液闪法测量水中氚放射性活度的淬灭效应   总被引：3，自引：2，他引：1  

张向阳  刘福亮  张琳  郭华良 《岩矿测试》2010,29(4):469-471

采用液体闪烁计数法进行放射性同位素测量时存在淬灭效应,而且几乎每个样品的淬灭程度都不同,并影响测量精度。采用液体闪烁计数法测量水中氚的放射性活度,淬灭是难以避免的,因此要进行淬灭校正,才能使不同淬灭程度的样品的测量结果具有可比性。淬灭校正的方法有很多,外标准校正法是一种比较可靠的方法。文章采用氚外标准校正法进行实验,得出淬灭校正曲线即探测效率E与淬灭参数SQP(E)的关系式为E=0.001 3SQP(E)-0.707 6,经过样品验证,该曲线是可靠的。采用外标准校正法适合于大批样品的测量。  相似文献   

波束角偏差对多波束测量的影响及校正     

董庆亮  孙昊  张哲  李明叁 《海洋测绘》2014,34(5):27-30

波束角偏差是影响多波束系统测量精度的因素之一,严重时导致测量的海底地形成凸凹形状的伪地形。论述了波束角偏差产生的原因以及对多波束系统测量精度的影响,介绍了借用EM系列多波束系统配置的横向参数校准软件对波束角偏差进行校正的方法,经实际应用,该方法很好地校正了波束角偏差,提高了测量数据的精度。  相似文献   

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陈钊  李辉  邢乐林  孙少安  张晓彤  张品 《大地测量与地球动力学》2014,34(2):27-30

???????????????????????????????????????????????????80 cm??130 cm??????????????????????仯??????0.02×10^-8 ms^-2/cm??????????仯????仯??????????????????????FG5??A10???????????????????????????????????????????????????仯????????  相似文献   

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����Ӣ  �¹�  ������  ��־��  ����� 《大地测量与地球动力学》2014,34(6):114-118

??????????????(BDS)???????????????????????????и???????????????????????????????????????????????t??????????????????????????????????BDS??????????????????????????????????????????t??????????????????????cm/s?????????????λ???????????????????????????mm/s???????????????У????????????????????????豸????????????????cm/s??????????????????????????????豸????????????????dm/s????????????????????????????????????????  相似文献   

商业平板式超滤膜包完整性检验：对海洋胶体生物地球化学研究的启示     

LIN Liangshi  CAI Yihu  SUN Xiuwu  CHEN Min 《海洋学报(英文版)》2014,33(9):109-116

The performance and integrity of a cassette cross-flow ultrafilter(Pellicon 2, Millipore) are examined with a suite of macromolecules of different molecular masses. The retention coefficient during the cross-flow ultrafiltration experiments increases with increasing molecular mass and reaches 90% with 10 kDa dextran in both milli-Q water and ultrafiltered seawater media. Based on a 90% retention coefficient, the molecular mass cut-off for the ultrafiltration membrane is defined at 10 kDa, which is ten times(1 kDa) that rated by the manufacturer. To further validate the accuracy of the laboratory calibration, the samples from the lower Zhujiang River and the Jiulong River Estuary are ultrafiltered with the cassette ultrafiltration membrane and the colloidal organic carbon abundances in these samples are quantified with the ultrafiltration permeation model based on time series permeation subsamples. The colloidal organic carbon abundances are 5.8%–21.1% in the Jiulong River Estuary and 5.6%–11.0% in the lower Zhujiang River. These are consistent with the reported values for both estuaries as well as with the colloidal organic carbon abundances in marine environments over the coastal and open oceans with 10 kDa cut-off membranes. Therefore, these field data support the laboratory calibration result and indicate the validity of the experimental and quantification procedure adopted. The discrepancy between the nominal molecular mass cut-off and the actual pore size of the ultrafiltration membrane should be of great concern for research in colloidal and nanoparticle biogeochemistry. Careful examination of the membrane integrity should be taken during ultrafiltration experiments in order to avoid misleading molecular mass cut-off information.  相似文献   

天宫一号超光谱仪红外谱段的实验室定标     

黄小仙  傅雨田 《遥感学报》2014,18(Z1):35-41

天宫一号超光谱仪红外谱段光谱范围是8.0—10.5 μm,采用红外线列焦平面推扫方式成像.通过实验室定标实验,获得了每个探测元对应的辐射响应系数和响应线性度,并得到每一探测元的动态范围与噪声等效温差,验证了图像输出校正效果,同时,根据定标实验误差来源分析计算了最终的辐射定标误差.  相似文献   

GNSS约束的MERSI/FY-3A PWV校准方法EI北大核心CSCD     

赵庆志  杜正  姚顽强  姚宜斌 《测绘学报》2022,51(2):159-168

精确的水汽信息对于短临天气预警和长期气候监测具有重要意义。本文针对搭载在我国第2代极轨卫星风云三号A星(FY-3A)上中分辨率光谱成像仪(medium-resolution spectral imager,MERSI)获取水汽精度较低的现状,提出一种GNSS约束的MERSI/FY-3A PWV校准方法。首先,对MERSI/FY-3A的PWV段产品进行处理得到水汽日产品,并利用GNSS和无线电探空(radiosonde,RS)数据对其进行评估;然后,根据PWV的季节分布特性,构建GNSS约束的MERSI/FY-3A PWV季节自适应校准模型;最后,分别利用GNSS、RS和再分析资料对校准后的MERSI/FY-3A水汽进行对比,验证提出方法的有效性。研究表明:本文提出的PWV校准方法,能够有效改善MERSI/FY-3A水汽日产品和旬产品的精度,改善率分别为58.63%和68.72%。该方法可为遥感水汽快速校准研究提供重要的理论依据。  相似文献   

LA‐ICP‐MS Analysis of Small Samples: Carbonate Reference Materials and Larval Fish Otoliths     

Angélique V. Lazartigues  Pascal Sirois  Dany Savard 《Geostandards and Geoanalytical Research》2014,38(2):225-240

This article proposes a methodology to analyse the composition of very small carbonate samples such as larval fish otoliths. The chemical composition of otoliths, which are carbonate structures in the inner ear, is often used to explore population dynamics in fishes. Recent advances in laser ablation‐inductively coupled plasma‐mass spectrometry have suggested its potential application to this field. In this study, analyses were performed using a 193 nm ArF Resonetics LA system, coupled to an Agilent 7700X‐ICP‐MS, with the following ablation parameters: a beam diameter of 5 μm, energy of 3 mJ, 2.7 J cm^?2, laser repetition rate of 10 Hz and translation speed of 2.5 μm s^?1. NIST SRM 610 glass was used as the primary calibration material. Performing this protocol, characterisation of a USGS GP‐4 reference material was achieved with suitable precision and accuracy, but the USGS MACS‐3 reference material appeared more heterogeneous under the ablation conditions tested. Calibration was performed using two different beam diameters (5 and 11 μm). Capelin (Mallotus villosus) otoliths measuring between 10 and 20 μm in diameter were tested. Even though a smaller beam diameter and lower energy were used compared with those normally employed to analyse larger otoliths, the method was successful.  相似文献   

基于加速器控制网的GPS绝对测量精度探讨     

马娜  董岚  梁静  向伟  罗涛  王铜  刘璨  柯志勇  何振强 《北京测绘》2014,(6):23-27

针对当前散裂中子源准直测量控制网空间距离大、绝对精度要求高,常规测量难以满足需要的问题,提出采用不受通视限制、高精度的GPS测量解决,通过GPS在“标准检测场”准直实验,计算分析后处理软件、观测仪器及观测时长对GPS绝对测量精度的影响,结果表明,1km的测区范围,商业软件解算结果优于科研软件,且商业软件中TTC解算精度最高;分体机比一体机观测精度更高,但随观测时长增长,二者精度相当;观测时长超过8小时以上,基线值将趋于稳定。  相似文献   

经纬仪与视觉深度组合测量     

于英  范百兴  向民志 《测绘工程》2014,(4):40-44

组合测量是精密大尺寸测量的重要研究方向,提出一种经纬仪与视觉深度组合测量方法,对方法的原理以及其中的标定技术和高精度中心定位技术进行论述。精度验证实验表明,组合技术的定位测量精度优于0.05mm,准直精度优于2″,证明测量方法的正确性和可行性。  相似文献