Precise and Accurate In Situ Determination of Lead Isotope Ratios in NIST,USGS, MPI‐DING and CGSG Glass Reference Materials using Femtosecond Laser Ablation MC‐ICP‐MS     

Chen Kaiyun  Yuan Honglin  Bao Zhian  Zong Chunlei  Dai Mengning 《Geostandards and Geoanalytical Research》2014,38(1):5-21

Lead isotope ratio data were obtained with good precision and accuracy using a 266 nm femtosecond laser ablation (fLA) system connected to a multi‐collector ICP‐MS (MC‐ICP‐MS) and through careful control of analytical procedures. The mass fractionation coefficient induced by 266 nm femtosecond laser ablation was approximately 28% lower than that by 193 nm excimer laser ablation (eLA) with helium carrier gas. The exponential law correction method for Tl normalisation with optimum adjusted Tl ratio was utilised to obtain Pb isotopic data with good precision and accuracy. The Pb isotopic ratios of the glass reference materials NIST SRM 610, 612, 614; USGS BHVO‐2G, BCR‐2G, GSD‐1G, BIR‐1G; and MPI‐DING GOR132‐G, KL2‐G, T1‐G, StHs60/80‐G, ATHO‐G and ML3B‐G were determined using fLA‐MC‐ICP‐MS. The measured Pb isotopic ratios were in good agreement with the reference or published values within 2s measurement uncertainties. We also present the first high‐precision Pb isotopic data for GSE‐1G, GSC‐1G, GSA‐1G and CGSG‐1, CGSG‐2, CGSG‐4 and CGSG‐5 glass reference materials obtained using the femtosecond laser ablation MC‐ICP‐MS analysis technique.  相似文献   

基于MapGIS K9的航空物探图框绘制软件开发     

吴高微  ;闫红雨 《物探与化探》2014,(3):607-609

在分析MapGIS自带的图框绘制功能存在的不足和航空物探图框构成的基础上,应用C#语言和MapGIS K9的二次开发接口,开发航空物探图框绘制软件。实际应用表明,该软件能快速、方便地绘制不同种类的图框,提高工作效率;图框要素样式库易维护、易扩展,用户可根据实际需要进行定制。  相似文献   

多波束数据处理系统技术研究          下载免费PDF全文

张哲  顾锦华  谢丛涛  王莹 《海洋测绘》2010,30(2):52-54

针对当前多波束测深数据成果现状,探讨以Oracle 9i数据库为基础,搭建ArcGIS 8.3的SDE为空间数据引擎的多波束水深空间数据库,结合ComGIS技术开发多波束数据处理系统。系统功能包括测深数据的输入、管理、分析、显示、制图和绘图输出,改变了一般基于文件方式的多波束水深数据处理方式,成功的将空间数据库技术融入系统中,并有效运用了ComGIS开发系统前端平台,丰富了系统功能,具有一定的参考价值。  相似文献   

Sub-Alfvénic flows in the quiet and recurrent solar winds     

Gong-liang Zhang 《Chinese Astronomy and Astrophysics》1996,20(4):482-486

Observed instances are given in this paper to show that sub-Alfvénic flow can be formed in the quiet and recurrent low-speed solar wind streams. This kind of flow appears in regions with abnormal enhancement of Alfvénic speed and is associated with a specific type of magnetic configuration.  相似文献   

基于GIS的油田井位自动成图系统研究   总被引：1，自引：0，他引：1  

万剑华  刘善伟  刘国庆 《测绘科学》2007,32(6):91-93

针对油田生产中油水井数据的特点和管理需求,设计并开发了油田井位自动成图系统:基于Oracle9i与ArcSDE9.0创建空间数据库;基于ASP.NET技术开发浏览器端更新与维护属性数据;基于C与MapObjects2.3开发客户端实现成图及应用功能;对自动成图原理、远程数据访问、图属互查等功能提供了实现方法。  相似文献   

复合面状对象拓扑关系的表达模型     

陈占龙  冯齐奇  吴信才 《测绘学报》2015,44(4):438-444

为表达复合面状对象间的细节拓扑关系,对经典9-交集模型进行了改进,给出两种基于分解思想的9-交集模型,其中分解成简单区域的9-交集模型方法相对简单,但表现形式繁琐;分解成点集的9-交集模型的表现形式符合经典9-交集模型,但计算较为复杂。通过示例比较了两种扩展9-交集模型及经典9-交集模型的表达能力。结果表明,两种扩展交集模型均能准确地表达出复合面状对象各子部分之间的拓扑关系的细节,扩充了9-交集模型的表达能力。  相似文献   

一种基于实践九号卫星的快速系统误差补偿技术     

雷蓉  李禄  邓磊  李奇峻 《测绘科学技术学报》2015,32(2):152-156

直接利用光学遥感卫星的严格成像模型对地面点进行定位,定位误差与卫星姿态测量误差有关,其中包括地球自转引起的偏流角误差和姿态角常差。偏流角误差可以根据星历数据予以有效消除,而姿态角常差一般要利用少量控制点进行消除。基于此,在消除偏流角的影响下,这里采用了一种改进的四元数算法——P-H算法用于快速计算姿态角常差,并对系统误差进行补偿。该技术较常用的欧拉角解算,具有原理简单,计算速度快和结果稳定的特点。通过实践九号卫星影像的实验表明,运用该技术能快速和大幅度提高卫星在稀少控制点情况下的定位精度。  相似文献   

Determination of Ga,Ge, Mo,Ag, Cd,In, Sn,Sb, W,Tl and Bi in USGS Whole‐Rock Reference Materials by Standard Addition ICP‐MS          下载免费PDF全文

Richard M. Gaschnig  Roberta L. Rudnick  William F. McDonough 《Geostandards and Geoanalytical Research》2015,39(3):371-379

A procedure for determining a wide range of chalcophile and siderophile elements in typical crustal rocks using standard addition and ICP‐SFMS (inductively coupled plasma sector field mass spectrometry) is presented. New results for Ga, Ge, Mo, Ag, Cd, In, Sn, Sb, W, Tl and Bi abundances in USGS whole‐rock reference materials AGV‐2, BHVO‐1, BIR‐1, G‐2, GSP‐1 and W‐2 are reported using this analytical procedure. Intermediate precision of means based on multiple dissolved aliquots of each USGS reference material was 10% RSD or better for Ga, Ge, In and Sn in all, and similarly good for Ag, Cd, Sb, Tl and Bi in most reference materials. Poorer intermediate precision of Mo and W measurements in several reference materials is probably due to higher analytical blanks on these elements and powder heterogeneity due to a sulfide‐related nugget effect in the specific case of Mo in GSP‐1. Results for all elements fell within the range of available published data with the exception of Ag, which yielded systematically higher concentrations than found in the literature for five of the six reference materials, likely reflecting interference from unresolved polyatomic species.  相似文献   

A Review of the IAG GeoPT™ and Certification Programmes,their Protocols,and the Differences between the Original and Potential Modifications to the Certification Protocol          下载免费PDF全文

Jean S. Kane 《Geostandards and Geoanalytical Research》2015,39(4):419-432

The IAG conducts two programmes, the GeoPT ^? proficiency test and a certification programme that are closely interconnected. Both support the quality control/quality assurance activities of geochemical laboratories. Each derives an estimate of ‘true value’ for a number of samples, but arrives at that estimate, and its uncertainty, differently. This review discusses the history of the two programmes and compares the ‘true values’ and their uncertainties obtained through each. It then considers ‘fitness‐for‐purpose’ issues related to both GeoPT ^? and certification uncertainties. Issues related to potential modification of the IAG protocol for certification are also considered.  相似文献   

The Reliability of Assigned Values from the GeoPT Proficiency Testing Programme from an Evaluation of Data for Six Test Materials that have been Characterised as Certified Reference Materials          下载免费PDF全文

Philip J. Potts  Michael Thompson  Peter C. Webb 《Geostandards and Geoanalytical Research》2015,39(4):407-417

Assigned values derived from the GeoPT proficiency testing programme were compared with certified values for six certified reference materials that have been used as test materials in the GeoPT programme. Statistical analysis showed that there were few significant differences between these sets of data and that these differences had no significant impact on the GeoPT assessment when fitness‐for‐purpose criteria were taken into account.  相似文献