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51.
提出了国家地理空间信息基准框架内改进与更新原有的大地坐标基准、高程基准和重力基准的建设道路及解决原则。 相似文献
52.
高斯平面坐标换算到测区平均高程面上的方法 总被引:5,自引:2,他引:5
依据高斯投影原理,提出了一种在高斯平面与任决高程平面间进行坐标转换的方法,并设计了相应的计算软件。 相似文献
53.
用差热和热(失)重法、pH值检验、离子色谱等分析方法考察和证实了Cl-对平菲尔特管重量法测定化合水(H2O+)的干扰,研究其影响规律,提出用系数校正方法可获得H2O+的准确结果。方法用于含氯深海沉积物和大洋多金属结核标准物质中H2O+的定值分析,取得满意结果 相似文献
54.
多金属结核中二氧化锰的测定 总被引:1,自引:0,他引:1
用过量的含有H2SO4的(NH4)2Fe(SO4)2溶液分解多金属结核的同时,还原了试样中的MnO2,然后以K2Cr2O7标准溶液滴定测定了多金属结核中的MnO2。就样品分解过程中的加热温度和时间对测定结果的影响及标准溶液的标定等问题进行了讨论,经多次测定,方法重现性好。应用此方法为新研制的多金属结核标准物质提供了MnO2的定值数据,其结果与初定值相符,无剔除值,精密度(RSD,n=8)小于06%。 相似文献
55.
着重介绍了间隔式钻孔灌注桩在挡土护坡技术中的应用方法,设计时的主要参考依据,计算土压力理论的应用原则以及施工中需注意的几个问题,为进行深基础挡土护坡的工程提供了部分参考依据。 相似文献
56.
Analysis of Sediments and Soils by X-Ray Fluorescence Spectrometry Using Matrix Corrections Based on Fundamental Parameters 总被引:2,自引:0,他引:2
Jacinta Enzweiler Maria Aparecida Vendemiatto 《Geostandards and Geoanalytical Research》2004,28(1):103-112
Wavelength dispersive X-ray fluorescence spectrometry (WD-XRF) is widely used for the analysis of soils and sediments using well characterised procedures. However, difficulties can occur with samples such as unknowns containing small amounts of ore materials and samples collected from contaminated sites where trace elemental concentrations can exceed the concentration range for routine analysis. We studied the performance of a commercially available method, based on fundamental parameters (FP) to correct matrix effects. The spectrometer was originally calibrated with elemental or simple compound calibrants. Samples were analysed as pressed powder pellets. Eighteen sediment and soil reference materials, three of them with certified values for some of their constituents, were used to evaluate accuracy, by comparing results with recommended values and their standard deviations (RV ± 2s) or certified values and their confidence intervals (CV ± Cl). When results fell systematically outside these intervals, calibrations were refined with geochemical reference materials. The best agreement of results with recommended and certified values was obtained when the contents of H2 O and C in each sample were included as matrix constituents during calculations. The detection limits of trace elements tended to be relatively high, because the measuring conditions employed were not maximised for sensitivity. The main advantage of the method tested was that it enabled the analysis of samples with high concentrations of trace elements and the determination of elements such as F, Bi, Sb and W, which are not commonly included in quantitative XRF analysis of geological samples. 相似文献
57.
A Reflection on Mg, Cd, Ca, Li and Si Isotopic Measurements and Related Reference Materials 总被引:6,自引:1,他引:6
Jean Carignan Damien Cardinal Anton Eisenhauer Albert Galy Mark Rehkamper Frank Wombacher Nathalie Vigier 《Geostandards and Geoanalytical Research》2004,28(1):139-148
This contribution aims to report the reflections we had with the scientific community during two international workshops on reference materials for stable isotopes in Davos (2002) and Nice (2003). After evaluating the isotopic homogeneity of some existing reference materials, based on either certificates, literature data or specific inter-laboratory rounds, we confirm these as primary reference materials or propose new ones relative to which stable isotope compositions should be reported. We propose DSM-3 for Mg, NIST SRM 915a for Ca, L-SVEC for Li and NBS28 for Si. Cadmium does not yet have a well identified delta zero material, although three commercial mono-elemental Cd solutions have yielded the same isotopic composition relative to one another. In order to scale the linearity of any mass spectrometer, some secondary reference materials are also proposed: Cambridge-1 solution for Mg, the "Münster-Cd" and JEPPIM Cd solutions for Cd and the "Big Batch" silicate for Si. The team from Nancy propose to prepare a mixed spike solution for Li isotopes. Well-characterised natural samples such as ocean or continental waters, diatoms, sponges, rocks and minerals are needed to validate the entire analytical procedure, particularly to take into account the effect of sample mineralisation and of chemical manipulations for elemental separation prior to analysis. 相似文献
58.
Precise/ Small Sample Size Determinations of Lithium Isotopic Compositions of Geological Reference Materials and Modern Seawater by MC-ICP-MS 总被引:6,自引:1,他引:6
Alistair B. Jeffcoate Tim Elliott Alex Thomas Claudia Bouman 《Geostandards and Geoanalytical Research》2004,28(1):161-172
The Li isotope ratios of four international rock reference materials, USGS BHVO-2, GSJ JB-2, JG-2, JA-1 and modern seawater (Mediterranean, Pacific and North Atlantic) were determined using multi-collector inductively coupled plasma-mass spectrometry (MC-ICP-MS). These reference materials of natural samples were chosen to span a considerable range in Li isotope ratios and cover several different matrices in order to provide a useful benchmark for future studies. Our new analytical technique achieves significantly higher precision and reproducibility (< ± O.3%o 2s) than previous methods, with the additional advantage of requiring very low sample masses of ca . 2 ng of Li. 相似文献
59.
Natural disasters like floods, tornadoes, tropicalcyclones, heat and cold wavewreak havoc and cause tremendous loss ofproperty all over the world. Most ofthe natural disasters are either dueto weather or are triggered due toweather related processes.Extreme weather events claimed thousands oflives and caused damage on vastscale. Recent super cyclone which affectedOrissa in 1999, Bangladesh cyclone of1970 and Hurricane Andrew in 1992 areexamples of some of the more damagingtropical cyclones which affected developingas well as the developed world. Heatand cold waves are also extreme events,which cause enormous losses in terms oflives lost and human discomfort and ailmentsarising out of them. The heat waveof 1995 and 1998 are still fresh in the mindof the Indian public. The estimated lossof human lives due to heat wave in 1998 was morethan 15,000. Economic losses asa result of these disasters and in particular inassociation with tropical cyclones haveincreased enormously over the last three decades.During 1961–1991, total loss oflives from drought alone was 1,333,728 overthe whole world. In terms of economiclosses, there is 8–10 fold increase from thebase figure of 1960. The socio-economicimpact of natural disaster is complex dependingupon the vulnerability of the placeand mitigation strategies that are put in place.Meteorology plays a crucial role in forewarningpeople about the severe/extremeweather systems and a constant endeavour by themeteorological services worldover has gone a long way towards minimizing thelosses caused by natural disasters.The paper summarises the natural disasterstatistics over south Asia and the possibleprediction strategies for combating theirsocio-economic impacts. 相似文献
60.
通过对1983年12月28日、2002年12月26日百色市两次异常降雪天气过程的对比分析,发现冬季孟加拉湾槽的发展东移在其中起到了关键性的作用。由于孟加拉湾槽前暖湿气流强盛,这种强盛的西南暖湿气流在低空冷空气堆(冷锋)上发生强烈的系统性上升运动,从而导致百色市及其邻近地区出现异常的雨雪天气。 相似文献