Recommended Values of ²³⁹Pu, ²⁴⁰Pu and ^239+240Pu Concentrations in Reference Material IAEA-315 (Marine Sediment) Estimated by Thermal Ionisation Mass Spectrometry, Inductively Coupled Plasma-Mass Spectrometry and Alpha Spectrometry     

Taeko Shinonaga  Helmuth Aigner  Dilani Klose  Peter Spinder  Heinz Fröschl  David Donohue 《Geostandards and Geoanalytical Research》2008,32(1):93-101

The recommended concentrations of ²³⁹Pu, ²⁴⁰Pu and ^239+240Pu in reference material IAEA‐315 (marine sediment) were estimated by three analytical methods: isotope dilution thermal ionisation mass spectrometry (TIMS), isotope dilution inductively coupled plasma‐mass spectrometry (ICP‐MS) and alpha spectrometry. The determination of ²³⁹Pu and ²⁴⁰Pu (^239+240Pu by alpha spectrometry) was carried out with samples from randomly selected bottles using each method. Plutonium‐238 was also measured by alpha spectrometry. A plutonium‐242 reference material was used as a spike for the quantitative analysis. The influence of ²⁴²Pu in the samples was therefore calculated; however, this contribution was less than the range of uncertainty and did not influence the final results. The obtained data were statistically analysed using variance component analysis and paired comparison. The combined standard uncertainties from “method/measurement”, “bottle” and “sub‐sample” were in the order of 3 to 6%. The main contributions to the uncertainty were from the material heterogeneity and from systematic differences between methods. Based on this study with twenty‐seven analyses using 10–14 g sample mass, concentrations of (38 ± 3) Bq kg^?1, (28 ± 3) Bq kg^?1 and (66 ± 4) Bq kg^?1 are proposed as recommended values for ²³⁹Pu, ²⁴⁰Pu and ^239+240Pu, respectively, and (9.5 ± 0.4) Bq kg^?1 for ²³⁸Pu as an information value in reference material IAEA‐315. In mass concentration units, these amount to (16.4 ± 1.2) ng kg^?1, (3.3 ± 0.4) ng kg^?1 and (0.015 ± 0.003) ng kg^?1 for ²³⁹Pu, ²⁴⁰Pu and ²³⁸Pu, respectively. The certified reference materials NIST 4350B and NIST 4354 were also analysed by TIMS for quality assurance of the method used in this study.  相似文献   

应用GPS数据与重力数据确定大地水准面     

于小平  张廷玉  刘财  陈增宝  许惠平  庞贺民 《吉林大学学报(地球科学版)》2008,38(5)

作为GPS/重力边值问题理论及方法的应用,在对GPS/重力方法确定(似)大地水准面的原理进行简要介绍与分析的基础上,利用收集到的N区的600个GPS/重力数据和48个高精度GPS水准数据,计算出该区域的(似)大地水准面。通过拟合法和系统差直接改正法进行的精度分析表明,应用GPS/重力数据结合水准方法确定的该地区(似)大地水准面的精度达到厘米级精度。  相似文献   

Extreme value analysis of diamond-size distributions     

J. Caers  P. Vynckier  J. Beirlant  L. Rombouts 《Mathematical Geology》1996,28(1):25-43

Extreme value analysis provides a semiparametric method for analyzing the extreme long tails of skew distributions which may be observed when handling mining data. The estimation of important tail characteristics, such as the extreme value index, allows for a discrimination between competing distribution models. It measures the thickness of such long tailed distributions, if only a limited sample is available. This paper stresses the practical implementation of extreme value theory, which is used to discriminate a lognormal from a mixed lognormal distribution in a case study of size distributions for alluvial diamonds.  相似文献   

地震学定量预报指标的一种提取方法——对比筛选法     

周翠英  蒋海昆  王红卫  姜早峰 《地震》1994,(4)

鉴于目前地震学综合定量预报指标的缺乏和预报工作的急需,尝试使用“对比筛选法(简称CSM方法)”进行地震学定量预报指标的提取试验。较之以往作法的进展在于:1.同时使用“有震”和“无震”两类样本对比筛选;2.对不同地区的地震学参数进行了归一化处理。这样做的显著优点是:1.可以较有效地提取“有震异常”和“正常变化”指标;2.提取的异常和预报指标具有定量化和普适性特点。 试验研究使用大华北地震区资料,研究对象取中强地震。经内符和外推检验,证明该方法提取的异常和预报指标有效性和实用性较高。  相似文献   

地震综合效应场函数及其在地震预报中的应用──（一）地震综合效应场函数及其计算方法     

罗兰格 《华北地震科学》1994,(3)

在系统地分析了目前各种测震学地震预报方法科学思路的基础上,认为测震学地震预报方法基本上可以分为两大类。一类是以已经发生的一些地震作为未来可能发生的地震的“因”,即由于已经发生的地震对区域应力场的影响,导致未来发生较强地震。这一类包括的预报方法较多,如空区、条带、ｂ值、地震迁移、相关地震等等及其由此衍生出来的各种方法。另一类是把已经发生的一些地震作为区域应力场增强的“果”,即已经发生的地震是区域应力场增强过程中的一种反映,而未来地震不一定是已经发生的地震所导致的结果。这一类包括“地震窗口”、小震群活动等方法。针对第一类方法,各种预报方法都是力图从地震三要素中提取未来地震的信息,而具体作法又都是利用地震三要素这个多维空间的某个剖面。为了从地震活动诸要素的多维空间提取综合信息,我们对每个地震加入了破裂面方位,构成了地震第四要素,并依据地震４要素建立了地震综合效应场函数。地震综合效应场函数概括了多种测震学地震预报方法的科学思路和预报经验,从而可以形成测震学的综合预报方法。  相似文献   

浙闽山区茶叶生产基地评价的探讨   总被引：6，自引：0，他引：6  

华熙成 《地理研究》1994,13(3):98-103

茶叶基地的评价包括对基地的自然和经济条件的评估,应用系统分析方法,将自然和经济条件进行定量的综合评估,用综合评价值区分基地间的差异,最后定性与定量相结合,提出茶叶生产基地的合理布局.  相似文献   

Prediction of the occurrence of Related Strong Earthquakes in Italy     

Inessa A. Vorobieva  Giuliano F. Panza 《Pure and Applied Geophysics》1993,141(1):25-41

In the seismic flow it is often observed that a Strong Earthquake (SE), is followed by Related Strong Earthquakes (RSEs), which occur near the epicenter of the SE with origin time rather close to the origin time of the SE. The algorithm for the prediction of the occurrence of a RSE has been developed and applied for the first time to the seismicity data of the California-Nevada region and has been successfully tested in several regions of the world, the statistical significance of the result being 97%. To date it has been possible to make five successful forward predictions, with no false alarms or failures to predict.The algorithm is applied here to the Italian territory, where the occurrence of RSEs is a particularly rare phenomenon. Our results show that the standard algorithm is successfully directly applicable without adjustment of the parameters. Eleven SEs are considered. Of them, three are followed by a RSE, as predicted by the algorithm, eight SEs are not followed by a RSE, and the algorithm predicts this behaviour for seven of them, giving rise to only one false alarm. Since, in Italy, often the series of strong earthquakes is relatively short, the algorithm has been extended to handle such a situation. The result of this experiment indicates that it is possible to attempt to test a SE, for the occurrence of a RSE, soon after the occurrence of the SE itself, performing timely preliminary recognition on reduced data sets. This fact, the high confidence level of the retrospective analysis, and the first successful forward predictions, made in different parts of the World, indicates that, even if additional tests are desirable, the algorithm can already be considered for routine application to Civil Defence.  相似文献   

首都减灾圈的思考与建议     

张少泉  吕庆书 《地震》1993,(5):47-61

首都减灾圈,系首都减轻自然灾害预测防治圈。1991年12月20—21日在北京召开了《首都圈自然灾害及其减灾对策研讨会》。本文根据这次会议所提供的材料,在从整体上实现减灾的思想指导下,就首都减灾圈的“成灾背景”、“首都减灾圈的组成”、“首都减灾圈的灾害预测与防治状况”、“首都减灾圈的灾害关联性分析”、“首都减灾圈的减灾实效预估”和“首都减灾圈的减灾对策与实施”等六个带有共同性的问题,进行了讨论。供制定首都圈减灾方案时参考。  相似文献   

新疆地震预报研究     

朱令人 《内陆地震》1993,7(2):90-105

新疆的地震预报是1970年开始的。二十多年来在“边观测、边研究、边预报”、“多路探索、多兵种联合作战”、“走综合预报之路”的方针指导下取得了长足的进展。建设了43个地震台站,投入189套仪器,建成了遍布全疆的地震无线通讯网,开展了历史地震调查和地震烈度区划工作,建立健全了地震会商预报制度,进行了多方面的地震预报研究。实际地震预报统计分析表明,扣除自然发震概率之后,趋势预报的成功率约0.3,短临预报的成功率约0.1。在前兆台网控制范围内取得了一些震例,说明地震确实是有前兆的,但又是非常复杂的。地震预报作为科学难题还有漫长的路要走。作者简要地讨论了地震观测的间接性和地震异常的离散性、难以区别的地震异常和地壳变动异常、建立在复杂现象基础上的地震前兆以及地震的混沌性对地震预报的影响等科学问题。  相似文献   

大别杂岩中混合岩的矿物空间分布研究   总被引：2，自引：0，他引：2  

王江海 《岩石矿物学杂志》1993,12(3):243-250

介绍了矿物空间分布研究的基本原理及两种统计方法(接触频数法和线切法)。作者对混合岩矿物空间分布的研究表明:(1)前人提出的统计方法存在方法上的缺陷和应用上的局限性,作者推导出矿物接触类型的概率公式;(2)部分浅色体中矿物显示聚集分布的特征,而绝大部分的浅色体中矿物具有分散分布的特点。结合质量平衡和地球化学研究认为:大别杂岩中主体混合岩成因机制是重熔和交代作用。  相似文献