Trace Element Analysis of NIST SRM 614 and 616 Glass Reference Materials by Laser Ablation Microprobe-Inductively Coupled Plasma-Mass Spectrometry   总被引：3，自引：0，他引：3  

Masanori Kurosawa  Simon E. Jackson  Shigeho Sueno 《Geostandards and Geoanalytical Research》2002,26(1):75-84

Fifty elements in NIST SRM 614 and 616 glass reference materials were determined by laser ablation microprobe-inductively coupled plasma-mass spectrometry (LAM-ICP-MS). The values determined for NIST SRM 614 agreed well with the NIST-certified and information values (mean relative difference ± 3.6%), except for B, Sc and Sb. The values determined for NIST SRM 616 agreed with the NIST-certified and information values within a mean relative difference of ± 1.5%, except for B, Sc and Ga. In addition, at an 80 μm sampling scale, NIST SRM 614 and 616 glass discs were homogeneous for trace elements within the observed precisions of 5 and 15% (mean), respectively. Detection limits were in the range 0.01 - 0.3 μg g⁻¹ for elements of lower mass numbers (amu < 80) and 1 - 10 ng g⁻¹ for heavy elements (amu > 80). Detection at the sub ng g⁻¹ level is possible for most of the heavy elements by using an ablation pit size larger than 10 0 μm.  相似文献   

G-Probe-1 - An International Proficiency Test for Microprobe Laboratories - Report on Round 1 : February 2002 (TB-1 Basaltic Glass)     

Philip J. Potts  Michael Thompson  Stephen Wilson 《Geostandards and Geoanalytical Research》2002,26(2):197-235

Results are presented for round one of a new international proficiency testing programme designed for microprobe laboratories involved in the routine analysis of silicate minerals. The sample used for this round was TB-1, a basaltic glass fused and prepared by the USGS. Thirty nine laboratories contributed data to this round, the majority of major element results being undertaken by EPMA and the majority of trace elements by LA-ICP-MS. Assigned values were derived from the median of results produced by nine selected laboratories that analysed powdered material by conventional ICP-MS, INAA and XRF techniques using bulk powders of the sample. Submitted microprobe results were evaluated using a target precision calculated using the Horwitz function, adopting the same criteria as those used for "applied" geochemistry laboratories in the companion GeoPT proficiency testing programme for laboratories involved in the routine bulk analysis of silicate rocks. An evaluation of results from participating microprobe laboratories indicated that overall, data were compatible with this precision function. A comparison between the performance of bulk and microprobe techniques used in the analysis of the basaltic glass showed remarkably good agreement, with significant bias only observed for the major oxide MgO.  相似文献   

小波变换在少震、弱震区地下水位数据分析中的应用   总被引：12，自引：2，他引：12  

敬少群  王佳卫  童迎世 《华南地震》2002,22(2):9-15

利用小波变换和多尺度分析原理，对位于少震弱震区的湖南的具有不同变化形态的6口典型井4年的水位日均值序列进行了分析。结果显示，通过多尺度分析可以很方便地将水位日均值序列中的高频部分与低频部分分开，而且对不同井孔的含水层系统而言，分离出去的频率成分的主模是不同的，这反应出不同井孔的含水层系统对同一频率的响应存在差异，主模的频率反映了正常背景下井孔－含水层系统的优势频率。Morlet小波分析的结果对时间序列的突然变化和周期结构都有很好的反映。  相似文献   

分形在地貌学中应用的几个问题的分析   总被引：5，自引：0，他引：5  

李锰  朱令人  龙海英 《地震研究》2002,25(2):155-162

就实际地貌分形研究工作中经常遇到的截面约定、自仿射分形局域维与渡越长度、分维的比较以及过渡分形等几个问题进行了分析和探讨，并提出了在应用过程中的注意事项和解决方案。  相似文献   

小波分析在声发射资料处理中的初步应用   总被引：1，自引：0，他引：1  

陈顺云  杨润海  王赟赟  赵晋明  许昭永 《地震研究》2002,25(4):328-334

针对声发射数据分析的一些难点，把最近20年发展起来的小波技术引入声发射资料处理中，分析证明结果可靠。它在本中的应用有：（1）提取有效信息。小波强大分解（细化0能力可用来从高口音中找出有效记录，分解合成时可以去掉不理想的通道，使声发射数据更加“规则化”，有望实现到时自动判读。（2）对相互叠加的事件进行有效分离。结合全波记录，可使事件尽可能少丢失，提高声发射数量统计及b值计算等的精度。（3）使成份复杂的声发射波形数据分离成具有单一特征的波，但分解后的波究竟属于P波还是S波，甚至面波，尚难确定。  相似文献   

To afforest the desert with the technology of peat composed of rotten mosses and the sustainable development of the oases     

王周琼 《中国科学D辑(英文版)》2002,45(Z1)

Only by providing the good conditions for the growth of plants can a favorable ecologicalenvironment on which human beings rely for existence be created. The upside-down-T dou-ble-layer water-conserving afforestation way is developed according to the situation of the short-age of water resources, low soil fertility and vast land in the arid areas. The characteristics of theafforestation way are to change the microenvironment in the root area of the plants, provide thefavorable conditions for the growth of plants, and reduce the necessary conditions for the growth ofplants in large areas in the arid regions. Meanwhile, the size of its water-conserving layer can bechanged according to the size of the planted trees. The different ways of the bottom wa-ter-conserving layer can be used according to the requirements. The afforestation way is suitablefor planting trees on a small scale and also for afforesting on a large scale under the adverse cir-cumstances in the arid areas, and has been effectively used in the afforestation in the hinterland ofTaklamakan Desert and the southern marginal zone of Gurbantonggut Desert. The prospects ofthe afforestation way are broad in afforestation and desertification control in the desert regions.  相似文献   

Horizontal and vertical components of earthquake ground motions at liquefiable sites   总被引：1，自引：0，他引：1  

J. Yang  T. Sato  S. Savidis  X. S. Li 《Soil Dynamics and Earthquake Engineering》2002,22(3)

Field observations on ground motions from recent earthquakes imply that current knowledge is limited with regard to relating vertical and horizontal motions at liquefiable sites. This paper describes a study with the purpose of clarifying this emerging issue to some extent. A series of numerical analyses is carried out on a liquefiable soil deposit with a verified, fully coupled, nonlinear procedure. It is shown that the transformation of vertical motions in the deposit differs considerably from the transformation of horizontal motions. Both the amplitude and frequency content of the horizontal motions are strongly dependent on the shaking level or the associated nonlinear soil behavior. The transfer function for vertical motions is however likely to be independent of the intensity of input motions; no reduction in the amplitude occurs even in the case of strong shaking. The results are shown to be in consistence with the laboratory observations on shaking table tests and recent field observations that less nonlinearity exists for vertical motions. It is also shown that the possibility exists for using information on spectral ratios between the horizontal and vertical surface motions to quickly identify in situ soil behavior and liquefaction that are not readily covered by conventional field or laboratory experimentation procedures.  相似文献   

Viscous damping formulation and high frequency motion propagation in non-linear site response analysis     

Youssef M. A. Hashash   《Soil Dynamics and Earthquake Engineering》2002,22(7)

Non-linear time domain site response analysis is widely used in evaluating local soil effects on propagated ground motion. This approach has generally provided good estimates of field behavior at longer periods but has shortcomings at relatively shorter periods. Viscous damping is commonly employed in the equation of motion to capture damping at very small strains and employs an approximation of Rayleigh damping using the first natural mode only. This paper introduces a new formulation for the viscous damping using the full Rayleigh damping. The new formulation represents more accurately wave propagation for soil columns greater than 50 m thick and improves non-linear site response analysis at shorter periods. The proposed formulation allows the use of frequency dependent viscous damping. Several examples, including a field case history at Treasure Island, California, demonstrate the significant improvement in computed surface response using the new formulation.  相似文献   

Verification of the dualism ordering method by the canonical correspondence analysis: fish community samples     

Tadeusz Penczak  Francisco Godinho  Angelo A. Agostinho 《Limnologica》2002,32(1)

Two ordination techniques (Romaniszyn diagram, RD, and Canonical correspondence analysis, CCA) were applied to the same data set (fish assemblage composition along two Paraná river tributaries and associated environmental variables), to identify spatial community patterns and further to evaluate the performance of RD. The major patterns in these Brazilian streams were successfully revealed by both methods (i.e. clear separation of both tributaries on the basis of fish assemblage composition and environmental factors), but more complex situations may limit the application of RD in comparison with CCA.  相似文献   

皮肤图像分析系统对祛斑类化妆品功效评价的研究   总被引：13，自引：0，他引：13  

孟如松  蔡瑞康  赵广  马慧军  周付根  姜志国  赵宇 《CT理论与应用研究》2002,11(1):20-25

目的是探索如何获得不同色素性皮肤病的清晰图像，研制出操作简单、自动化与精度高的皮肤图像分析系统。方法：应用多光谱皮肤显微偏振光与数字图像处理技术，测量目标皮损形状、面积、灰度、积分光密度及色素颜色参数的变化等。结果：用祛斑类化妆品和药物治疗136例黄褐斑、经该系统测量分析后各治疗组相关参数随时间的推移呈下降趋势，而药物组与对照组相比各参数值明显下降、与各组相比均有显著差异（P＜0．05），并提出客观的疗效评定单位“ID”值。结论：该系统是一种潜力较大的皮肤表面色素定量工具，客观性和重复性好，灵敏度高，不对观察对象造成损伤，在临床获得满意效果。  相似文献