铝片还原-硫酸铁铵容量法测定钛铁矿中高含量     

李锟 《化工矿产地质》2007,29(2):112-114

试样经碱熔,盐酸提取的钛,在以盐酸、硫酸、磷酸组成的强酸性溶液体系中,利用铝片的强还原性,还原四价钛为三价钛。再用三价铁氧化三价钛为四价钛,过量的三价铁离子与硫氢酸根离子生成血红色络合物,根据此原理测定高含量钛。实验证明,溶液在此强酸性体系中,隔绝空气和控制时间的条件下,其含量范围在0.13%～100%内,测定结果准确度高。  相似文献   

利用催化动力学原理测定化探样中微量碘的含量     

吴萍  李锟 《化工矿产地质》2007,29(1):42-44

在HAc-NaAc形成的中性缓冲溶液体系中,利用碘的催化动力学原理,使N-N-四甲基-4-4-二氨基二苯甲烷与氯胺T的氧化反应,生成蓝色络合物来测定地探样中微量碘的含量。通过实验,最佳试剂加入量为8%的HAc溶液5mL,8%的Na2CO3溶液3mL,0.1%的N-N-四甲基-4-4-二氨基二苯甲烷溶液5mL所组成的溶液体系中,在加入0.1%的氯胺T1mL显色后,其测定结果准确度、精密度高,检出限低,测定化探样中微量碘时该方法可以推广应用。  相似文献   

滇中富民县宝石洞旅游地质特征与成景机制探讨     

周余国  张帆  周坤  周琛粟  王玉朝  王健  范凯 《高校地质学报》2021,27(4):480-488

滇中富民县宝石洞岩溶地下河洞穴景观系统规模适中,洞内岩溶景观千姿百态,洞中有宝(玛瑙),洞外有优美的生态环境和多元民族宗教文化以及潜在的温泉资源,加上优越的交通区位,旅游要素集群度较高,具较高开发价值.文章根据宝石洞地区区域地质背景,分析了该地区区域地史演化特征,根据本次对宝石洞的实地探测成果,总结了宝石洞旅游地质特征...  相似文献   

河流-三角洲体系微相控烃及机理研究:以珠江口盆地恩平组煤系烃源岩为例     

李燕  邓运华  李友川 《现代地质》2021,35(4):1065-1077

河流-三角洲体系煤系烃源岩是重要的油气来源,传统的研究方法主要为单井点分析,对研究区的勘探程度和资料情况的依赖性大,而且认识滞后于勘探,很难在油气勘探和有利生烃洼陷的预测中发挥作用.对珠江口盆地恩平组煤系烃源岩进行系统研究,揭示煤系烃源岩发育的特征和有利地质条件,并将沉积微相分析与烃源岩的地球化学指标(有机质丰度、生烃...  相似文献   

世界主要海洋强国综合实力测评研究     

殷克东  张斌  王立彭  张燕歌 《海洋技术学报》2007,26(4):121-125

文章在回顾世界海洋强国发展历程和分析现阶段发展特点的基础上,构建国家层面的海洋综合实力评价指标体系,并结合层次分析法和加权积决策理论建立了综合实力测评模型。通过选取世界上8个有代表意义的海洋强国,结合其海洋综合实力的现状分析,利用测评模型对其进行测评排序,为我国"海洋强国"战略的科学规划提供参考。  相似文献   

海洋发光弧菌生长和发光条件的研究     

方宏达  董燕红  袁茵  李秀芹  易斌 《海洋通报》2007,26(4):66-70

海洋生物发光研究对渔业、环境监测等有着举足轻重的意义。根据从湛江东海岛海域沉积物样品中分离出的一株海洋发光弧菌(Vibrio sp.,编号为D2),对这株菌的生长和发光条件进行了初步研究。实验结果表明,海洋发光弧菌D2在pH7.0、温度35℃、NaCl浓度为2.0%时,生长状态最好;在pH5~6、温度20℃、NaCl浓度为3.0%、细菌密度OD600达0.08时,发光强度最高。  相似文献   

Formation and evolution of the modem warm current system in the East China Sea and the Yellow Sea since the last deglaciation     

LI Tiegang  NAN Qingyun  JIANG Bo  SUN Rongtao  ZHANG Deyu  LI Qing 《中国海洋湖沼学报》2009,27(2)

To reconstruct the formation and evolution process of the warm current system within the East China Sea (ECS) and the Yellow Sea (YS) since the last deglaciation, the paleoceangraphic records in core DGKS9603, core CSH1 and core YSDPI02, which were retrieved from the mainstream of the Kuroshio Current (KC), the edge of the modem Tsushima Warm Current (TWC) and muddy region under cold waters accreted with the Yellow Sea Warm Current (YSWC) respectively, were synthetically analyzed. The results indicate that the formation and evolution of the modem warm current system in the ECS and the YS has been accompanied by the development of the KC and impulse rising of the sea level since the last deglaciation. The influence of the KC on the Okinawa Trough had enhanced since 16 cal kyr BE and synchronously the modem TWC began to develop with the rising of sea level and finally formed at about 8.5 cal kyr BP. The KC had experienced two weakening process during the Heinrich event 1 and the Younger Drays event from 16 to 8.5 cal kyr BP. The period of 7-6 cal kyr BP was the strongest stage of the KC and the TWC since the last deglaciation. The YSWC has appeared at about 6.4 cal kyr BP. Thus,the warm current system of the ECS and the YS has ultimately formed. The weakness of the KC,indicated by the occurrence of Pulleniatina minimum event (PME) during the period from 5.3 to 2.8 cal kyr BE caused the main stream of the TWC to shift eastward to the Pacific Ocean around about 3 cal kyr BP. The process resulted in the intruding of continent shelf cold water mass with rich nutrients. Synchronously, the strength of the YSWC was relatively weak and the related cold water body was active at the early-mid stage of its appearance against the PME background, which resulted in the quick formation of muddy deposit system in the southeastern YS. The strength of the warm current system in the ECS and the YS has enhanced evidently, and approached to the modern condition gradually since 3 cal kyr BP.  相似文献   

Discrete time-delay control of an autonomous underwater vehicle: Theory and experimental results     

R.P. Kumar  D. Sen 《Ocean Engineering》2009,36(1):74-81

A discrete time-delay control (DTDC) law for a general six degrees of freedom unsymmetric autonomous underwater vehicle (AUV) is presented. Hydrodynamic parameters like added mass coefficients and drag coefficients, which are generally uncertain, are not required by the controller. This control law cancels the uncertainties in the AUV dynamics by direct estimation of the uncertainties using time-delay estimation technique. The discrete-time version of the time-delay control does not require the derivative of the system state to be measured or estimated, which is required by the continuous-time version of the controller. This particularly provides an advantage over continuous-time controller in terms of computational effort or availability of sensors for measuring state derivatives, i.e., linear and angular accelerations. Implementation issues for practical realization of the controller are discussed. Experiments on a test-bed AUV were conducted in depth, pitch, and yaw degrees of freedom. Results show that the proposed control law performs well in the presence of uncertainties.  相似文献   

Underwater autonomous manipulation for intervention missions AUVs   总被引：1，自引：0，他引：1  

Giacomo Marani  Song K. Choi  Junku Yuh 《Ocean Engineering》2009,36(1):15-23

Many underwater intervention tasks are today performed using manned submersibles or remotely operated vehicles in teleoperation mode. Autonomous underwater vehicles are mostly employed in survey applications. In fact, the low bandwidth and significant time delay inherent in acoustic subsea communications represent a considerable obstacle to remotely operate a manipulation system, making it impossible for remote controllers to react to problems in a timely manner.Nevertheless, vehicles with no physical link and with no human occupants permit intervention in dangerous areas, such as in deep ocean, under ice, in missions to retrieve hazardous objects, or in classified areas. The key element in underwater intervention performed with autonomous vehicles is autonomous manipulation. This is a challenging technology milestone, which refers to the capability of a robot system that performs intervention tasks requiring physical contacts with unstructured environments without continuous human supervision.Today, only few AUVs are equipped with manipulators. SAUVIM (Semi Autonomous Underwater Vehicle for Intervention Mission, University of Hawaii) is one of the first underwater vehicle capable of autonomous manipulation.This paper presents the solutions chosen within the development of the system in order to address the problems intrinsic to autonomous underwater manipulation. In the proposed approach, the most noticeable aspect is the increase in the level of information transferred between the system and the human supervisor.We describe one of the first trials of autonomous intervention performed by SAUVIM in the oceanic environment. To the best knowledge of the authors, no sea trials in underwater autonomous manipulation have been presented in the literature. The presented operation is an underwater recovery mission, which consists in a sequence of autonomous tasks finalized to search for the target and to securely hook a cable to it in order to bring the target to the surface.  相似文献   

Systematic conservation planning in the Mediterranean: a flexible tool for the identification of no-take marine protected areas     

Maiorano  Luigi; Bartolino  Valerio; Colloca  Francesco; Abella  Alvaro; Belluscio  Andrea; Carpentieri  Paolo; Criscoli  Alessandro; Jona Lasinio  Giovanna; Mannini  Alessandro; Pranovi  Fabio; Reale  Bruno; Relini  Giulio; Viva  Claudio; Ardizzone  Gian Domenico 《ICES Journal of Marine Science》2009,66(1):137-146

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