熔融制样-X射线荧光光谱法测定电气石中12种主次量元素     

夏传波  成学海  张会堂  赵伟  王卿 《岩矿测试》2018,37(1):36-42

电气石是一类含硼的铝硅酸盐矿物,化学成分复杂、化学稳定性强,不易湿法分解,B_2O_3含量较高,导致其主次量元素的同时测定存在一定困难。本文采用熔融法制样,建立了X射线荧光光谱法测定电气石Na_2O、MgO、Al_2O_3、SiO_2、P_2O_5、K_2O、CaO、TiO_2、V_2O_5、Cr_2O_3、MnO、TFe_2O_3等主次量元素的分析方法。样品与四硼酸锂-偏硼酸锂-氟化锂(质量比为4.5∶1∶0.4)混合熔剂的稀释比例为1∶10,消除了粒度效应和矿物效应;在缺少电气石标准物质的情况下,选择土壤、水系沉积物及多种类型的地质标准物质绘制校准曲线,利用含量与电气石类似的标准物质验证准确度,测定结果的相对标准偏差小于4.2%。采用所建方法测定四种不同类型电气石实际样品,测定值与经典化学法基本吻合。本方法解决了电气石不易湿法分解和硼的干扰问题,测定结果准确可靠,与其他方法相比操作简便,分析周期短。  相似文献   

海上高产高含蜡井测试工艺优化研究和应用          下载免费PDF全文

冯大龙  黄伟  谭振兴  袁则名 《探矿工程》2021,48(6):39-43

为研究海上高产高含蜡油气井测试工艺优化方案,以东海西湖凹陷某井测试作业中所暴露出的问题为导向,开展西湖高产高含蜡储集层测试问题原因分析和国内外技术调研,同时进行了测试管柱和地面测试流程的流动性保障技术研究及原油燃烧保障技术研究。研究表明地面流程结蜡、大油嘴放喷返排出大颗粒碎屑及大产量原油燃烧导致燃烧头损坏是影响测试的主要原因,因此对测试管柱、地面测试流程及燃烧保障等进行工艺优化,以解决高产高含蜡油气井测试相关问题。  相似文献   

Brittleness index predictions from Lower Barnett Shale well-log data applying an optimized data matching algorithm at various sampling densities     

David A.Wood 《地学前缘(英文版)》2021,12(6):444-457

The capability of accurately predicting mineralogical brittleness index(BI)from basic suites of well logs is desir-able as it provides a useful indicator of the fracability of tight formations.Measuring mineralogical components in rocks is expensive and time consuming.However,the basic well log curves are not well correlated with BI so correlation-based,machine-learning methods are not able to derive highly accurate BI predictions using such data.A correlation-free,optimized data-matching algorithm is configured to predict BI on a supervised basis from well log and core data available from two published wells in the Lower Barnett Shale Formation(Texas).This transparent open box(TOB)algorithm matches data records by calculating the sum of squared errors be-tween their variables and selecting the best matches as those with the minimum squared errors.It then applies optimizers to adjust weights applied to individual variable errors to minimize the root mean square error(RMSE)between calculated and predicted(BI).The prediction accuracy achieved by TOB using just five well logs(Gr,pb,Ns,Rs,Dt)to predict BI is dependent on the density of data records sampled.At a sampling density of about one sample per 0.5 ft BI is predicted with RMSE～0.056 and R2～0.790.At a sampling density of about one sample per 0.1 ft BI is predicted with RMSE～0.008 and R2～0.995.Adding a stratigraphic height index as an additional(sixth)input variable method improves BI prediction accuracy to RMSE～0.003 and R2～0.999 for the two wells with only 1 record in 10,000 yielding a BI prediction error of＞±0.1.The model has the potential to be applied in an unsupervised basis to predict BI from basic well log data in surrounding wells lacking mineralogical measure-ments but with similar lithofacies and burial histories.The method could also be extended to predict elastic rock properties in and seismic attributes from wells and seismic data to improve the precision of brittleness index and fracability mapping spatially.  相似文献   

Coupled finite‐element simulation of injection well testing in unconsolidated oil sands reservoir     

Bin Xu  Ron C.K. Wong 《国际地质力学数值与分析法杂志》2013,37(18):3131-3149

This paper presents a finite‐element (FE) model for simulating injection well testing in unconsolidated oil sands reservoir. In injection well testing, the bottom‐hole pressure (BHP) is monitored during the injection and shut‐in period. The flow characteristics of a reservoir can be determined from transient BHP data using conventional reservoir or well‐testing analysis. However, conventional reservoir or well‐testing analysis does not consider geomechanics coupling effects. This simplified assumption has limitations when applied to unconsolidated (uncemented) oil sands reservoirs because oil sands deform and dilate subjected to pressure variation. In addition, hydraulic fracturing may occur in unconsolidated oil sands when high water injection rate is used. This research is motivated in numerical modeling of injection well testing in unconsolidated oil sands reservoir considering the geomechanics coupling effects including hydraulic fracturing. To simulate the strong anisotropy in mechanical and hydraulic behaviour of unconsolidated oil sands induced by fluid injection in injection well testing, a nonlinear stress‐dependent poro‐elasto‐plastic constitutive model together with a strain‐induced anisotropic permeability model are formulated and implemented into a 3D FE simulator. The 3D FE model is used to history match the BHP response measured from an injection well in an oil sands reservoir. Copyright © 2013 John Wiley & Sons, Ltd.  相似文献   

热解石墨坩埚的应用     

张恩慈  吴贤欣 《岩矿测试》1990,9(2):138-141

本文介绍本院研制的热解石墨坩埚的特性和应用情况。该坩埚具有纯度高、致密、耐高温、耐强酸强碱腐蚀、易洗涤等特点,已广泛应用于矿物、建材、玻璃等方面试样的前处理。与铂、银、镍、刚玉、石英等坩埚比较,具有引入杂质少成本低等优点。  相似文献   

纵观近代岩矿测试分析技术   总被引：1，自引：0，他引：1  

祖振杰  叶松 《地学前缘》1994,(Z1)

本文就近代岩矿测试分析技术作了较为全面的介绍。文章指出，地矿部从８０年代起，由于引进了大批现代先进仪器设备，使岩矿测试分析技术出现了崭新面貌，形成为多学科相结合的新格局，从而促进地质科学在理论上和实践上均取得显著进步，在某些学科领域已发生了根本性变化，并为地质或其它市场提供了大量信息，为促进科技成果转化为生产力作出了巨大贡献。纵观近代岩矿测试分析技术，文章提出了多机联用、整体分析和拓宽测试分析领域的建议，以更好地为祖国经济主战场服务。  相似文献   

反循环中心取样雾化钻探应用于砾岩型金矿取样地质效果及其编录方法     

刘宝成  袁力 《吉林地质》1994,13(2):75-81

中心取样钻探是一种全新的钻探方法，具有效率快、取样准确、岩样采取率高的特点。可用于砾岩型金矿勘探评价，获取的矿层深度、品位、厚度、岩心采取率等均能满足地质要求，利用回返物质能够进行正常地质编录。  相似文献   

离子质谱计测定地质样品中镁同位素组成方法学研究     

周瑶琪  柴之芳 《岩矿测试》1995,14(1):7-14

应用信通公司研制的离子质谱计（ＳＴ－ＩＭＳ），建立了地质样品镁同位素分析的实验流程和误差分析方法，为进一步分析微量地质样品中镁同位素组成和分布奠定了基础。  相似文献   

The variogram sill and the sample variance   总被引：1，自引：0，他引：1  

Randal J. Barnes 《Mathematical Geology》1991,23(4):673-678

The relationship between the sill of the variogram and the sample variance is explored. The common practice of using the sample variance as an estimate of the variogram sill is questioned, and a conceptual framework for determining the appropriateness of this heuristic is constructed.  相似文献   

高精度锥体棱镜的“自差法”检测技术   总被引：2，自引：0，他引：2  

殷达安  林银森 《测绘学报》1994,23(3):216-221

本文提出一种采用“自差法”检测高精度锥体棱镜的新方法，阐述检测原理与装置，建立检测角度和面形误差的定量判据，并给出一个实例说明其应用。实践表明，“自差法”检测技术对于产品质量的控制，具有快速准确和简便实用等特点。  相似文献