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91.
海水中234Th的超低水平液闪谱仪测定 总被引:2,自引:1,他引:2
本文提出了利用超低水平液闪谱仪测定海水中234Th的方法.海水经氢氧化铁吸附共沉淀富集后,接着用阴离子交换和TBP/煤油萃取进行Th同位素的分离与纯化.对一系列测定条件进行了详细的研究,提出了测定海水中234Th的适宜程序,即在含有234Th和产额示踪剂230Th的纯化后的5mol/dm3HNO3溶液中加入TBP/煤油进行萃取,然后用0.1mol/dm3HNO3反萃取,后者是先用契伦柯夫计数法测量234Th(通过234mPa),后加入闪烁液Hisafe 3用α/β模式测量α放射体230Th.对于α和β放射体液闪谱仪的计数效率分别为100%和55.7%±2.7%.234Th的化学回收率和总探测效率分别为70%~80%和30%~45%.该法测定海水中的234Th快速、简便和高效. 相似文献
92.
Nonlinear interactions between large waves and freely floating bodies are investigated by a 2D fully nonlinear numerical wave tank (NWT). The fully nonlinear 2D NWT is developed based on the potential theory, MEL/material-node time-marching approach, and boundary element method (BEM). A robust and stable 4th-order Runge–Kutta fully updated time-integration scheme is used with regriding (every time step) and smoothing (every five steps). A special φn-η type numerical beach on the free surface is developed to minimize wave reflection from end-wall and wave maker. The acceleration-potential formulation and direct mode-decomposition method are used for calculating the time derivative of velocity potential. The indirect mode-decomposition method is also independently developed for cross-checking. The present fully nonlinear simulations for a 2D freely floating barge are compared with the corresponding linear results, Nojiri and Murayama’s (Trans. West-Jpn. Soc. Nav. Archit. 51 (1975)) experimental results, and Tanizawa and Minami’s (Abstract for the 6th Symposium on Nonlinear and Free-surface Flow, 1998) fully nonlinear simulation results. It is shown that the fully nonlinear results converge to the corresponding linear results as incident wave heights decrease. A noticeable discrepancy between linear and fully nonlinear simulations is observed near the resonance area, where the second and third harmonic sway forces are even bigger than the first harmonic component causing highly nonlinear features in sway time series. The surprisingly large second harmonic heave forces in short waves are also successfully reproduced. The fully updated time-marching scheme is found to be much more robust than the frozen-coefficient method in fully nonlinear simulations with floating bodies. To compare the role of free-surface and body-surface nonlinearities, the body-nonlinear-only case with linearized free-surface condition was separately developed and simulated. 相似文献
93.
对南海南部ODP1143站氧同位素11-5e期大约2ka分辨率的粉红色Globigerinoides ruber进行分析,发现其冰期/间冰期旋回与代表全球冰量的底栖有孔虫氧同位素(δ^18O)的变化相反,即在间冰期时含量低,而冰期时高,与其他海区的记录相反。海水表层温度和温跃层深度转换函数结果以及碎壳率的变化显示,在一定的温度背景下,温跃层深度的变化可能是控制粉红色G.ruber冰期旋回的主要因素,而这段时期南海南部溶解作用的影响则不明显。 相似文献
94.
固定化鲅鱼乙酰胆碱酯酶的制备及部分性质测定 总被引:3,自引:0,他引:3
酶的固定化是酶传感器制备过程中重要的1个环节.研究采用直接共价法固定鲅鱼乙酰胆碱酯酶(AChE).制备方法为:0.1g CNBr活化的Sepharose 4B凝胶用1mmol/L的HCl充分溶胀后,与活力为10U的AChE溶液混合,于4℃下150r/min振荡8h.所制备的固定化酶活力回收率较高(96%),对pH值和温度变化的适应能力均优于非固定化酶;在3个月保存期内,前者的活力损失13%,而后者的活力则下降89%.这说明固定过程能够大大提高AChE的抗逆性和保持酶活力的稳定,有利于酶传感器的制备. 相似文献
95.
96.
A seismic refraction study on old (110 Myr) lithosphere in the northwest Pacific Basin has placed constraints on crustal and uppermantle seismic structure of old oceanic lithosphere, and lithospheric aging processes. No significant lateral variation in structure other than azimuthally anisotropic mantle velocities was found, allowing the application of powerful amplitude modeling techniques. The anisotropy observed is in an opposite sense to that expected, suggesting the tectonic setting of the area may be more complex than originally thought. Upper crustal velocities are generally larger than for younger crust, supporting current theories of decreased porosity with crustal aging. However, there is no evidence for significant thickening of the oceanic crust with age, nor is there any evidence of a lower crustal layer of high or low velocity relative to the velocity of the rest of Layer 3. The compressional and shear wave velocities rule out a large component of serpentinization of mantle materials. The only evidence for a basal crustal layer of olivine gabbro cumulates is a 1.5 km thick Moho transition zone. In the slow direction of anisotropy, upper mantle velocities increase from 8.0 km s-1 to 8.35 km s-1 in the upper 15 km below the Moho. This increase is inconsistent with an homogeneous upper mantle and suggests that compositinal or phase changes occur near the Moho. 相似文献
97.
太平洋海域海平面变化的灰色系统分析 总被引:3,自引:1,他引:3
应用灰色系统理论,对太平洋海域48个长期验潮站的月均海平面分别建立了GM(1,1)模型。GM(1,1)模型能较好地反映太平洋海域的海平面变化的趋势,它除了能给出连续的海平面变化速率外,同时能方便地给出海平面变化的加速率。模拟结果表明,在太平洋地壳均衡假设下,太平洋海域的月均海平面以平均速率0.17cm/a上升。在太平洋海域所取的48个长期验潮站中,有40个站在加速上升,全部站的平均加速度为0.00029cm/a2。且加速率逐渐增大。当然这些加速率都很小,但作为一种普遍性的趋势,这已足以说明:太平洋海域的海平面在加速上升 相似文献
98.
顶空气相色谱法测定海水二甲基硫和浮游植物细胞二甲基硫丙酸的研究 总被引:12,自引:2,他引:12
建立了顶空GC/FPD测定海水中二甲基硫(DMS)和浮游植物细胞中二甲基硫丙酸(DMSP)的方法,并研究盐度、温度、气液相比DMS诸因素对DMS顶空灵敏度的影响。该法对DMS测定的相对标准偏差均小于6%,平均回收率为106%,最低检出限为20ng/L。细胞DMSP先经碱作用转化为DMS,在50℃下作用时间不少于6h,峰高与浓度的双对数线性相关系数大于0.99。对1994年冬、1995年夏采自胶州湾 相似文献
99.
100.
In this study we test Talley's hypothesis that Oyashio winter mixed-layer water (26.5–26.6σ θ) increases its density to produce the North Pacific Intermediate Water (NPIW) salinity minimum (26.7– 26.8σθ) in the Mixed Water Region, assuming a combination of cabbeling and double diffusion. The possible density change of Oyashio
winter mixed-layer water is discussed using an instantaneous ratio of the change of temperature and salinity along any particular
intrusion (R
l
). We estimate the range of R
l
DD
required to convert Oyashio winter mixed-layer water to the NPIW salinity minimum due to double diffusion, and then assume
double-diffusive intrusions as this conversion mechanism. A double-diffusive intrusion model is used to estimate R
l
DD
in a situation where salt fingering dominates vertical mixing, as well as to determine whether Oyashio winter mixed-layer
water can become the NPIW salinity minimum. Possible density changes are estimated from the model R
l
DD
by assuming the amount of density change due to cabbeling. From these results, we conclude that Oyashio winter mixed-layer
water contributes to a freshening of the lighter layer of the NPIW salinity minimum (around 26.70σθ) in the MWR. 相似文献