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iCAP 6300电感耦合等离子体发射光谱仪的常规维护方法 总被引：1，自引：1，他引：0
电感耦合等离子体发射光谱仪在使用过程中,由于控制气体流量的电磁阀出现机械性移位,致使工作气流量过于偏大或偏小,对进样系统及分析数据产生不利影响;长期频繁使用条件下,由于控制光学系统的机械定位装置的磨损,致使谱峰坐标偏离而影响仪器灵敏度;很长时间不能"引燃"等离子体,检查进样系统和氩气纯度并没有发现异常,需要验证RF发生器有无功率输出时有一定的困难;在等离子体工作时产生的高温尾气的长期作用下,难免造成点火头末端铜丝的锈蚀,致使点火头放电微弱,不能"引燃"等离子体。因此,为保证仪器的正常运行,提高工作效率,确保检测数据的准确度,实验室应建立健全电感耦合等离子体发射光谱仪维护保养方案,解决上述问题。本文结合实际工作经验,以iCAP 6300电感耦合等离子体发射光谱仪为例,提出可以借助"Manufacturing and Service.exe"程序校正工作气流量,验证RF发生器是否输出功率;利用C 193.091 nm谱线为基准校正谱线修正CID检测器的谱峰坐标系统;另外,对点火头、分析软件数据库及主机灰尘的清理也进行了详细的维护说明,这些措施有益于保障仪器的性能及提高设备的利用率。 相似文献
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Diurnal variations of two mountain-plain solenoid （MPS） circulations associated with ＂first-step＂ terrain [Tibetan Plateau （TP）] and ＂second-step＂ terrain （high mountains between the TP and ＂east plains＂） in China and their influence on the south west vortex （SWV） and the mei-yu front vortex （MYFV） were investigated via a semi-idealized mesoscale numerical model [Weather Research and Forecasting （WRF）] simulation integrated with ten-day average fields （mei-yu period of 1-10 July 2007）. The simulations successfully reproduced two MPS circulations related to first and second-step terrain, diurnal vari- ations from the eastern edge of the TP to the Yangtze River-Huaihe River valleys （YHRV）, and two precipitation maximum centers related to the SWV, MYFV. Analyses of the averaged final seven-day simulation showed the different diurnal peaks of precipitation at different regions： from the aftemoon to early evening at the eastern edge of the TP; in the early evening to the next early morning in the Sichuan Basin （SCB）; and in the late evening to the next early morning over the mei-yu front （MYF）. Analyses of individual two-day cases confirmed that the upward branches of the nightlime MPS circulations enhanced the precipitation over the SWV and the MYFV and revealed that the eastward extension of the SWV and its con vection were conducive to triggering the MYFVs. The eastward propagation of a rainfall streak from the eastern edge of the TP to the eastern coastal region was primarily due to a series of convective activities of several systems from west to east, including the MPS between the TP and SCB, the SWV, the MPS between second-step terrain and tile east plains, and the MYFV. 相似文献
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作者组装了电磁阀进样PIA-FAAS仪,并考察了取样体积,载流速度,反应圈长度等因素对分散度的影响。用FIA-FAAS标准加入内插法测定了卤水中的锂,结合MBT-MLBK体系萃取,有机相进样测定了地质样品中的痕量钯。实验结果表明:电磁阀进样FIA—FAAS仪具有结构简单,操作方便,分散度易控制,精密度高,准确度好,分析速度快等优点,有一定的实用性。 相似文献
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