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A. L.?Huber M.?Heuer K. T.?FehrEmail author K.?Bente E.?Schmidbauer G. D.?Bromiley 《Physics and Chemistry of Minerals》2004,31(2):67-79
Clinopyroxenes along the solid solution series hedenbergite (CaFeSi2O6)–petedunnite (CaZnSi2O6) were synthesized under hydrothermal conditions and different oxygen fugacities at temperatures of 700 to 1200 °C and pressures of 0.2 to 2.5 GPa. Properties were determined by means of X-ray diffraction, electron microprobe analysis and 57Fe Mössbauer spectroscopy at 298 K. Unit-cell parameters display a linear dependency with changing composition. Parameters a0 and b0 exhibit a linear decrease with increasing Zn content while the monoclinic angle increases linearly. Parameter c0 is not affected by composition and remains constant at a value of 5.248 Å. The molar volume can be described according to the equation Vmol (ccm mol–1)=33.963(16)–0.544(31)*Zn pfu. The isomer shifts of ferrous iron on the octahedral M1 site in hedenbergite are not affected by composition along the hedenbergite–petedunnite solid solution series and remain constant at an average value of 1.18 mm s–1. Quadrupole splittings of Fe2+ on the M1 are, however, strongly affected by composition, and they decrease linearly with increasing petedunnite component in hedenbergite, ranging from 2.25 mm s–1 for pure hedenbergite end member to 1.99 mm s–1 for a solid solution containing 84 mole% petedunnite. The half-widths of intermediate solid solutions vary between 0.26 and 0.33 mm s–1, indicating, in accordance with the microprobe analyses and X-ray diffraction, that samples are homogeneous and well-crystallized. The data from this study demonstrate that the crystallinity of hedenbergitic clinopyroxenes can be improved by using oxide mixtures as starting materials. Crystal sizes for intermediate compositions range up to 70 m, suitable for standard single-crystal X-ray analysis.This paper is dedicated to Prof. Dr. Georg Amthauer, Salzburg, on occasion of his 60th birthday 相似文献
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建立了Synthesis法前兆群体异常信息提取的数学模型。选取滇东地区1995-2000年9月间常用的20项前兆资料,研究中强地震前后Synthesis法前兆群体异常的变化特征。研究结果表明,在研究时段内,Synthesis法前兆群体异常占时率为0.158,为小概率事件。地震对应率为5/6=0.83,虚报率为1/6=0.17,地震均是在异常结束后3个月之内发生,是对应概率很高的短期预报指标。成组异常出现均有成组地震对应,群体前兆“组异常”特征显著。处于计算前兆观测点中心的澄江地震前,异常幅度突出,预示了Synthesis值计算有利于提取近源短期异常。实际检验了Synthesis法在地震短期预报中的预报意义,获得了满意的效果。 相似文献
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A practical and reliable method for the preparation of fine-grained forsterite and forsterite–enstatite polycrystals, in
the system MgO–SiO2, is described. The method employs state-of-the-art techniques from materials science, namely sol-gel synthesis, powder processing
and sintering. The resulting dense polycrystalline materials are homogeneously fine-grained (1–2 μm) and uniformly foam-textured.
Moreover, they are highly reproducible in composition and microstructure. The enstatite content can be controlled to within
∼1%, in the range 0–50%, and densities up to 98% of theoretical density can be achieved. The method thus yields polycrystalline
forsterite–enstatite material suitable for a range of geochemical, petrological and geophysical studies.
Received: 19 October 1999 / Accepted: 18 June 2001 相似文献
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K. Golap N. Udaya Shankar S. Sachdev R. Dodson Ch. V. Sastry 《Journal of Astrophysics and Astronomy》1998,19(1-2):35-53
A new, meter-wave radio telescope has been built in the north-east of Mauritius, an island in the Indian Ocean, at a latitude
of -20.14‡. The Mauritius Radio Telescope (MRT) is a Fourier Synthesis T-shaped array, consisting of a 2048 m long East-West
arm and an 880 m long South arm. In the East-West arm 1024 fixed helices are arranged in 32 groups and in the South arm 16
trolleys, with four helices on each, which move on a rail are used. A 512-channel digital complex correlation receiver is
used to measure the visibility function. At least 60 days of observing are required for obtaining the visibilities up to 880
m spacing. The Fourier transform of the calibrated visibilities produces a map of the area of the sky under observation with
a synthesized beam width 4′ × 4.6′ sec(δ + 20.14‡) at 151.5 MHz.
The primary objective of the telescope is to produce a sky survey in the declination range –70‡ to –10‡ with a point source
sensitivity of about 200 mJy (3a level). This will be the southern sky equivalent of the Cambridge 6C survey. In this paper
we describe the telescope, discuss the array design and the calibration techniques used, and present a map made using the
telescope. 相似文献
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提出一种以硫酸二甲酯和硫脲为基本原料的合成甲硫酸的改进方法。该方法的特点是:1.使S—甲基异硫脲硫酸盐的碱解直接在反应液中进行,而无需分离此中间体,从而使合成工艺大为简化,并能避免中间体在乙醇母液中的损失;2.甲硫酸的总产率可提高到70%以上,且能从反应液中回收副产物双氰胺。此法不仅适用于甲硫醇的实验室制备,而且能用于工业化生产。 相似文献
49.
17—115℃沥青铀矿的合成及其形成速度的实验研究 总被引:1,自引:0,他引:1
本文介绍了17—115℃沥青铀矿合成的方法及对产品的鉴定结果。实验是在只有六价铀与硫代乙酰胺存在的非常简单的体系中进行的。合成的最低温度为17℃。沥青铀矿的结晶速度在不同的温度和pH条件下是不同的。温度越高,结晶速度越快。在酸性溶液中沥青铀矿结晶速度快,中性中较慢,碱性中最慢。但随着温度的提高,酸、中、碱性溶液结晶速度的差值迅速缩小。82℃时,无论酸、中、碱性溶液中的沥青铀矿均能在半小时内结晶出来。 相似文献
50.
《Chemie der Erde / Geochemistry》2016,76(3):449-460
Four iron-containing natural oxalates, usually classified as organic minerals, are known (humboldtine, minguzzite, stepanovite and zhemchuzhnikovite). Their occurrences and general properties are presented and briefly discussed. The subsequent part of the review is devoted to the discussion of synthetic oxalato-complexes, analogous to these natural species, including usual synthetic procedures and a thorough analysis of their crystallographic and structural peculiarities. The thermal, spectroscopic and magnetic properties of these complexes are also analyzed in detail and comparisons with other closely related complexes are also included in the discussions. 相似文献