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碳酸铷、硼酸化学计量比混合,蒸发溶液,直至五硼酸铷RbB5O8·4H2O晶体析出。经粉末X射线衍射(XRD)、拉曼光谱(Raman spectroscopy)、热重/微商热重/差示扫描量热(TG/DTG/DSC)、原子吸收光谱等实验方法,确定其化学组成及结构。298.15、333.15K时测量溶液的物理化学性质(密度、电导、pH),并与经验方程进行拟合,研究五硼酸铷溶液的物化性质随浓度、温度的变化规律。根据文献报道的平衡常数,实验测量的pH数据,采用牛顿迭代法进一步研究五硼酸铷溶液中主要存在的硼酸根离子对类型、含量以及物种的形成。 相似文献
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三肇凹陷榆树林油田扶杨油层中泥岩、粉砂岩和砂岩样品主量元素和微量元素地球化学分析表明,多数主量元素含量中等,与全球平均大陆上地壳(UCC)相比,Fe_2O_3、MgO、CaO、Na_2O含量较低,而TiO_2、Al_2O_3、K_2O、MnO含量均略高;样品中的相容元素(V、Cr、Co、Ni等)含量均低于澳大利亚后太古宙页岩(PAAS)和UCC;稀土元素总量为102×10~(-6)~276×10~(-6),平均为188×10~(-6),与PAAS表现出相似的球粒陨石标准化曲线,显示了相似的物源和构造背景。元素间的相关性分析显示大部分元素与SiO_2负相关而与Al_2O_3正相关,说明大部分元素受到黏土矿物吸附作用的影响,石英与长石矿物对这些元素表现出一定的稀释效应。根据主元素物源判别方程图和Th-Hf-Co图投影及La/Hf、(Gd/Yb)N值,扶杨油层物源主要来自后太古宙长英质火山岩,可能卷入了部分再循环沉积岩。通过一系列的构造背景判别图解分析,表明扶杨油层沉积时以大陆岛弧环境为主。在对油层组进行了纵向古气候分析后,认为FI油层组沉积时处于一个构造活动强、干旱的环境中,所形成的沉积岩储层物性更好,是油气勘探开发的重点层位。 相似文献
64.
The black shale series that formed in the Ediacaran–Cambrian transition are important stratigraphic records of the co-evolution of the paleo-ocean, -climate, and -biology. In this study, we measured Re–Os isotopic compositions of the black shale in the Niutitang Formation from the Gezhongwu section in Zhijin, Guizhou Province. The samples had high Re and Os contents, with Re ranging from 21.27 to 312.78 ng/g and Os ranging from 0.455 to 7.789 ng/g. The Re–Os isotope isochron age of 522.9 ± 8.6 Ma implies deposition of the Niutitang black shale predated the Chengjiang Fauna, providing an age constraint for the expansion of oceanic anoxia in the study area. The initial 187Os/188Os ratio of 0.826 ± 0.026 indicates that enhanced continental weathering might have triggered the expansion of the oceanic anoxia. 相似文献
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Yajie Zhang Yao Li Jing Ge Gaopeng Li Zhisheng Yu Haishan Niu 《Environmental Earth Sciences》2018,77(12):462
Drought monitoring is a key topic in environmental monitoring and assessment although there is still a need to determine the correlation between drought monitoring indices and remote sensing products. We analyzed the correlation between the self-calibrating Palmer Drought Severity Index (sc_PDSI), the Standardized Precipitation Index and the Standardized Precipitation Evapotranspiration Index (SPEI) and terrestrial water storage monitored through the Gravity Recovery and Climate Experiment (GRACE) on a monthly timescale from 2002 to 2015 in China. As a consequence of anomalies in the soil water budget, the highly significant correlation between the sc_PDSI and the GRACE satellite-observed terrestrial water storage suggested that these two datasets are the most suitable for use in monitoring droughts. In comparing the three drought indices, the sc_PDSI was introduced as a means of drought monitoring in the Yangtze, Pearl, Huaihe, Southeast and Songhua River Basins, whereas the SPEI was found to be more applicable to other major river basins, such as the Inland River Basin. These diverse spatial behaviors are caused by the differences between the hydrological droughts characterized by these three drought indices. 相似文献
67.
Zizhan Hu Xuguang Tang Chen Zheng Menglin Guan Jingwei Shen 《Environmental Earth Sciences》2018,77(14):540
Due to its negative impact on the living environment of human beings, ambient air pollution has become a global challenge to human health. In this study, surface observations of six criteria air pollutants, including PM2.5, PM10, SO2, NO2, CO and O3, were collected to investigate the spatial and temporal variation in the Beijing–Tianjin–Hebei (BTH) region during 2013–2016 and to explore the relationships between atmospheric pollutants and meteorological variables using quantile regression model (QRM) and multiple linear regression model (MLRM). The results show that BTH region has experienced significant air pollution, and the southern part generally has more severe conditions. The annual average indicates clear decreasing trends of the particulate matters, SO2 and CO concentrations over the last 4 years and slight increasing trends of NO2 and O3 in several cities. The seasonal and monthly characteristics indicate that the concentrations of five species reach their maxima in the winter and their minima in the summer, whereas O3 has the opposite behaviour. Finally, the pseudo R2 values show that the QRMs have the best performance in the winter, followed by spring, fall, and summer. Specifically, all the meteorological factors have significant impacts on air pollution but change with pollutants and seasons. The MLRM results are generally consistent with the QRM results in all seasons, and the inconsistencies are more common in the fall and winter. The results of this research provide foundational knowledge for predicting the response of air quality to climate change in the BTH region. 相似文献
68.
Juanle Wang Eryang Chen Ge Li Lu Zhang Xiaoming Cao Yongjie Zhang Yujie Wang 《Environmental Earth Sciences》2018,77(16):590
Concentrations of suspended solids in lakes can affect the latter’s primary productivity and reflect changes in sediment deposition. Determining the temporal and spatial distribution of suspended solid concentrations has important significance in lake water environmental management; this is particularly urgent for Poyang Lake, the largest freshwater lake in China. In this study, suspended solid concentration inversion models for Poyang Lake were created using a semi-empirical method with regression analysis between continuously measured suspended solid concentration data and multi-band moderate-resolution imaging spectroradiometer images for spring, summer, autumn, and winter from 2009 to 2012. The coefficient of determination (R2) is from 0.6 to 0.9 and the average relative error for the accuracy verification was between 10 and 30%. The seasonal distributions of suspended solid concentrations in Poyang Lake from 2000 to 2013 were then obtained using optimal reversal models. The results showed that the seasonal variation in suspended solid concentrations had a “W” shape in which high spring and autumn and low summer and winter values. The suspended solid concentrations increased annually from 2000 to 2013 and were mainly distributed in the northern and central portions of the lake, with lower values along the shorelines. Further analysis indicated that the large difference in water level between the wet and dry seasons is an important factor in explaining these seasonal variations. Moreover, the suspended solid concentrations were poorly correlated with water temperature and chlorophyll-a concentration but more highly correlated with the deferred chlorophyll-a concentration. 相似文献
69.
为了客观地确定数据点投图后分布的主要区域,本文提出了一种基于数据密度确定数据主要分布区域的方法。利用该方法可以更加直观地了解数据分布,并可以作为数据清洗的预处理手段。本文基于GEOROC大数据,以全碱对硅(TAS)图解为例,进行了分析和验证。通过提取GEOROC 数据库中与TAS 图解相关的岩石样本中SiO2、Na2O、K2O 和烧失量含量数据,通过数据常规清洗和归算,最终获得24 个种类合计13.3 万条有效数据。通过数据投点、分区统计和提取80% 数据的分布区域,验证了24种岩石样品与TAS图解的吻合程度。通过综合研究分析发现,有6类岩石的数据分布与TAS图解定义区域基本一致,18类岩石的数据分布与TAS图解定义区域有系统性偏差。大数据研究证明了TAS图解的不足之处,利用全碱和SiO2作为指标,难以实现提升总体分类的准确性。 相似文献
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