Determination of Chlorine Contents in Geological Survey of Japan Reference Materials by Prompt Gamma Neutron Activation Analysis     

Takashi Sano  Takaaki Fukuoka  Toshiaki Hasenaka 《Geostandards and Geoanalytical Research》2004,28(3):443-448

We determined chlorine contents in nine GSJ (Geological Survey of Japan) reference materials (JB-1, 1a, 2, 3; JA-1, 2, 3; JR-1, 2) by prompt gamma neutron activation analysis, employing the standard addition method. Pressed powder disks of each reference material were used for neutron irradiation and gammaray measurement, after known quantities (25-200 μl) of sodium chloride solution were added. The influence of the nearby sodium peak overlap was checked, and fluctuations in the chlorine count rate were corrected using silicon as an internal standard. The slopes of calibration lines for seven reference materials (JB-1, 2, 3; JA-1, 2, 3; JR-2) and SiO₂ powders fall within 5% error, and their chlorine values were obtained from the intercepts. Chlorine contents in JB-1 a and JR-1 were also determined by using the calibration lines. Our chlorine values ranged from 26.1 to 934 μg g-¹, which agrees well with the previously reported values.  相似文献   

Excess Ar-free phengite in ultrahigh-pressure metamorphic rocks from the Lago di Cignana area, Western Alps     

Chitaro Gouzu  Tetsumaru Itaya  Hironobu Hyodo  Takaaki Matsuda   《Lithos》2006,92(3-4):418-430

Ar/Ar analyses of phengites and paragonites from the ultrahigh-pressure metamorphic rocks (zoisite–clinozoisite schist, garnet–phengite schist and piemontite schist) in the Lago di Cignana area, Western Alps were carried out with a laser probe step-heating method using single crystals and a spot dating method on thin sections. Eight phengite and two paragonite crystals give the plateau ages of 37–42 Ma with 96–100% of ³⁹Ar released. Each rock type also contains mica crystals showing discordant age spectra with age fractions (20–35 Ma) significantly younger than the plateau ages. Phengite inclusions in garnet give ages of 43.2 ± 1.1 Ma and 44.4 ± 1.5 Ma, which are significantly older than the spot age (36.4 ± 1.4 Ma) from the matrix phengites, and the plateau ages from the step-heating analyses. Inclusion ages (43 and 44 Ma) are consistent with a zircon SHRIMP age (44 ± 1 Ma) in this area. These results suggest that the oceanic materials that underwent a simple subduction related UHPM, form excess ⁴⁰Ar-free phengite and that the peak metamorphism is ca. 44 Ma or little older. We suggest that matrix phengites experienced a retrogression reaction changing their chemistry contemporaneously with deformation related to the exhumation of rocks releasing significant radiogenic ⁴⁰Ar from the crystals. This has lead to the apparent ages of the matrix phengites that are significantly younger than the inclusion age.  相似文献   

Determination of Ti, K, Sm and Gd Values in Geological Survey of Japan Reference Materials by Prompt Gamma Neutron Activation Analysis     

Takashi Sano  Toshiaki Hasenaka  Hiroyuki Sawahata  Takaaki Fukuoka 《Geostandards and Geoanalytical Research》2006,30(1):31-37

Prompt gamma neutron activation analysis was applied to the determination of the titanium, potassium, samarium and gadolinium contents of nine Geological Survey of Japan (GSJ) reference materials (JB-1, 1a, 2, 3; JA-1, 2, 3; JR-1, 2). Firstly, the values in JB-1 were determined by the standard addition method: pressed powder disks of JB-1 were used for neutron irradiation and gamma-ray measurements, after known quantities of standard reagents had been added. Secondly, the contents of eight other reference materials were determined by comparison methods using JB-1 as the comparative standard. The precision of analyses were obtained by replicate determinations on these samples. The relative standard deviation was generally less than 5%. For most samples, analysed values agreed well (< 5%) with the recommended values.  相似文献   

Partial mass isolation in tall buildings     

M. Ziyaeifar  H. Noguchi 《地震工程与结构动力学》1998,27(1):49-65

To find an economical approach in the seismic design of tall buildings, it is proposed to isolate a part of the structure by an isolator layer located in the height of building. Application of this technique causes a fundamental change in basic dynamic characteristics of the system. As a result, all major modal shapes of structure exhibit large displacement at the level of the isolator. A viscous damping device integrated into the isolation layer utilizes this relative movement to effectively reduce the earthquake input energy transmitted to the system. This technique is quite versatile and easily adjustable to different applications including seismic retrofit of buildings. Numerical analysis of some basic examples in this study shows desirable performances for a variety of applications. © 1998 John Wiley & Sons, Ltd.  相似文献   

New age constraints on counter-clockwise rotation of NE Japan     

Ayumi K. Baba  Takaaki Matsuda  Tetsumaru Itaya  Yutaka Wada  Noriyuki Hori  Masahiko Yokoyama  Nobuaki Eto  Rieko Kamei  Haider Zaman  Tesfaye Kidane  Yo-Ichiro Otofuji 《Geophysical Journal International》2007,171(3):1325-1341

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CCD Photometry of KZ Hya using the 45-CM Telescope in Paraguay     

Fredy Doncel  Alexis Troche  Takeshi Noguchi 《Astrophysics and Space Science》2004,290(3-4):399-408

A SX Phe-type pulsating variable KZ Hya (HD94033) was observed with CCD set attached to the 45-cm reflector at Asuncion Astronomical Observatory in Paraguay. In the present work, 12 maximum phases were covered. A new ephemeris has been obtained, and the result suggests a probable change of the pulsation period of KZ Hya.  相似文献   

Hayabusa‐returned sample curation in the Planetary Material Sample Curation Facility of JAXA     

Toru YADA  Akio FUJIMURA  Masanao ABE  Tomoki NAKAMURA  Takaaki NOGUCHI  Ryuji OKAZAKI  Keisuke NAGAO  Yukihiro ISHIBASHI  Kei SHIRAI  Michael E. ZOLENSKY  Scott SANDFORD  Tatsuaki OKADA  Masayuki UESUGI  Yuzuru KAROUJI  Maho OGAWA  Shogo YAKAME  Munetaka UENO  Toshifumi MUKAI  Makoto YOSHIKAWA  Junichiro KAWAGUCHI 《Meteoritics & planetary science》2014,49(2):135-153

Abstract– The Planetary Material Sample Curation Facility of JAXA (PMSCF/JAXA) was established in Sagamihara, Kanagawa, Japan, to curate planetary material samples returned from space in conditions of minimum terrestrial contaminants. The performances for the curation of Hayabusa‐returned samples had been checked with a series of comprehensive tests and rehearsals. After the Hayabusa spacecraft had accomplished a round‐trip flight to asteroid 25143 Itokawa and returned its reentry capsule to the Earth in June 2010, the reentry capsule was brought back to the PMSCF/JAXA and was put to a series of processes to extract recovered samples from Itokawa. The particles recovered from the sample catcher were analyzed by electron microscope, given their ID, grouped into four categories, and preserved in dimples on quartz slide glasses. Some fraction of them has been distributed for initial analyses at NASA, and will be distributed for international announcement of opportunity (AO), but a certain fraction of them will be preserved in vacuum for future analyses.  相似文献   

Investigation of cutting methods for small samples of Hayabusa and future sample return missions     

Masayuki Uesugi  Ryo Noguchi  Tooru Matsumoto  Junya Matsuno  Takashi Nagano  Akira Tsuchiyama  Shigenori Harada  Kaori Yokoyama  Yoshiaki Yodo  Noboru Takeda  Toru Yada  Shogo Yakame  Yuzuru Karouji  Yukihiro Ishibashi  Masanao Abe  Tatsuaki Okada  Akio Fujimura  Mitsuru Ebihara  Fumio Kitajima  Keisuke Nagao  Tomoki Nakamura  Hiroshi Naraoka  Takaaki Noguchi  Ryuji Okazaki  Hisayoshi Yurimoto 《Meteoritics & planetary science》2014,49(7):1186-1201

We report the investigation of cutting methods for Hayabusa samples. The purpose of our study is to explore the possibility of applying multiple analyses to a single particle effectively. We investigated the cutting performance of a blade dicing saw, laser, focused ion beam (FIB), and physical breaking by microindenter. Cutting performance was examined by estimating the aspect ratio of the cut slit, i.e., depth over width of the slit. We also investigated the possible contamination and sample damage by cutting. The result of the investigation shows that we can cut the samples from <50 μm to 500 μm using those methods with aspect ratios from 10 to 20, although they would introduce some contamination or damage to the samples. Our investigations also provide an important basis for the analysis of samples obtained by future sample return missions.  相似文献   

Three‐dimensional microstructure of samples recovered from asteroid 25143 Itokawa: Comparison with LL5 and LL6 chondrite particles     

Akira Tsuchiyama  Masayuki Uesugi  Kentaro Uesugi  Tsukasa Nakano  Ryo Noguchi  Toru Matsumoto  Junya Matsuno  Takashi Nagano  Yuta Imai  Akira Shimada  Akihisa Takeuchi  Yoshio Suzuki  Tomoki Nakamura  Takaaki Noguchi  Masanao Abe  Toru Yada  Akio Fujimura 《Meteoritics & planetary science》2014,49(2):172-187

In this study, the three‐dimensional (3‐D) microstructure of 48 Itokawa regolith particles was examined by synchrotron microtomography at SPring‐8 during the preliminary examination of Hayabusa samples. Moreover, the 3‐D microstructure of particles collected from two LL6 chondrites (Ensisheim and Kilabo meteorites) and an LL5 chondrite (Tuxtuac meteorite) was investigated by the same method for comparison. The modal abundances of minerals, especially olivine, bulk density, porosity, and grain size are similar in all samples, including voids and cracks. These results show that the Itokawa particles, which are surface materials from the S‐type asteroid Itokawa, are consistent with the LL chondrite materials in terms of not only elemental and isotopic composition of the minerals but also 3‐D microstructure. However, we could not determine whether the Itokawa particles are purely LL5, LL6, or a mixture of the two. No difference between the particles collected from Rooms A and B of the sample chamber, corresponding to the sampling sequence of the spacecraft's second and first touchdowns, respectively, was detected because of the statistically small amount of particles from Room B.  相似文献   

Crystallization temperature determination of Itokawa particles by plagioclase thermometry with X‐ray diffraction data obtained by a high‐resolution synchrotron Gandolfi camera     

Masahiko Tanaka  Tomoki Nakamura  Takaaki Noguchi  Aiko Nakato  Hatsumi Ishida  Toru Yada  Kei Shirai  Akio Fujimura  Yukihiro Ishibashi  Masanao Abe  Tatsuaki Okada  Munetaka Ueno  Toshifumi Mukai 《Meteoritics & planetary science》2014,49(2):237-244

The crystallization temperatures of Itokawa surface particles recovered by the space probe Hayabusa were estimated by a plagioclase geothermometer using sodic plagioclase triclinicity. The Δ131‐index required for the thermometer, which is the difference in X‐ray diffraction peak positions between the 131 and 11 reflections of plagioclase, was obtained by a high‐resolution synchrotron Gandolfi camera developed for the third generation synchrotron radiation beamline, BL15XU at SPring‐8. Crystallization temperatures were successfully determined from the Δ131‐indices for four particles. The observed plagioclase crystallization temperatures were in a range from 655 to 660 °C. The temperatures indicate crystallization temperatures of plagioclases in the process of prograde metamorphism before the peak metamorphic stage.  相似文献