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111.
112.
Analysis of Sediments and Soils by X-Ray Fluorescence Spectrometry Using Matrix Corrections Based on Fundamental Parameters 总被引:2,自引:0,他引:2
Jacinta Enzweiler Maria Aparecida Vendemiatto 《Geostandards and Geoanalytical Research》2004,28(1):103-112
Wavelength dispersive X-ray fluorescence spectrometry (WD-XRF) is widely used for the analysis of soils and sediments using well characterised procedures. However, difficulties can occur with samples such as unknowns containing small amounts of ore materials and samples collected from contaminated sites where trace elemental concentrations can exceed the concentration range for routine analysis. We studied the performance of a commercially available method, based on fundamental parameters (FP) to correct matrix effects. The spectrometer was originally calibrated with elemental or simple compound calibrants. Samples were analysed as pressed powder pellets. Eighteen sediment and soil reference materials, three of them with certified values for some of their constituents, were used to evaluate accuracy, by comparing results with recommended values and their standard deviations (RV ± 2s) or certified values and their confidence intervals (CV ± Cl). When results fell systematically outside these intervals, calibrations were refined with geochemical reference materials. The best agreement of results with recommended and certified values was obtained when the contents of H2 O and C in each sample were included as matrix constituents during calculations. The detection limits of trace elements tended to be relatively high, because the measuring conditions employed were not maximised for sensitivity. The main advantage of the method tested was that it enabled the analysis of samples with high concentrations of trace elements and the determination of elements such as F, Bi, Sb and W, which are not commonly included in quantitative XRF analysis of geological samples. 相似文献
113.
A Reflection on Mg, Cd, Ca, Li and Si Isotopic Measurements and Related Reference Materials 总被引:6,自引:1,他引:6
Jean Carignan Damien Cardinal Anton Eisenhauer Albert Galy Mark Rehkamper Frank Wombacher Nathalie Vigier 《Geostandards and Geoanalytical Research》2004,28(1):139-148
This contribution aims to report the reflections we had with the scientific community during two international workshops on reference materials for stable isotopes in Davos (2002) and Nice (2003). After evaluating the isotopic homogeneity of some existing reference materials, based on either certificates, literature data or specific inter-laboratory rounds, we confirm these as primary reference materials or propose new ones relative to which stable isotope compositions should be reported. We propose DSM-3 for Mg, NIST SRM 915a for Ca, L-SVEC for Li and NBS28 for Si. Cadmium does not yet have a well identified delta zero material, although three commercial mono-elemental Cd solutions have yielded the same isotopic composition relative to one another. In order to scale the linearity of any mass spectrometer, some secondary reference materials are also proposed: Cambridge-1 solution for Mg, the "Münster-Cd" and JEPPIM Cd solutions for Cd and the "Big Batch" silicate for Si. The team from Nancy propose to prepare a mixed spike solution for Li isotopes. Well-characterised natural samples such as ocean or continental waters, diatoms, sponges, rocks and minerals are needed to validate the entire analytical procedure, particularly to take into account the effect of sample mineralisation and of chemical manipulations for elemental separation prior to analysis. 相似文献
114.
Precise/ Small Sample Size Determinations of Lithium Isotopic Compositions of Geological Reference Materials and Modern Seawater by MC-ICP-MS 总被引:6,自引:1,他引:6
Alistair B. Jeffcoate Tim Elliott Alex Thomas Claudia Bouman 《Geostandards and Geoanalytical Research》2004,28(1):161-172
The Li isotope ratios of four international rock reference materials, USGS BHVO-2, GSJ JB-2, JG-2, JA-1 and modern seawater (Mediterranean, Pacific and North Atlantic) were determined using multi-collector inductively coupled plasma-mass spectrometry (MC-ICP-MS). These reference materials of natural samples were chosen to span a considerable range in Li isotope ratios and cover several different matrices in order to provide a useful benchmark for future studies. Our new analytical technique achieves significantly higher precision and reproducibility (< ± O.3%o 2s) than previous methods, with the additional advantage of requiring very low sample masses of ca . 2 ng of Li. 相似文献
115.
Natural disasters like floods, tornadoes, tropicalcyclones, heat and cold wavewreak havoc and cause tremendous loss ofproperty all over the world. Most ofthe natural disasters are either dueto weather or are triggered due toweather related processes.Extreme weather events claimed thousands oflives and caused damage on vastscale. Recent super cyclone which affectedOrissa in 1999, Bangladesh cyclone of1970 and Hurricane Andrew in 1992 areexamples of some of the more damagingtropical cyclones which affected developingas well as the developed world. Heatand cold waves are also extreme events,which cause enormous losses in terms oflives lost and human discomfort and ailmentsarising out of them. The heat waveof 1995 and 1998 are still fresh in the mindof the Indian public. The estimated lossof human lives due to heat wave in 1998 was morethan 15,000. Economic losses asa result of these disasters and in particular inassociation with tropical cyclones haveincreased enormously over the last three decades.During 1961–1991, total loss oflives from drought alone was 1,333,728 overthe whole world. In terms of economiclosses, there is 8–10 fold increase from thebase figure of 1960. The socio-economicimpact of natural disaster is complex dependingupon the vulnerability of the placeand mitigation strategies that are put in place.Meteorology plays a crucial role in forewarningpeople about the severe/extremeweather systems and a constant endeavour by themeteorological services worldover has gone a long way towards minimizing thelosses caused by natural disasters.The paper summarises the natural disasterstatistics over south Asia and the possibleprediction strategies for combating theirsocio-economic impacts. 相似文献
116.
于3个假说和林冠上方2m处的气象变量,采用Penman-Monteith组合模型估算了一个生长季节内川西亚高山林区分别以云杉(SF)、冷杉(FF)和白桦(BF)为优势树种的3个林分的湿林冠蒸发速率(Er)。研究结果表明,SF、FF和BF的湿林冠蒸发量(E)分别为44.51mm、88.51mm和57.8mm,分别占总降雨量的9.2%、16.6%和10.2%。与SF和BF相比,FF具有最高的月平均Er和蒸发比例。SF、FF和BF的平均Er分别为0.097mm/h(变化范围:0.028-0.487mm/h)、0.242mm/h(变化范围:0.068~0.711mm/h)和0.149mm/h(0.060~0.576mm/h)。最高和最低的月平均Er分别在6月(SF、FF和BF分别为0.120mm/h、0.317mm/h和0.169mm/h)和10月(SF、FF和BF分别为0.083mm/h、0.187mm/h和0.101mm/h)。8:00至16:00期间的平均点Er显著高于0:00至8:00以及16:00至0:00期间的平均Er。Er显著的日变化和月变化主要归因于林冠上方的太阳辐射、空气温度和相对湿度的变化。 相似文献
117.
沙尘天气等对西安市空气污染影响的研究 总被引:7,自引:10,他引:7
通过对西安市1981—2000年TSP、SO2和NOx年平均浓度资料,1998—2000年周报和日报环境监测资料以及相应的地面、高空常规气象观测资料的统计分析,研究了该市空气污染的时间变化特点以及沙尘天气等几种气象条件对其浓度变化的影响。结果表明:(1)颗粒污染物(TSP和PM10)是西安市的首要污染物,其次是SO2。1981—2000年期间,TSP年平均浓度降低了75%,SO2年平均浓度降低了77%,NOx年平均浓度总体上变化不大;这三种污染物月平均浓度的年变化都呈单周期型,冬季1月份最高,夏季最低(TSP是7月份最低,SO2和NOx是8月份最低)。(2)2001年春季3~4月份沙尘天气的频繁发生,使西安市空气污染日出现全年的第二个多发期(23d·月-1),这有别于正常年份仅在冬季1月份出现一个浓度峰值的特点;强沙尘暴天气过程会使西安市PM10浓度在非常短的时间内提高3倍左右,造成严重的颗粒物污染。(3)西安市冬半年出现轻度污染以上级别的几率明显大于夏半年。影响西安市的地面天气系统可归纳为12类,当受不同天气系统控制时,其污染状况会有较大差异。(4)西安市一年四季都有逆温存在,100m平均逆温强度为0.90℃;全年以低层逆温出现日数最多,但冬季贴地逆温出现日数最多,厚度最厚,强度最大,是造成西安市冬季空气污染严重的最重要气象因素之一。(5)西安 相似文献
118.
119.
分析了自动气象站分钟雨量资料获取与转换的必要性,介绍了雨量资料获取的思路与具体方法.通过这种方法,实现了商丘市所有自动气象站雨量资料的共享,并与GPRS、GSM乡级自动雨量站资料进行融合. 相似文献
120.