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121.
石墨炉原子吸收光谱法测定土壤样品中镉 总被引:5,自引:0,他引:5
采用磷酸氢二铵作基体改进剂塞曼扣背景石墨炉原子吸收光谱法测定土壤样品中镉,方法检出限DL=0.012μg/g,精密度RSD在3.55%~7.33%,满足了土壤样品中镉测定的镉质量要求。 相似文献
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Research relevance, 'knowledge transfer' and the geographies of CASE studentship collaboration 总被引:1,自引:0,他引:1
The Co-operative Awards in Science and Engineering (CASE) studentship programme of the UK Research Councils provide one example of wider efforts internationally to encourage so-called 'knowledge transfer' and thereby harness publicly supported university research more closely to the goals of national competitiveness, regional economic development and local regeneration. In this paper we describe the implications of how the various UK research councils have interpreted the objectives and beneficiaries of 'knowledge transfer', both for the relative opportunities available to human and physical geographers for collaboration through CASE and for the sorts of values that their research must serve. Then, we draw on unpublished data from the Economic and Social Research Council (ESRC) to explore the geographies of CASE studentship allocation and participation. The broad regional and institutional patterns of participation we describe have important implications for ongoing debates in the UK about research selectivity and the role of the university as an engine of local development, while the striking disciplinary patterns of CASE participation, and in particular the overwhelming success of geographers in this competitive programme, provide an opportunity to reassess claims about whether and for whom geographical research is relevant. 相似文献
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Sandro Fadda 《Geostandards and Geoanalytical Research》2005,29(1):143-156
Major concentrations of Al2O3, Fe2O3, MgO, CaO, Na2O and K2O, minor levels of TiO2, P2O5 and thirty petrologically, geochemically and environmentally significant trace elements have been determined in microwave oven acid leachates of whole powdered coal samples by direct current plasma‐atomic emission spectrometry (DCP‐AES). A single sample preparation procedure was suitable for all the determinations with no additional dilution step for major elements solution. Dried samples (0.5 g) were treated in low‐pressure PFA digestion vessels with HF/HCl/HNO3/HClO4 acids to quantitatively extract the analytes from the bulk material, while leaving the major part of organic matrix as a residue. The major constituents of geological samples, in particular the easily ionised elements (EIEs) such as alkali and alkaline earths, may complicate the instrumental determinations in DCP‐AES because of differential enhancements of elemental emission intensities and stray light interferences. Taking account of these factors, the coal matrix is considered to have very low major oxide totals as compared to many other common geo‐environmental and related materials (rocks, sediments, soil, ashes etc.). The sample size employed here, while yielding a relatively concentrated solution to cover a wide range of elemental determinations, provided a sample matrix that significantly diminished interferences for DCP measurements. The need for closely matching the unknowns and calibrators was eliminated except for overall acidity and an excess quantity of caesium for EIE buffering. Calibration of the spectrometer was accomplished by simple aqueous single element solutions as high concentration calibrators in addition to a reagent blank as a low concentration calibrator. Two point working curves were established to allow for the maximum concentrations of each element expected in the unknowns. The precision of determinations under routine conditions as well as the reproducibility of the leaching and precision of instrumental measurements have been evaluated. Relative standard deviations (RSD) were of 1–2% for those elements whose concentrations in solid samples were well above the limits of quantification. Method detection limits in the buffered solutions were also evaluated. To evaluate the accuracy of the microwave oven‐DCP method a suite of eight certified coal reference materials of differing rank, were analysed with good agreement with the certified and/or available published data. Results are presented for the uncertified major oxides in the AR series reference materials. 相似文献
126.
A new methodology for deriving the uplift load–displacement response of long driven piles in cohesionless soils is proposed. This method accounts for the effects of the friction fatigue processes during pile driving and the existence of locked-in residual stresses at the end of pile driving before commencing the pile load test. A hyperbolic formulation is utilized to simulate the nonlinear load transfer curves (the so-called t–z curves). The utility of this technique is demonstrated for a field pullout load test on a driven pile in sand. Predicted and measured load–displacement curves showed good agreement, indicating that this approach yields reasonable results as long as representative input parameters are employed. 相似文献
127.
珠江口盆地白云凹陷新生代构造演化动力学 总被引:42,自引:0,他引:42
白云凹陷构造演化史的研究对在白云凹陷开展油气勘探和深水沉积研究具有重要的意义。通过对断裂与沉积结构平面和剖面特点的分析,结合岩浆活动特点,文中提出白云凹陷是一个复式地堑,推测这种结构特点与凹陷下地壳的强烈韧性减薄和颈缩变形有关,表现为热岩石圈的伸展。其发育机制推测与白云凹陷位于构造转换带上有关,特殊的构造位置使白云凹陷成为强烈构造变形区,岩石圈地壳强烈减薄,伴随伸展过程和地幔上涌,脆性地壳或上地幔中部分熔融物质的出现导致岩石圈强度的急剧降低,在区域伸展应力场下以韧性流变方式减薄。岩浆在构造转换带下聚集并发育主岩浆房,由于白云凹陷南北边缘没有发育正断裂系统,岩浆主要沿垂直伸展的方向运移,因此在珠琼运动一幕和二幕南南东向伸展应力作用下,岩浆向白云凹陷的东部和西部运移至北西向基底深大断裂处,那里由于北西向断裂表现为左行张剪性质而成为压力较低的地区,从而成为岩浆上涌和侵位的地方。在岩浆聚集的地区,活动岩浆体附近的脆性变形被分散的韧性变形所取代,因此在凹陷的东北和西南两个角上,发育了张性和张剪性小断裂群,由于热岩石圈弹性较差,白云凹陷长期持续沉降。白云凹陷的断裂活动和沉积演化史还受到南海海盆扩张活动的影响。 相似文献
128.
对薄壁金刚石钻头胎体进行了性能分析和配方设计探讨,尤其根据被钻切介质对钻头胎体性能的要求作了较详细的分析,从理论分析结合实践经验筛选出了钻切建筑石材和各种钢筋砼的钻头胎体配方,在生产中满足了钻头工作条件的要求。 相似文献
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130.
Transient seepage analysis in zoned anisotropic soils based on the scaled boundary finite‐element method 下载免费PDF全文
The scaled boundary finite‐element method, a semi‐analytical computational scheme primarily developed for dynamic stiffness of unbounded domains, is applied to the analysis of unsteady seepage flow problems. This method is based on the finite‐element technology and gains the advantages of the boundary element method as well. Only boundary of the domain is discretized, no fundamental solution is required and singularity problems can be modeled rigorously. Anisotropic and non‐homogeneous materials satisfying similarity are modeled with no additional efforts. In this study, firstly, formulation of the method for the transient seepage flow problems is derived followed by its solution procedures. The accuracy, simplicity and applicability of the method are demonstrated via four numerical examples of transient seepage flow – three of them are available in the literature. Homogenous, non‐homogenous, isotropic and anisotropic material properties are considered to show the versatility of the technique. Excellent agreement with the finite‐element method is observed. The method out‐performs the finite‐element method in modeling singularity points. Copyright © 2014 John Wiley & Sons, Ltd. 相似文献