共查询到20条相似文献，搜索用时 46 毫秒
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采用HCl-HNO3-HF-HCl O4,HCl-HNO3-HF-H2SO4敞口,HCl-HNO3-HF-HCl O4密闭和HNO3-HF密闭消解4种方法溶矿,利用电感耦合等离子体发射光谱(ICP-AES)测定,建立了超基性岩石中钾、钠、钙、铝、铁、钛、锰、钴、镍、铬、钒、锶、锌等元素的同时测定方法。对电感耦合等离子体发射光谱仪测定的最佳仪器条件及分析谱线进行了选择,并对镁基体的影响进行了研究,采取标准溶液中加入适量的镁作基体匹配,以消除基体影响。实验结果表明:采用HNO3-HF密闭溶矿,具有检出限低、灵敏度高,操作简便、快速等突出优点。该方法测定值与推荐值基本吻合,分析方法的精密度满足《地质矿产实验室测试质量管理规范》的要求。 相似文献
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采用氢氟酸-盐酸-硝酸-硫酸四酸溶矿,建立了电感耦合等离子体发射光谱仪法(ICP-AES)同时测定钒钛磁铁矿、钛铁矿中铝、钙、镁、钾、钠、锰、钛、铬、锶、锌和钒11种元素的方法。对最佳仪器条件及分析谱线进行了优化筛选,并探讨了4种消解方法及酸度对测定的影响。实验结果表明:ICP-AES法测定钒钛磁铁矿、钛铁矿中铝、钙、镁、钾、钠等元素,与原子吸收光谱法、分光光度法、滴定法、重量法等单一元素测定方法相比较,具有检出限低、灵敏度高、测量范围宽、操作简便,适合大批量样品测定等突出优点。方法准确度(RE)小于10%,元素精密度(RSD,n=12)为0.68%~5%。采用国家一级标准物质进行了方法验证,取得了令人满意的结果。 相似文献
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一、在地质领域中的应用
20世纪60年代,火焰原子吸收光谱法已应用到各种岩石样品中的钙、镁、钾、钠、铁、铜、锰、锌、钴、镍以及金、银等元素的测定。由于该方法的高特效性和抗干扰性,即使对痕量元素的分析,也无需进行主要成分的分离,因此,很快为地球化学实验室所接受, 相似文献
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正尊敬的人类朋友,我是最近几年涌现的颇受人类朋友喜爱的宝石新宠,我叫电气石,是电气石族矿物的总称,是以含硼为特征的铝、钠、铁、镁、锂、锰的环状结构硅酸盐矿物,分子式为NaR_5Al_6B_3Si_6O_(27)(OH)_4,R为Mg、Mn、Fe、Li、Al。以Fe~(2+)为主的称黑电气石,亦称铁电气石;以镁为主的称褐色镁电气石,呈玫红色、红色、蓝绿色、黄色和无色;以铝、锂为主的称锂电气石;以锰为主的称钠锰电气石。我(电气石) 相似文献
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流动注射—试钛灵分光光度法测定岩石中全铁和钛,是在原有方法的基础上,引进了流动注射技术,从而提高了样品的分析速度、准确度、精密度,并使样品测试的线性范围有了明显的改善。本方法快速、灵敏、简便、可靠,每小时提供110个测试数据,其铁、钛的相对标准偏差分别为0.82％和2.87％。 相似文献
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杨钟堂 《地球科学与环境学报》1981,(1)
本文从应力矿物的变形现象;构造岩岩石类型;破碎矿物颗粒的粒径变异;构造岩化学元素的迁移变化和构造岩胶结物及胶结类型的变化等几方面讨论了在宏观上表现为正断层的陕西临潼牡丹沟北北东向断裂带的构造岩石学特征,从而确定了该断裂为一以扭为主的压扭性力学性质的破裂结构面,是快速应力作用的结果,其影响宽度可达三十米,断裂化学元素迁移能力顺序为钾、钠、铝、钙、镁、钛、铁、硅。 相似文献
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采用HClHNO3HF HClO4,HClHNO3HF H2SO4敞口和HClHNO3HFHClO4,HClHNO3HF H2SO4微波消解4种方法溶矿,利用电感耦合等离子体发射光谱（ICPAES）测定,建立了钛铁矿中钾、钠、钙、镁、钡、锶、锌等元素的同时测定方法。对电感耦合等离子体发射光谱仪测定的最佳仪器条件及分析谱线进行了选择,并对钛、铁基体的影响、溶矿提取酸度以及溶矿残渣进行了研究。实验结果表明：采用HClHNO3HF HClO4敞口溶矿,具有检出限低、灵敏度高,操作简便、快速等突出优点。该方法测定值与推荐值基本吻合,分析方法的精密度满足《地质矿产实验室测试质量管理规范》的要求。 相似文献
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The ability of cell to modulate the fluidity of plasma membrane was crucial to the survival of microorganism at low temperature. Plasma membrane proteins, fatty acids and carotenoids profiles of Antarctic psychrophilc yeast Rhodotorula sp. NJ298 were investigated at -3 ℃, 0 ℃ and 8 ℃. The results showed that plasma membrane protein content was greater at -3 ℃ than that at 8 ℃, and a unique membrane polypeptide composition with an apparent molecular mass of 94.7 kDa was newly synthesized with SDS-PAGE analysis; GC analysis showed that the main changes of fatty acids were the percentage of unsaturated fatty acids (C18∶ 1 and C18∶ 2) and shorter chain saturated fatty acid (C10∶ 0) increased along with the decrease of the culture temperature from 8 ℃ to -3 ℃; HPLC analysis indicated that astaxanthin was the major functional carotenoids of the plasma membrane, percentage of which increased from 54.6±1.5% at 8 ℃ to 81.9±2.1% at -3 ℃. However the fluidity of plasma membrane which was determined by measuring fluorescence anisotropy was similar at -3 ℃, 0 ℃ and 8 ℃. Hence these changes in plasma membrane's characteristics were involved in the cellular cold-adaptation by which NJ298 could maintain normal plasma membrane fluidity at near-freezing temperature. 相似文献
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《极地研究(英文版)》2014,(4)
正1 Aims and Scope Advances in Polar Science(APS)is an international,peer-reviewed journal jointly sponsored by the Polar Research Institute of China and the Chinese Arctic and Antarctic Administration.APS is a comprehensive academic journal dedicated to presentation of multi-disciplinary achievements in Arctic and Antarctic expeditions and research.Its primary purpose 相似文献
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《中国海洋大学学报(英文版)》2014,(4)
<正>Copyright Submfnion of a roanusatpt inks:that the work described has not been published before(exoept In the form of an abstrW or as part of a published lecture,review,or thesis);that it is not under consideration for publication elsewhere that its publication has been approved by ail 相似文献
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《中国海洋大学学报(英文版)》2014,(6)
<正>The Journal of Ocean University of China(Oceanic and Coastal Sea Research)is a comprehensive academic quarterly sponsored by the Ocean University of China,published one volume per year.This journal is devoted to the publication of the theoretical and applied research results on oceanography and marine fisheries.The fieldcovered include the physical,chemical,biological,geo- 相似文献
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Massimo GRECO 《山地科学学报》2014,(6):1383-1384
<正>The 35th IAHR World Congress was held in Chengdu,China from September 8 to September 132013.The title of the conference was:"The Wise Finds Pleasure in Water:Meandering through Water Science and Engineering".During the congress,1239 papers were presented in 139sessions for oral presentations and 7 sessions for poster presentations.After the Congress,a Committee was appointed to select some of the best papers presented at the Congress for publication,after a 相似文献
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As an important component of the cryosphere,sea ice is very sensitive to the climate change.The study of the sea ice physics needs accurate sea ice thickness.This paper presents an electromagnetic-induction(EM) technique which can be used to measure the sea ice thickness distribution efficiently,and the successful application in Bothnian Bay.Based on the electromagnetic field theory and the electrical properties of sea ice and seawater,EM technique can detect the distance between the instrument and the ice/water interface accurately,than the sea ice thickness is obtained.Contrastive analysis of the apparent conductivity data obtained by EM and the value of drill-hole at same positions allows a construction of a transformable formula of the apparent conductivity to sea ice thickness.The verification of the sea ice thickness calculated by this formula indicates that EM technique is able to get reliable sea ice thickness with average relative error of only 12%.The statistic of all ice thickness profiles shows that the level ice distribution in Bothnian Bay was 0.4-0.6 m. 相似文献
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Based on the hydrographic data in austral summer during the 22nd Antarctic Expedition of China(2005/2006),some features can be found about the northern margin of Emery ice shelf as follows.The heat content in the surface layer(0-50 m) at the eastern end and the western end of the ice-shelf margin is much higher than that at the middle.The upper mixing-layer depth and the seasonal thermocline depth at the middle of the ice-shelf northern margin are much shallower than those at the both ends.However there is much less difference between the middle and the ends in the bottom layer.The remote sensing photos show that the inhomogeneity in the surface-layer water is closely related to the spatial distribution of the floes and polynia in the area. 相似文献
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Phylogenetic analysis based on 16S rDNA of 8 strains of cultivable bacteria isolated from Arctic sea-ice was studied.The results showed that strain BJ1 belonged to genus Planococcus,which was a genus of low mole percent G C gram-positive bacteria;strain BJ6 belonged to genus Burkholderia of β-proteobacteria and the rest 6 strain all belonged to γ-proteobacteria,of which strain BJ8 was a species of Pseudoalteromonas,strain BJ2-BJ5 and BJ7 were members of genus Psychrobacter.Phylogenetic analysis also indicated that bacteria of genus Psychrobacter of the isolates formed a relatively independent phylogenetic cluster in comparison with other bacteria belonged to genus Psychrobacter. 相似文献
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《极地研究(英文版)》2014,(3)
正1 Aims and Scope Advances in Polar Science(APS)is an international,peer-reviewed journal jointly sponsored by the Polar Research Institute of China and the Chinese Arctic and Antarctic Administration.APS is a comprchensive academic journal dedicated to presentation of multi-disciplinary achievements in Arctic and Antarctic expeditions and research.Its primary purpose is to publish achievements in fundamental research,applied 相似文献