225 signals was better for younger samples (<20 ka) than for older ones (>50 ka); the cause of this variation is unclear. 相似文献
5.
Xiao Fu Jia-Fu Zhang Duo-Wen Mo Chen-Xi Shi Hui Liu Yi-Yin Li Li-Ping Zhou 《Quaternary Geochronology》2010,5(2-3):353-359
The Qujialing site is a representative Neolithic archaeological site in the middle reaches of the Yangtze River, China. Absence of suitable material for radiocarbon dating in this region makes the timing of the similar sites difficult. Here we applied optically stimulated luminescence (OSL–SAR) and thermoluminescence (TL–SAR) techniques to date the archaeological and natural deposits from the Qujialing site with known age, testing the techniques on samples at archaeological sites in this region. The results showed that the luminescence properties of quartz from sediment and baked earth samples are very similar. The quartz OSL ages obtained for a sediment sample and a baked earth sample from the cultural layer are 5.4 ± 0.3 and 5.1 ± 0.3 ka, respectively. The quartz TL age of the baked earth sample is 5.6 ± 0.5 ka. These dates are consistent with the calibrated radiocarbon ages (4.9 ± 0.1 and 5.1 ± 0.1 ka cal BP (±1σ)) of the two charcoal samples from the cultural layer at a nearby locality, and are also in agreement with the age of Qujialing culture period. The results indicate that the OSL dating techniques can be applied to date similar archaeological sites in the middle reaches of the Yangtze River, China. 相似文献
6.
The Wulanmulun site found in 2010 is an important Paleolithic site in Ordos (China), from which lots of stone and bone artifacts and mammalian fossils have been recovered. It was previously dated by radiocarbon and optically stimulated luminescence (OSL) techniques on quartz. To further confirm the reliability of the chronology constructed based on OSL ages and test the applicability of the recently developed pIRIR procedure on sediments from northern China, twenty-four sediment samples (including eolian, lacustrine and fluvio-eolian sands) from the site were determined using the multi-elevated-temperature post-IR IRSL (MET-pIRIR or pIRIR) procedure on potassium feldspar. The results show that the studied samples have two MET-pIRIR De preheat plateaus (280–320 and 340–360 °C), and the bleaching rates of the luminescence signals are associated with sample ages and stimulation temperatures. All the pIRIR ages (7–155 ka) corrected for anomalous fading and residual dose obtained after solar bleaching for 15 h are larger than the corresponding quartz OSL ages (4–66 ka) previously determined, even for the young eolian samples (<10 ka). But the corrected IRSL(50 °C) ages (6–85 ka) are broadly consistent with the quartz ages. It appears that the IRSL(50 °C) ages are more reliable, although this contradicts the previously results obtained by other people. On the other hand, we also obtained an extended age plateau between the stimulation temperatures of 50 and 290 °C in the plot of age versus stimulation temperature (A-T plot) by subtracting different residual doses obtained after different bleaching times. The reliability of the plateau ages requires further investigation. For the sediment samples from this site, quartz should be more suitable for dating than K-feldspar, and the quartz OSL ages of 50–65 ka for its cultural layer should be reliable. 相似文献
7.
River terraces represent important records of landscape response to e.g. base-level change and tectonic movement. Both these driving forces are important in the southern Iberian Peninsula. In this study, Optically Stimulated Luminescence (OSL) dating was used to date two principal river terraces in the Tabernas Basin, SE Spain. A total of 23 samples was collected from the fluvial terraces for dating using quartz OSL. Sixteen of the samples could not be dated because of low saturation levels (e.g. typical 2xD0 < 50 Gy). The remaining seven samples (5 fossil and 2 modern analogues) were investigated using both multi-grain and single-grain analysis. Single grain results show that: (i) measurements from multi-grain aliquots overestimate ages by up to ∼ 4 ka for modern analogues and young samples (<5 ka), presumably because (ii) the presence of many saturated grains has biased the multi-grain results to older ages. Despite the unfavourable luminescence characteristics we are able to present the first numerical ages for two terrace aggradation stages in the Tabernas Basin, one at ∼16 ka and the other within the last 2 ka. 相似文献
8.
Optically stimulated luminescence (OSL) dating was performed on Late Quaternary deltaic sequences from a 55-m-long core sampled from the Nakdong River estuary, Korea. OSL ages obtained from chemically separated fine (4–11 μm) and coarse (90–212 μm) quartz grains ranged from 29.4 ± 2.6 to 0.4 ± 0.04 ka, revealing clear consistency between the grain-size fractions. The De values from the standardized growth curve (SGC) are consistent with those from the single-aliquot regenerative-dose (SAR) procedure, which suggests that the SGC is valid for the Nakdong deltaic sediments. The 14C ages of shells and wood fragments ranged from 11 to 2.9 ka, demonstrating reasonable agreement with the OSL ages, within the error range. However, the limited number and random sampling interval of the 14C age data (10 ages) result in a simple linear and exponential trend in the depth–age curve. In contrast, OSL ages obtained by high-resolution sampling show down-section variations in the depth–age curve, indicating the occurrence of rapid changes in sedimentation rate. It is suggested that the high-sampling-resolution OSL ages provide a more realistic and detailed depth–age curve and sedimentation rate. The Nakdong deltaic sediments were divided into five units based on sedimentation rate. The lowest (unit 5) shows a break in sedimentation between the last glacial maximum (LGM) and the Holocene. The sedimentation rate increased in units 4 and 3, presumably corresponding to the early to middle Holocene sea level rise and high stand. Unit 2 shows a gradually decreasing sedimentation rate following the regression of the shoreline, until about 2 ka. The progradation of the Nakdong River delta resulted in the rapid accumulation of unit 1 during the last 2000 years. 相似文献
9.
The prehistoric site of Ifri n'Ammar is situated in northeastern Morocco, in the northern prolongation of the Middle Atlas Mountains. It is a key location in unravelling the history of anatomically modern humans (AMH) in northern Africa as it reveals Middle and Late Palaeolithic occupation phases since ∼170 ka. Whilst the archaeological sequence within the rock shelter has been well studied, the timing of landscape dynamics around Ifri n'Ammar is still poorly understood. This study therefore aims to establish a detailed chronology of the Wadi Selloum profile at the apron of the shelter, based on optically stimulated luminescence (OSL) dating of ephemeral stream deposits. Coarse-grain quartz was used for single-grain and multiple-grain dating procedures to investigate the luminescence properties of these deposits and to get more accurate age information concerning the phases of human occupation. Continuous wave OSL (CW-OSL) revealed a dominant fast component for all quartz samples. The dose distribution of the uppermost samples showed overdispersion values >25% and significant positive skewness. We identified partial bleaching as the main source of scatter in the equivalent dose (De) distribution. The lowermost sample appeared to be close to signal saturation. The shapes of the dose response curve varied widely between aliquots and coarse quartz grains exhibited therefore very different dose saturation behaviours among aliquots. With fully saturated dose response curves (DRCs), meaningful D0 values were assumed for De estimation.The eight OSL samples yielded stratigraphically consistent ages ranging from 1.3 ± 0.2 ka to 76 ± 5 ka, thus reaching the Middle Palaeolithic period. Moreover, a pottery shard dated to 7.4 ± 0.6 ka (Early Neolithic period) by thermoluminescence (TL), perfectly matched the Holocene OSL samples extracted at the same depth of the profile. In summary, our results point to fluvial aggradation during OIS 5.1, the late glacial period, and the Holocene. 相似文献
10.
M. Demuro R.G. Roberts D.G. Froese L.J. Arnold F. Brock C.Bronk Ramsey 《Quaternary Geochronology》2008,3(4):346-364
Optically stimulated luminescence (OSL) dating of perennially frozen loess was tested on quartz grains extracted from deposits associated with the late Pleistocene Dawson tephra in western Yukon Territory, Canada. OSL samples were obtained from ice-rich loess bracketing the Dawson tephra, while radiocarbon (14C) samples were collected from the bulk sediments directly underlying the tephra and from a ground-squirrel burrow 2.7 m below the tephra. Here we report the OSL characteristics and ages of the extracted quartz grains, as well as additional radiocarbon ages for samples described in Froese [2002. Age and significance of the late Pleistocene Dawson tephra in eastern Beringia. Quaternary Science Reviews 21, 2137–2142; 2006. Seasonality of the late Pleistocene Dawson tephra and exceptional preservation of a buried riparian surface in central Yukon Territory, Canada. Quaternary Science Reviews 25, 1542–1551]. We refine the time of Dawson tephra deposition to between 25,420±70 and 25,290±80 14C a BP. Bayesian analysis of constraining radiocarbon ages places the deposition of the Dawson tephra at between 30,433 and 30,032 cal a BP. Linear modulation (LM) OSL analysis of multi-grain aliquots of quartz showed that the initial part of the decay curve is dominated by a rapidly bleached (‘fast’) component; these samples, however, had relatively dim continuous wave (CW) OSL signals at the multi-grain aliquot (each composed of 80 grains) and single-grain scales of analysis. The single-aliquot regenerative-dose protocol was applied to multi-grain aliquots and single grains to obtain equivalent dose (De) values for samples collected from below and above the Dawson tephra. The De values were examined graphically and numerically, the latter using the central age, minimum age, and finite mixture models. For multi-grain aliquots, the central age model gave weighted mean De values between 30 and 50 Gy, which greatly underestimated the expected De of 74–81 Gy for both samples studied. Possible reasons for these underestimations are discussed, and a solution proposed based on single-grain analysis. Measurements of single grains produced De values in agreement with the expected De, and yielded OSL ages of 28±5 and 30±4 ka for the samples taken from above and below the Dawson tephra, respectively. Examination of individual grains with differing luminescence behaviors showed that a significant number of the measured quartz grains exhibited anomalous luminescence properties that would have compromised the results obtained from multi-grain aliquots. We therefore recommend analysis of individual grains to overcome the age-shortfall from multi-grain analysis of these and similar samples of quartz. 相似文献
11.
Optical dating of a hyperconcentrated flow deposit on a Yellow River terrace in Hukou,Shaanxi, China
Jia-Fu Zhang Wei-Li Qiu Xiao-Qing Wang Gang Hu Rong-Quan Li Li-Ping Zhou 《Quaternary Geochronology》2010,5(2-3):194-199
A sand layer, interpreted as a hyperconcentrated flow deposit, was found interbedded between loess on a Yellow River terrace in Hukou, Shaanxi, China. The site is known as the Longwangchan Palaeolithic site. The deposits from the terrace were dated using optically stimulated luminescence (OSL). Two samples from the sand layer were dated to 30 ± 2 and 33 ± 3 ka using coarse-grained (CG) quartz, and to 82 ± 7 and 94 ± 5 ka using fine-grained (FG) quartz, respectively. The CG quartz OSL ages are believed to be reliable on the basis of the OSL ages of the bracketing loess samples. The overestimation of the FG quartz OSL ages of the sand samples is explained in terms of hyperconcentrated flow processes during sediment transport and deposition. The large difference between the CG and FG quartz OSL ages of the sand samples helps to better understand the formation of the hyperconcentrated flow deposit. The hyperconcentrated flow deposit in this study indicates an extreme river flood occurring at ～30 ka in this area. In addition, the stone artifacts found in the lower loess layer overlying the bedrock of the terrace were dated to ～47 ka. 相似文献
12.
Coastal plain of Hangzhou Bay, to the south of the present Yangtze Estuary, is closely linked to the evolution of the Yangtze River delta. However, absolute age of Pre-Holocene sediments is limited, which hinders the understanding of this area's environmental evolution. In this study, using optically stimulated luminescence (OSL), single aliquots and single grains of quartz and K-feldspar were used to date the late Quaternary sediments in coastal plain on the southern Hangzhou Bay. The vertical difference in particle size composition render either silt- or sand-sized quartz for dating. Cross-checking of multiple OSL dating methods indicated that the upper ∼65 m recorded the Holocene part of the succession; sediment from a depth of 136.6 m was dated to ∼180 ka. It was found that the single-grain method was more reliable in comparison to single-aliquot age, the former minimized the effect of signal components. Single-grain quartz and K-feldspar luminescence yielded consistent ages at sample depth of 136.6 m (∼160–180 ka), while the latter gave robust age at depth of 115.5 m (∼150 ka). This chronology is in general in accordance with neighbouring cores and can constrain paleomagnetic dating results in those cores. Taking together, the study site has thickest Holocene deposits in comparison to the highland centered around Taihu Lake on the southern Yangtze delta. Moreover, the luminescence characteristics of quartz from different sample depths, behaved differently with respect to luminescence sensitivity, signal components and saturation level, perhaps reflecting varied provenance and weathering characteristics caused by climate change. 相似文献
13.
Quartz optically stimulated luminescence (OSL) dating has been applied to sandy beach ridge systems from the Magdalen Islands in the center of the Gulf of St. Lawrence (Quebec, Canada) to provide the first chronological framework for these features. Nineteen beach ridges (22 samples) from four different sites throughout the archipelago were investigated. At one of the sites, samples were taken at 9 m and 7.5 m depth using a vibracore. The quartz is dominated by the fast OSL component and a single-aliquot regenerative-dose (SAR) protocol was used to measure the equivalent doses; a low preheat (180°C/10 s) was chosen to avoid the influence of thermal transfer. The average dose recovery ratio of all samples is 1.02 ± 0.02 (n = 130) suggesting that the SAR protocol works satisfactorily on this material. The OSL ages are internally consistent and supported by independent age control (radiocarbon). The OSL ages indicate that the ridges were built between 2.6 ± 0.2 ka and 0.40 ± 0.10 ka, i.e. during a period of sea level rise. This rise eroded adjacent sandstone cliffs, which contributed a significant sediment supply to the littoral drift and beaches. Some low-lying coasts in the archipelago are still prograding, despite a relative sea level increase of ∼1.6 mm/a over the last 600 years. The late Holocene ages obtained in this study indicate that these processes have been active for at least the past two thousand years. This study demonstrates for the first time that OSL dating using quartz has great potential in this area, and is an appropriate method for establishing precise chronologies for coastal sediments in this region of the Gulf of St. Lawrence. 相似文献
14.
Testing the application of quartz and feldspar luminescence dating to MIS 5 Japanese marine deposits
The applicability of both quartz and feldspar luminescence dating was tested on twenty-five samples from a marine succession now forming a coastal cliff at Oga Peninsula, Honshu Island, Japan. The quartz optically stimulated luminescence (OSL) signal shows thermal instability and linear modulated (LM)-OSL analysis revealed the dominance of a slow component. When compared with independent age control provided by two marker tephras, the quartz OSL ages grossly underestimate the depositional age. In contrast, potassium (K)-rich feldspar is a suitable dosimeter when measured using post-IR infrared stimulated luminescence (IRSL) at 225 °C (pIRIR225). Scanning electron microscope (SEM) analyses on the feldspar extracts revealed that the grains are amorphous with small crystalline inclusions; using standard internal dose rate parameters, this would result in a too large dose rate. Dose rates were calculated using the observed grain size of 40 ± 20 μm with an assumed K concentration of 12.5 ± 0.5%. The fading corrected pIRIR225 ages agree well with independent age control, and the sediments of the Katanishi Formation were deposited between 82 ± 6 and 170 ± 16 ka. This study demonstrates that pIRIR dating of feldspar is a powerful chronological tool for the dating of sediments of volcanic origin. 相似文献
15.
Geochemically-fingerprinted tephra beds provide unique chronostratigraphic markers for comparing Quaternary sedimentary records across eastern Beringia (Alaska and Yukon Territory). Establishing reliable numerical age control on these tephra horizons enables them to be placed within firm temporal frameworks and increases their potential as correlative tools for regional palaeoenvironmental reconstructions. To this end we present new single-grain and multi-grain quartz optically stimulated luminescence (OSL) chronologies for loess deposits bracketing three well-documented and regionally significant variants of the Sheep Creek tephra (SCt) at two sites in west-central Yukon Territory (Ash Bend and Quartz Creek). Single-grain OSL ages bracketing the SCt-A and SCt-K reveal that these tephras were deposited during late Marine Isotope Stage (MIS) 5 or early MIS 4. The SCt-C variant and associated organic-rich bed at Ash Bend were likely deposited during late MIS 5, based on a single-grain OSL age of ∼81 ka for the overlying sediments. The single-grain OSL ages obtained for these deposits are in stratigraphic order and in broad agreement with a fission track age estimate of ∼77 ka for the SCt-K. In contrast, comparative chronologies obtained using multi-grain aliquots are stratigraphically inconsistent and unexpectedly young when compared with the independent SCt-K age. Detailed examination of the single-grain OSL datasets reveal a range of unfavourable luminescent properties that could have contributed to the multi-grain aliquot age discrepancies; including, very low yields of luminescent grains, weak OSL signal sensitivities and large populations of aberrant grains (particularly 0 Gy grains and ‘dim’ grains with a tendency to sensitise during the equivalent dose (De) measurement sequence) that have similarly sized OSL signals as grains used for De analysis. Synthetic aliquot De datasets constructed from single-grain OSL measurements reveal that the large proportional light sum contributions of 0 Gy and dim grains could possibly account for multi-grain age underestimations in some of the Ash Bend samples. In light of these potentially problematic averaging effects, we do not consider the multi-grain OSL ages to be reliable and suggest that single-grain approaches may be preferable for dating sediments with similar quartz luminescence behaviours across this region. 相似文献
16.
Holocene flood events in the Yangtze River are associated with variations in East Asian Summer Monsoon (EASM) precipitation, and so Yangtze delta sediments may preserve information about the frequency and magnitude of EASM precipitation. These flood/drought cycles of the EASM directly affect the living standards of East Asian population. However, despite its importance, little chronological control is available for the Yangtze Delta sediments; because biogenic carbonate only occurs sporadically, it has proved the difficulty to discuss sedimentation mechanisms and rates in any detail.In 2013 two sediment cores (YD13-G3 and H1) were taken from the Yangtze subaqueous delta to investigate precipitation history. In this study, we investigate the potential of quartz OSL dating of the fine silt fraction (fine-grained quartz; 4–11 μm) from these cores to estimate the depositional age of the sediments. We test whether: (1) Yangtze subaqueous delta sediments contain quartz with suitable characteristics for dating, and (2) quartz grains are well-bleached during/before the transportation process, by examining a modern analogue of suspended particulate matter, and by cross-checking with the doses derived from infrared stimulated luminescence (IRSL) signals (both IR50 and pIRIR160) from feldspar in polymineral fine grains. We find that both the quartz and feldspar luminescence characteristics are satisfactory (quartz dose recovery ratio 1.067 ± 0.004; n = 250, pIRIR160 dose recovery ratio 1.01 ± 0.02; n = 151). Modern suspended particulate matter has measured quartz equivalent doses between 0.1 and 0.2 Gy, suggesting that this material was sufficiently bleached during/before transportation to allow dating of Holocene sediments (mean dose rates of ∼3 Gy ka−1). OSL ages of 44 samples from the 2 cores show apparently rapid accumulation at ∼6 ka between 9.65 and 5.50 m in core H1 and ∼2 ka throughout core G3 and between 5.0 and 0.0 m in core H1. The pIRIR160 signals suggest less light exposure of the core top sediments and of those from the transition layer between ∼6 ka to ∼2 ka, although there is no evidence for incomplete bleaching of quartz. The question remains as to whether significant deposition took place only at these two times, or whether the record has been disturbed by erosion/reworking. 相似文献
17.
Reliable chronology is critical for reconstructing estuarine delta process. In this study, detailed chronological framework has been performed on a core HPQK01 (52 m in depth) from the central Pearl River delta (PRD) of China. Both quartz OSL and feldspar post-IR IRSL (pIRIR) methods for late Pleistocene sediments, as well as radiocarbon dating for Holocene sediments, were applied to date the core. Results show that quartz OSL ages range from 125 ± 18 ka to 58 ± 6 ka, and that all of them were minimum ages due to the OSL signal saturation. Feldspar pIR200IR290 protocol shows some overestimation in dose recovery test, with the recovered to the given ratio of 1.2, while a ratio of around 1 was obtained for feldspar pIR50IR250 signals. Robust ages have been obtained from feldspar fading corrected pIR50IR250 dating with ages ranging from 150 ± 17 ka to 98 ± 12 ka. AMS 14C results suggest that subtidal-intertidal zone was deposited during the middle Holocene from 8.21 ± 0.19 cal ka BP to 4.99 ± 0.25 cal ka BP. The sedimentology of core HPQK01 record two marine transgressive-regressive cycles. Based on the dating results, the lower fluvial sediment unit (T2) could be correlated to marine isotope stage (MIS) 6, and the lower marine unit (M2) was deposited during MIS 5. A sedimentary hiatus occurred with age range of from MIS 4 to MIS 2. Since middle Holocene, another marine stratum (M1) has been accumulated. Overall, our findings suggest that feldspar pIRIR dating method has the potential to establish the Quaternary chronostratigraphic framework of the PRD for samples with ages within 150 ka. 相似文献
18.
Dust depositions are critical archives for understanding interior aridification and westerly climatic changes in Central Asia. Accurate and reliable dating of loess is very important for interpreting and correlating environmental records. There remains a disparity between luminescence ages and radiocarbon dating of late Quaternary loess from the Ili Basin in Central Asia. In this study, we establish a closely spaced quartz optically stimulated luminescence (OSL) chronology for the 20.5-m-thick Nilka loess section in the Ili Basin. Based on OSL ages, two intervals of higher mass accumulation rate occurred at 49–43 ka and 24–14 ka. We further compare these OSL ages with 23 accelerator mass spectrometry (AMS) 14C ages of bulk organic matter. The results indicate that the OSL and radiocarbon ages agree well for ages younger than ca. 25 14C cal ka BP. However, beyond 30 cal ka BP, there is no consistent increase in AMS 14C age with depth, while the OSL ages continue to increase. These differences confirm the observation that the AMS 14C ages obtained using conventional acid–base–acid (ABA) pretreatment are severely underestimated in other terrestrial deposits in Central Asia, which could be due to 2–4% modern carbon contamination. However, OSL dating is applicable for constructing an accurate chronology beyond 30 cal ka BP. We suggest caution when interpreting paleoenvironmental changes based on radiocarbon ages older than 25 cal ka BP. 相似文献
19.
The loess deposits surrounding the high mountainous regions of Central Asia play an important role in understanding environmental changes in Eurasia on orbital and sub-orbital timescales. However, problems with dating Central Asian loess have limited the interpretation of climatic and environmental data, especially on sub-orbital timescales. We selected a controversial loess section, Zeketai (ZKT, with a thickness of 23 m), in the Yili basin in Xinjiang Province in western China, to establish a detailed and systematic Optically Stimulated Luminescence (OSL) chronology. Quartz grains of 38–63 μm were isolated from 15 samples and the single-aliquot regenerative-dose (SAR) protocol was employed for De determination. OSL ages are in stratigraphic order and range from 13.8 ± 1 to 72 ± 6 ka, suggesting continuous loess accumulation during the last glaciation. We compared these dating results with that of the previously published fine-grain sized quartz (4–11 μm) using simplified multiple aliquot regenerative-dose (SMAR) protocol, and with the previous published radiocarbon dating (14C) ages on snail shells. With the exception of three young samples from the upper 6 m of the section, the SMAR dating results are basically consistent with the results using the SAR protocol. Both the SMAR and SAR OSL ages are consistently older than the 14C ages, and the radiocarbon date results should be used with caution since they appear to have been underestimated. 相似文献
20.
When electron spin resonance (ESR) is applied to sedimentary quartz, dealing with the poor bleachability of the signals is particularly challenging. In this study, we used both the single-grain optically stimulated luminescence (OSL) and the single aliquot ESR dating of quartz from deep sand deposits preserving a Stone Age archaeological sequence to combine the advantages of the two methods: good bleaching behaviour and extended age range. Using the youngest samples at each sampling site we were able to calculate the mean ESR residual age from the difference between the OSL ages and the apparent ESR ages. Focusing mainly on the single aliquot regenerative dose (SAR) protocol here, we were able to calculate the mean ESR residual age for the Ti and Al centres, including the non-bleachable signal component for the latter. For the NP site, residual ages of 209 ± 13 ka and 695 ± 23 ka were calculated for the two centres, whereas for the ZS site 268 ± 39 ka and 742 ± 118 ka were determined. These residual ages are significant and cannot be neglected. Thus, the residual age was subtracted from the apparent ESR ages. The validity of the residual subtraction method was tested through a comparison of the oldest OSL age from each site with the residual subtracted ESR age. For both NP and ZS sites, the residual subtracted Ti and Al ages were consistent with the OSL age within 2-σ uncertainty, and therefore confirm the robustness of the subtraction method. Within the NP sequence, we were able to locate the end of the Early Stone Age at 590 ± 86 ka, and this provides a maximum age for the transition to the Middle Stone Age in this part of south-central Africa. 相似文献